Water-stable Cd()/Zn() coordination polymers as recyclable luminescent sensors for detecting hippuric acid in simulated urine for indexing toluene exposure with high selectivity, sensitivity and fast response

Three novel Cd( ii )/Zn( ii ) coordination polymers (CPs), namely [Cd(L)(BPDC) 0.5 H 2 O]·0.5H 2 O ( 1 ), [Zn 2 (L) 2 (BPDC)]·2H 2 O ( 2 ) and [Cd 2 (L)(BTC)H 2 O]·3H 2 O ( 3 ) (L = 4-(tetrazol-5-yl)phenyl-4,2′:6′,4′′-terpyridine, H 2 BPDC = 4,4′-biphenyldicarboxylic acid, and H 3 BTC = 1,3,5-benzen...

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Published inDalton transactions : an international journal of inorganic chemistry Vol. 5; no. 2; pp. 553 - 561
Main Authors Zhao, Jiao-Jiao, Zhang, Lei, Liu, Peng-Yu, Chen, Wei-Zhe, Liu, Zhi-Liang, Wang, Yan-Qin
Format Journal Article
LanguageEnglish
Published England Royal Society of Chemistry 14.01.2021
Subjects
Acids
Cadmium
Cadmium - chemistry
Cadmium - urine
Coordination Complexes - chemical synthesis
Coordination Complexes - chemistry
Coordination polymers
Crystallography
Energy transfer
Fluorescence
Hippurates - chemistry
Hippurates - urine
Hippuric acid
Humans
Hydrogen bonds
Limit of Detection
Metabolites
Nitrogen atoms
Polymers - chemistry
Selectivity
Sensitivity
Sensors
Tetrazoles
Toluene
Toluene - chemistry
Urine
Water - chemistry
Zinc - chemistry
Zinc - urine
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Abstract Three novel Cd( ii )/Zn( ii ) coordination polymers (CPs), namely [Cd(L)(BPDC) 0.5 H 2 O]·0.5H 2 O ( 1 ), [Zn 2 (L) 2 (BPDC)]·2H 2 O ( 2 ) and [Cd 2 (L)(BTC)H 2 O]·3H 2 O ( 3 ) (L = 4-(tetrazol-5-yl)phenyl-4,2′:6′,4′′-terpyridine, H 2 BPDC = 4,4′-biphenyldicarboxylic acid, and H 3 BTC = 1,3,5-benzenetricarboxylic acid), have been successfully synthesized and characterized. CP 1 and CP 2 display new two-dimensional double-layered honeycomb frameworks containing uncoordinated nitrogen atoms from pyridine and tetrazole rings, which can easily form hydrogen bonds with various analytes. CP 3 exhibits a 3D framework also with uncoordinated nitrogen atoms from pyridine and tetrazole rings. The fluorescence explorations indicate that CPs 1-3 exhibit strong blue luminescence and excellent chemical stability under a relatively wide range of pH conditions. It is worth noting that CPs 1-3 can quantitatively detect hippuric acid (HA), which is a metabolite of toluene in human urine, with high selectivity, sensitivity, fast response and relatively low detection limits. Moreover, the sensing mechanism of CPs 1-3 for HA can mainly be ascribed to fluorescence resonance energy transfer (FRET). CPs 1-3 could be ideal candidates as HA sensors in human urine samples for practical applications. Notably, to the best of our knowledge, we report for the first time Cd( ii )/Zn( ii )-based luminescent sensors for detecting HA in simulated urine. Water stable Cd( ii )/Zn( ii ) coordination polymers exhibit rapid, sensitive, selective and recyclable detection towards hippuric acid in simulated urine for indexing toluene exposure.
