Steady self-scrolling of graphene sheets upon the solvation status of adsorbed polyhexylthiophene
Upon the tuning of solvent composition, the unfavorable solvation of adsorbed polyhexylthiophene is found able to drive graphene sheets to scroll steadily in solutions, resulting in nanoscrolls with a central void and regular stacking of internal layers. For theses steadily evolved graphene nanoscro...
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| Published in | Polymer (Guilford) Vol. 224; p. 123758 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
14.05.2021
Elsevier BV |
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| Online Access | Get full text |
| ISSN | 0032-3861 1873-2291 |
| DOI | 10.1016/j.polymer.2021.123758 |
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| Abstract | Upon the tuning of solvent composition, the unfavorable solvation of adsorbed polyhexylthiophene is found able to drive graphene sheets to scroll steadily in solutions, resulting in nanoscrolls with a central void and regular stacking of internal layers. For theses steadily evolved graphene nanoscrolls, the interlayer distance is subject to the average radius of adsorbed molecular coils and the bending rigidity of graphene hexagonal structural units restricts the reachable curvature of central voids. When the unfavorable solvation is progressively lessened upon slow crystallization of adsorbed polyhexylthiophene molecules, the reverse unwrapping ensues accordingly. On the other hand, the solvent evaporation initiates the dense growth of crystalline whiskers outward from graphene nanoscrolls and thus results in comb-like superstructures. With mutual impingement effects associated with present superstructures, oriented assembly and growth behaviors of crystalline whiskers are able to occur, creating nematic fields of crystalline whiskers.
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•The step-by-step advancement of steady graphene self-scrolling in solutions.•The adjustable solvation status of adsorbed molecules identified as the driving force of graphene self-scrolling.•Two identified thermodynamic regulating factors of graphene self-scrolling.•The dense outward growth of P3HTcrystalline whiskers on graphene nanoscrolls and evolved comb-like superstructures.•The self-organization of P3HT crystalline whiskers into nematic fields around comb-like superstructures. |
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| AbstractList | Upon the tuning of solvent composition, the unfavorable solvation of adsorbed polyhexylthiophene is found able to drive graphene sheets to scroll steadily in solutions, resulting in nanoscrolls with a central void and regular stacking of internal layers. For theses steadily evolved graphene nanoscrolls, the interlayer distance is subject to the average radius of adsorbed molecular coils and the bending rigidity of graphene hexagonal structural units restricts the reachable curvature of central voids. When the unfavorable solvation is progressively lessened upon slow crystallization of adsorbed polyhexylthiophene molecules, the reverse unwrapping ensues accordingly. On the other hand, the solvent evaporation initiates the dense growth of crystalline whiskers outward from graphene nanoscrolls and thus results in comb-like superstructures. With mutual impingement effects associated with present superstructures, oriented assembly and growth behaviors of crystalline whiskers are able to occur, creating nematic fields of crystalline whiskers.
[Display omitted]
•The step-by-step advancement of steady graphene self-scrolling in solutions.•The adjustable solvation status of adsorbed molecules identified as the driving force of graphene self-scrolling.•Two identified thermodynamic regulating factors of graphene self-scrolling.•The dense outward growth of P3HTcrystalline whiskers on graphene nanoscrolls and evolved comb-like superstructures.•The self-organization of P3HT crystalline whiskers into nematic fields around comb-like superstructures. Upon the tuning of solvent composition, the unfavorable solvation of adsorbed polyhexylthiophene is found able to drive graphene sheets to scroll steadily in solutions, resulting in nanoscrolls with a central void and regular stacking of internal layers. For theses steadily evolved graphene nanoscrolls, the interlayer distance is subject to the average radius of adsorbed molecular coils and the bending rigidity of graphene hexagonal structural units restricts the reachable curvature of central voids. When the unfavorable solvation is progressively lessened upon slow crystallization of adsorbed polyhexylthiophene molecules, the reverse unwrapping ensues accordingly. On the other hand, the solvent evaporation initiates the dense growth of crystalline whiskers outward from graphene nanoscrolls and thus results in comb-like superstructures. With mutual impingement effects associated with present superstructures, oriented assembly and growth behaviors of crystalline whiskers are able to occur, creating nematic fields of crystalline whiskers. |
| ArticleNumber | 123758 |
| Author | Ruan, Jrjeng Cheng, Horng-Long Wu, Ching-Feng Huang, Zheng-Kai Lin, Kun-Ta Lan, Yi-Kang Chou, Wei-Yang Pan, Chia-Hung |
| Author_xml | – sequence: 1 givenname: Zheng-Kai surname: Huang fullname: Huang, Zheng-Kai organization: Department of Materials Science and Engineering, National Cheng Kung University, Tainan, 70101, Taiwan – sequence: 2 givenname: Yi-Kang surname: Lan fullname: Lan, Yi-Kang organization: Materials and Electro-Optic Research Division, National Chung-Shan Institute of Science and Technology, Taoyuan, 32546, Taiwan – sequence: 3 givenname: Kun-Ta surname: Lin fullname: Lin, Kun-Ta organization: Department of Materials Science and Engineering, National Cheng Kung University, Tainan, 70101, Taiwan – sequence: 4 givenname: Chia-Hung surname: Pan fullname: Pan, Chia-Hung organization: Department of Materials Science and Engineering, National Cheng Kung University, Tainan, 70101, Taiwan – sequence: 5 givenname: Ching-Feng surname: Wu fullname: Wu, Ching-Feng organization: Department of Materials Science and Engineering, National Cheng Kung University, Tainan, 70101, Taiwan – sequence: 6 givenname: Horng-Long orcidid: 0000-0002-1631-2231 surname: Cheng fullname: Cheng, Horng-Long organization: Department of Photonics, National Cheng Kung University, Tainan, 70101, Taiwan – sequence: 7 givenname: Wei-Yang surname: Chou fullname: Chou, Wei-Yang organization: Department of Photonics, National Cheng Kung University, Tainan, 70101, Taiwan – sequence: 8 givenname: Jrjeng orcidid: 0000-0001-6857-6055 surname: Ruan fullname: Ruan, Jrjeng email: jrjeng@mail.ncku.edu.tw organization: Department of Materials Science and Engineering, National Cheng Kung University, Tainan, 70101, Taiwan |
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| Snippet | Upon the tuning of solvent composition, the unfavorable solvation of adsorbed polyhexylthiophene is found able to drive graphene sheets to scroll steadily in... |
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| SubjectTerms | 2D materials Coils Crystal structure Crystallinity Crystallization Evaporation Graphene Graphene nanoscroll Interlayers Nematic crystals Polyalkylthiophene Rigidity Scrolling Sheets Solvation Solvents Superstructures |
| Title | Steady self-scrolling of graphene sheets upon the solvation status of adsorbed polyhexylthiophene |
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