High-entropy FeCoNiMnCu alloy coating on ferritic stainless steel for solid oxide fuel cell interconnects

A high-entropy alloy coating of FeCoNiMnCu was prepared on SUS 430 steel via magnetron sputtering for solid oxide fuel cell (SOFC) interconnects application. The coated steels were subject to thermal exposure in air at 800 °C for up to 10 weeks. Phase constituents, microstructure and area specific r...

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Published inJournal of alloys and compounds Vol. 908; p. 164608
Main Authors Zhao, Qingqing, Geng, Shujiang, Zhang, Yu, Chen, Gang, Zhu, Shenglong, Wang, Fuhui
Format Journal Article
LanguageEnglish
Published Lausanne Elsevier B.V 05.07.2022
Elsevier BV
Subjects
Chromium oxides
Cobalt
Copper
Diffusion coating
Diffusion layers
Electrical property
Entropy
Ferritic stainless steel
Ferritic stainless steels
High entropy alloys
High-entropy alloy coating
High-entropy spinel coating
Interconnections
Iron constituents
Magnetron sputtering
Manganese
Nickel
Oxidation
Oxidation resistance
Protective coatings
Solid oxide fuel cell interconnect
Solid oxide fuel cells
Spinel
Steel constituents
High-entropy alloy coating
High-entropy spinel coating
Electrical property
Oxidation
Solid oxide fuel cell interconnect
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Abstract A high-entropy alloy coating of FeCoNiMnCu was prepared on SUS 430 steel via magnetron sputtering for solid oxide fuel cell (SOFC) interconnects application. The coated steels were subject to thermal exposure in air at 800 °C for up to 10 weeks. Phase constituents, microstructure and area specific resistance (ASR) of the coated steel before and after the oxidation testing were investigated. Results indicated the alloy coating was thermally converted into a high-entropy spinel coating of (Fe,Co,Ni,Mn,Cu)3O4 after oxidation and a protective Cr2O3 layer was formed at the steel/coating interface. The (Fe,Co,Ni,Mn,Cu)3O4 spinel coating effectively suppressed growth of Cr2O3 layer and outward diffusion of Cr during the long term exposure. Scale ASR of the coated steel was as low as 6.59 mΩ·cm2 at 800 °C after 10 weeks. It indicates that (Fe,Co,Ni,Mn,Cu)3O4 is a promising coating material for SOFC metallic interconnects. •A high-entropy alloy coating of FeCoNiMnCu is sputtered on SUS430 steel.•The coating is thermally converted into a high-entropy (Fe,Co,Ni,Mn,Cu)3O4 spinel.•The spinel coating effectively suppresses growth of Cr2O3 and out-diffusion of Cr.•Area specific resistance of coated steel is sufficiently low after long term exposure.
AbstractList A high-entropy alloy coating of FeCoNiMnCu was prepared on SUS 430 steel via magnetron sputtering for solid oxide fuel cell (SOFC) interconnects application. The coated steels were subject to thermal exposure in air at 800 °C for up to 10 weeks. Phase constituents, microstructure and area specific resistance (ASR) of the coated steel before and after the oxidation testing were investigated. Results indicated the alloy coating was thermally converted into a high-entropy spinel coating of (Fe,Co,Ni,Mn,Cu)3O4 after oxidation and a protective Cr2O3 layer was formed at the steel/coating interface. The (Fe,Co,Ni,Mn,Cu)3O4 spinel coating effectively suppressed growth of Cr2O3 layer and outward diffusion of Cr during the long term exposure. Scale ASR of the coated steel was as low as 6.59 mΩ·cm2 at 800 °C after 10 weeks. It indicates that (Fe,Co,Ni,Mn,Cu)3O4 is a promising coating material for SOFC metallic interconnects. •A high-entropy alloy coating of FeCoNiMnCu is sputtered on SUS430 steel.•The coating is thermally converted into a high-entropy (Fe,Co,Ni,Mn,Cu)3O4 spinel.•The spinel coating effectively suppresses growth of Cr2O3 and out-diffusion of Cr.•Area specific resistance of coated steel is sufficiently low after long term exposure.
A high-entropy alloy coating of FeCoNiMnCu was prepared on SUS 430 steel via magnetron sputtering for solid oxide fuel cell (SOFC) interconnects application. The coated steels were subject to thermal exposure in air at 800 °C for up to 10 weeks. Phase constituents, microstructure and area specific resistance (ASR) of the coated steel before and after the oxidation testing were investigated. Results indicated the alloy coating was thermally converted into a high-entropy spinel coating of (Fe,Co,Ni,Mn,Cu)3O4 after oxidation and a protective Cr2O3 layer was formed at the steel/coating interface. The (Fe,Co,Ni,Mn,Cu)3O4 spinel coating effectively suppressed growth of Cr2O3 layer and outward diffusion of Cr during the long term exposure. Scale ASR of the coated steel was as low as 6.59 mΩ·cm2 at 800 °C after 10 weeks. It indicates that (Fe,Co,Ni,Mn,Cu)3O4 is a promising coating material for SOFC metallic interconnects.
ArticleNumber 164608
Author Zhu, Shenglong
Geng, Shujiang
Wang, Fuhui
Zhang, Yu
Chen, Gang
Zhao, Qingqing
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  givenname: Fuhui
  surname: Wang
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  organization: Shenyang National Laboratory for Materials Science, Northeastern University, No. 3-11 Wenhua Road, Shenyang 110819, China
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Keywords High-entropy alloy coating
High-entropy spinel coating
Electrical property
Oxidation
Solid oxide fuel cell interconnect
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Snippet A high-entropy alloy coating of FeCoNiMnCu was prepared on SUS 430 steel via magnetron sputtering for solid oxide fuel cell (SOFC) interconnects application....
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StartPage 164608
SubjectTerms Chromium oxides
Cobalt
Copper
Diffusion coating
Diffusion layers
Electrical property
Entropy
Ferritic stainless steel
Ferritic stainless steels
High entropy alloys
High-entropy alloy coating
High-entropy spinel coating
Interconnections
Iron constituents
Magnetron sputtering
Manganese
Nickel
Oxidation
Oxidation resistance
Protective coatings
Solid oxide fuel cell interconnect
Solid oxide fuel cells
Spinel
Steel constituents
Title High-entropy FeCoNiMnCu alloy coating on ferritic stainless steel for solid oxide fuel cell interconnects
URI https://dx.doi.org/10.1016/j.jallcom.2022.164608
https://www.proquest.com/docview/2667261837
Volume 908
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