Use of oxygen/nickel ratios in the XPS characterisation of oxide phases on nickel metal and nickel alloy surfaces
► The O/Ni atomic ratios for a number of Ni oxides were calculated. ► The O/Ni ratios found to correspond well with the expected stoichiometry. ► Metal 2p peak shapes and O/Ni ratios used to estimate proportions of mixed oxides on metal surfaces. The O/Ni ratios derived from the X-ray photoelectron...
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| Published in | Journal of electron spectroscopy and related phenomena Vol. 185; no. 5-7; pp. 159 - 166 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.08.2012
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0368-2048 1873-2526 |
| DOI | 10.1016/j.elspec.2012.06.008 |
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| Abstract | ► The O/Ni atomic ratios for a number of Ni oxides were calculated. ► The O/Ni ratios found to correspond well with the expected stoichiometry. ► Metal 2p peak shapes and O/Ni ratios used to estimate proportions of mixed oxides on metal surfaces.
The O/Ni ratios derived from the X-ray photoelectron (XP) spectra of a number of well-characterised Ni oxides were calculated and found to correspond well to the expected O/Ni ratios for these oxides. The measured ratios, combined with the characteristic XP spectra, provide a higher level of confidence to the assignment of O 1s chemical species, particularly for surfaces with multiple phases present. As examples of this, we discuss the additional information imparted by O/Ni ratios measured for oxides that were electrochemically grown on Ni and NiCr-20% alloy surfaces. |
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| AbstractList | The O/Ni ratios derived from the X-ray photoelectron (XP) spectra of a number of well-characterised Ni oxides were calculated and found to correspond well to the expected O/Ni ratios for these oxides. The measured ratios, combined with the characteristic XP spectra, provide a higher level of confidence to the assignment of O 1s chemical species, particularly for surfaces with multiple phases present. As examples of this, we discuss the additional information imparted by O/Ni ratios measured for oxides that were electrochemically grown on Ni and NiCr-20% alloy surfaces. ► The O/Ni atomic ratios for a number of Ni oxides were calculated. ► The O/Ni ratios found to correspond well with the expected stoichiometry. ► Metal 2p peak shapes and O/Ni ratios used to estimate proportions of mixed oxides on metal surfaces. The O/Ni ratios derived from the X-ray photoelectron (XP) spectra of a number of well-characterised Ni oxides were calculated and found to correspond well to the expected O/Ni ratios for these oxides. The measured ratios, combined with the characteristic XP spectra, provide a higher level of confidence to the assignment of O 1s chemical species, particularly for surfaces with multiple phases present. As examples of this, we discuss the additional information imparted by O/Ni ratios measured for oxides that were electrochemically grown on Ni and NiCr-20% alloy surfaces. |
| Author | Payne, B.P. McIntyre, N.S. Biesinger, M.C. |
| Author_xml | – sequence: 1 givenname: B.P. surname: Payne fullname: Payne, B.P. organization: Department of Chemistry, The University of Western Ontario, London, ON N6A 5B7, Canada – sequence: 2 givenname: M.C. surname: Biesinger fullname: Biesinger, M.C. organization: Surface Science Western, The University of Western Ontario, London, ON N6A 5B7, Canada – sequence: 3 givenname: N.S. surname: McIntyre fullname: McIntyre, N.S. email: smcintyr@uwo.ca organization: Department of Chemistry, The University of Western Ontario, London, ON N6A 5B7, Canada |
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| Snippet | ► The O/Ni atomic ratios for a number of Ni oxides were calculated. ► The O/Ni ratios found to correspond well with the expected stoichiometry. ► Metal 2p peak... The O/Ni ratios derived from the X-ray photoelectron (XP) spectra of a number of well-characterised Ni oxides were calculated and found to correspond well to... |
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| SubjectTerms | Alloying additive Atomic ratios Mathematical analysis Mixed phase oxides Ni oxides Nickel Nickel base alloys Oxides Phases Spectra X-ray photoelectron spectroscopy XPS |
| Title | Use of oxygen/nickel ratios in the XPS characterisation of oxide phases on nickel metal and nickel alloy surfaces |
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