Thermal Properties of Olive Pomace Filled Linear Low Density Polyethylene Bio-Composites
Differential scanning calorimetry (DSC) and thermo-gravimetric analysis (TGA) were performed to evaluate the influence of olive pomace flour (OPF) and a coupling agent (C) on linear low-density polyethylene (LLDPE) bio-composites. The glass transition temperature (T g ), melting temperature (T m ),...
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Published in | Journal of macromolecular science. Physics Vol. 60; no. 11; pp. 957 - 969 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
Published |
New York
Taylor & Francis
02.11.2021
Marcel Dekker, Inc |
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Abstract | Differential scanning calorimetry (DSC) and thermo-gravimetric analysis (TGA) were performed to evaluate the influence of olive pomace flour (OPF) and a coupling agent (C) on linear low-density polyethylene (LLDPE) bio-composites. The glass transition temperature (T
g
), melting temperature (T
m
), enthalpy of fusion (ΔH
m
), crystallization temperature (T
cryst
.
), heat of crystallization (ΔH
cryst
,
) and percent crystallinity (X
c
) were extracted from the DSC results. The degradation behavior was extracted from the TGA. T
g
value (-114 °C) was unaffected by the addition of both OPF and C. A sharp DSC T
m
peak, around 125 °C, was observed with its position being dependent on both filler and C contents. The ΔH
m
for the filler at 40% content decreased slightly, from 132 J/g for 0% filler to 123 J/g. TGA showed that the thermal degradation of LLDPE in the composite became easier upon increasing the OPF filler and coupling agent. |
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AbstractList | Differential scanning calorimetry (DSC) and thermo-gravimetric analysis (TGA) were performed to evaluate the influence of olive pomace flour (OPF) and a coupling agent (C) on linear low-density polyethylene (LLDPE) bio-composites. The glass transition temperature (T
g
), melting temperature (T
m
), enthalpy of fusion (ΔH
m
), crystallization temperature (T
cryst
.
), heat of crystallization (ΔH
cryst
,
) and percent crystallinity (X
c
) were extracted from the DSC results. The degradation behavior was extracted from the TGA. T
g
value (-114 °C) was unaffected by the addition of both OPF and C. A sharp DSC T
m
peak, around 125 °C, was observed with its position being dependent on both filler and C contents. The ΔH
m
for the filler at 40% content decreased slightly, from 132 J/g for 0% filler to 123 J/g. TGA showed that the thermal degradation of LLDPE in the composite became easier upon increasing the OPF filler and coupling agent. Differential scanning calorimetry (DSC) and thermo-gravimetric analysis (TGA) were performed to evaluate the influence of olive pomace flour (OPF) and a coupling agent (C) on linear low-density polyethylene (LLDPE) bio-composites. The glass transition temperature (Tg), melting temperature (Tm), enthalpy of fusion (ΔHm), crystallization temperature (Tcryst.), heat of crystallization (ΔHcryst,) and percent crystallinity (Xc) were extracted from the DSC results. The degradation behavior was extracted from the TGA. Tg value (–114 °C) was unaffected by the addition of both OPF and C. A sharp DSC Tm peak, around 125 °C, was observed with its position being dependent on both filler and C contents. The ΔHm for the filler at 40% content decreased slightly, from 132 J/g for 0% filler to 123 J/g. TGA showed that the thermal degradation of LLDPE in the composite became easier upon increasing the OPF filler and coupling agent. |
Author | Aljnaid, Malek Banat, Raid Al-Rawashdeh, Manal |
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Snippet | Differential scanning calorimetry (DSC) and thermo-gravimetric analysis (TGA) were performed to evaluate the influence of olive pomace flour (OPF) and a... |
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SubjectTerms | bio-composite Calorimetry Composite materials coupling agent Coupling agents Crystallization Density Differential scanning calorimetry Enthalpy Fillers Glass transition temperature Gravimetric analysis Heat of crystallization linear low-density polyethylene Low density polyethylenes Melt temperature Melting olive pomace filler Polyethylene Thermal degradation Thermal properties Thermodynamic properties Transition temperatures |
Title | Thermal Properties of Olive Pomace Filled Linear Low Density Polyethylene Bio-Composites |
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