Assessment of Eutectic Solvent-Based Liquid-Liquid Microextraction to Determine Ponceau-4R in Various Beverage Samples

A sensitive, rapid, efficient, inexpensive, and easy-to-use vortex-assisted eutectic solvent microextraction process was extended to quantify Ponceau-4R (PN4R) in beverage samples followed by spectrophotometric detection. Here, a green solvent consisting of tetrabutylammonium bromide: n-octanol at a...

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Published inAnalytical letters Vol. 57; no. 17; pp. 2942 - 2958
Main Authors Narouei, Abdolmanan, Rahmani, Mashaallah
Format Journal Article
LanguageEnglish
Published Abingdon Taylor & Francis 21.11.2024
Taylor & Francis Ltd
Subjects
Beverage samples
Beverages
deep eutectic solvent
Eutectics
Liquid-liquid extraction
microextraction
Octanol
Ponceau-4R
Solvents
Spectrophotometry
Tetrabutylammonium bromide
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Abstract A sensitive, rapid, efficient, inexpensive, and easy-to-use vortex-assisted eutectic solvent microextraction process was extended to quantify Ponceau-4R (PN4R) in beverage samples followed by spectrophotometric detection. Here, a green solvent consisting of tetrabutylammonium bromide: n-octanol at a ratio of 1:3 was tested in the PN4R microextraction process. Also, different parameters affecting PN4R quantification through deep eutectic solvent in the microextraction model, including microliter volumes of extraction solvent, concentration of salt, extraction time, and pH were studied using multivariate procedures. Using this model, the maximum response was achieved with a eutectic solvent volume of 262 μL, extraction time of 5.3 min, pH 6.7, and 0.9% salt with Desirability = 1. The linear range was determined in optimum conditions to be from 15 to 1200 μg L −1 . The enrichment factor and limit of detection were achieved to be 50-fold and 4.5 μg L −1 , respectively. The limit of quantitation was 15 μg L −1 . To monitor PN4R, this model has been used in fruit juice samples with favorable recoveries in the range of 97.8%-101%.
AbstractList A sensitive, rapid, efficient, inexpensive, and easy-to-use vortex-assisted eutectic solvent microextraction process was extended to quantify Ponceau-4R (PN4R) in beverage samples followed by spectrophotometric detection. Here, a green solvent consisting of tetrabutylammonium bromide: n-octanol at a ratio of 1:3 was tested in the PN4R microextraction process. Also, different parameters affecting PN4R quantification through deep eutectic solvent in the microextraction model, including microliter volumes of extraction solvent, concentration of salt, extraction time, and pH were studied using multivariate procedures. Using this model, the maximum response was achieved with a eutectic solvent volume of 262 μL, extraction time of 5.3 min, pH 6.7, and 0.9% salt with Desirability = 1. The linear range was determined in optimum conditions to be from 15 to 1200 μg L −1 . The enrichment factor and limit of detection were achieved to be 50-fold and 4.5 μg L −1 , respectively. The limit of quantitation was 15 μg L −1 . To monitor PN4R, this model has been used in fruit juice samples with favorable recoveries in the range of 97.8%-101%.
A sensitive, rapid, efficient, inexpensive, and easy-to-use vortex-assisted eutectic solvent microextraction process was extended to quantify Ponceau-4R (PN4R) in beverage samples followed by spectrophotometric detection. Here, a green solvent consisting of tetrabutylammonium bromide: n-octanol at a ratio of 1:3 was tested in the PN4R microextraction process. Also, different parameters affecting PN4R quantification through deep eutectic solvent in the microextraction model, including microliter volumes of extraction solvent, concentration of salt, extraction time, and pH were studied using multivariate procedures. Using this model, the maximum response was achieved with a eutectic solvent volume of 262 μL, extraction time of 5.3 min, pH 6.7, and 0.9% salt with Desirability = 1. The linear range was determined in optimum conditions to be from 15 to 1200 μg L−1. The enrichment factor and limit of detection were achieved to be 50-fold and 4.5 μg L−1, respectively. The limit of quantitation was 15 μg L−1. To monitor PN4R, this model has been used in fruit juice samples with favorable recoveries in the range of 97.8%–101%.
Author Rahmani, Mashaallah
Narouei, Abdolmanan
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Snippet A sensitive, rapid, efficient, inexpensive, and easy-to-use vortex-assisted eutectic solvent microextraction process was extended to quantify Ponceau-4R (PN4R)...
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SubjectTerms Beverage samples
Beverages
deep eutectic solvent
Eutectics
Liquid-liquid extraction
microextraction
Octanol
Ponceau-4R
Solvents
Spectrophotometry
Tetrabutylammonium bromide
Title Assessment of Eutectic Solvent-Based Liquid-Liquid Microextraction to Determine Ponceau-4R in Various Beverage Samples
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