AbstractList Three novel Cd(ii)/Zn(ii) coordination polymers (CPs), namely [Cd(L)(BPDC)0.5H2O]·0.5H2O (1), [Zn2(L)2(BPDC)]·2H2O (2) and [Cd2(L)(BTC)H2O]·3H2O (3) (L = 4-(tetrazol-5-yl)phenyl-4,2':6',4''-terpyridine, H2BPDC = 4,4'-biphenyldicarboxylic acid, and H3BTC = 1,3,5-benzenetricarboxylic acid), have been successfully synthesized and characterized. CP 1 and CP 2 display new two-dimensional double-layered honeycomb frameworks containing uncoordinated nitrogen atoms from pyridine and tetrazole rings, which can easily form hydrogen bonds with various analytes. CP 3 exhibits a 3D framework also with uncoordinated nitrogen atoms from pyridine and tetrazole rings. The fluorescence explorations indicate that CPs 1-3 exhibit strong blue luminescence and excellent chemical stability under a relatively wide range of pH conditions. It is worth noting that CPs 1-3 can quantitatively detect hippuric acid (HA), which is a metabolite of toluene in human urine, with high selectivity, sensitivity, fast response and relatively low detection limits. Moreover, the sensing mechanism of CPs 1-3 for HA can mainly be ascribed to fluorescence resonance energy transfer (FRET). CPs 1-3 could be ideal candidates as HA sensors in human urine samples for practical applications. Notably, to the best of our knowledge, we report for the first time Cd(ii)/Zn(ii)-based luminescent sensors for detecting HA in simulated urine.Three novel Cd(ii)/Zn(ii) coordination polymers (CPs), namely [Cd(L)(BPDC)0.5H2O]·0.5H2O (1), [Zn2(L)2(BPDC)]·2H2O (2) and [Cd2(L)(BTC)H2O]·3H2O (3) (L = 4-(tetrazol-5-yl)phenyl-4,2':6',4''-terpyridine, H2BPDC = 4,4'-biphenyldicarboxylic acid, and H3BTC = 1,3,5-benzenetricarboxylic acid), have been successfully synthesized and characterized. CP 1 and CP 2 display new two-dimensional double-layered honeycomb frameworks containing uncoordinated nitrogen atoms from pyridine and tetrazole rings, which can easily form hydrogen bonds with various analytes. CP 3 exhibits a 3D framework also with uncoordinated nitrogen atoms from pyridine and tetrazole rings. The fluorescence explorations indicate that CPs 1-3 exhibit strong blue luminescence and excellent chemical stability under a relatively wide range of pH conditions. It is worth noting that CPs 1-3 can quantitatively detect hippuric acid (HA), which is a metabolite of toluene in human urine, with high selectivity, sensitivity, fast response and relatively low detection limits. Moreover, the sensing mechanism of CPs 1-3 for HA can mainly be ascribed to fluorescence resonance energy transfer (FRET). CPs 1-3 could be ideal candidates as HA sensors in human urine samples for practical applications. Notably, to the best of our knowledge, we report for the first time Cd(ii)/Zn(ii)-based luminescent sensors for detecting HA in simulated urine.
Three novel Cd( ii )/Zn( ii ) coordination polymers (CPs), namely [Cd(L)(BPDC) 0.5 H 2 O]·0.5H 2 O ( 1 ), [Zn 2 (L) 2 (BPDC)]·2H 2 O ( 2 ) and [Cd 2 (L)(BTC)H 2 O]·3H 2 O ( 3 ) (L = 4-(tetrazol-5-yl)phenyl-4,2′:6′,4′′-terpyridine, H 2 BPDC = 4,4′-biphenyldicarboxylic acid, and H 3 BTC = 1,3,5-benzenetricarboxylic acid), have been successfully synthesized and characterized. CP 1 and CP 2 display new two-dimensional double-layered honeycomb frameworks containing uncoordinated nitrogen atoms from pyridine and tetrazole rings, which can easily form hydrogen bonds with various analytes. CP 3 exhibits a 3D framework also with uncoordinated nitrogen atoms from pyridine and tetrazole rings. The fluorescence explorations indicate that CPs 1–3 exhibit strong blue luminescence and excellent chemical stability under a relatively wide range of pH conditions. It is worth noting that CPs 1–3 can quantitatively detect hippuric acid (HA), which is a metabolite of toluene in human urine, with high selectivity, sensitivity, fast response and relatively low detection limits. Moreover, the sensing mechanism of CPs 1–3 for HA can mainly be ascribed to fluorescence resonance energy transfer (FRET). CPs 1–3 could be ideal candidates as HA sensors in human urine samples for practical applications. Notably, to the best of our knowledge, we report for the first time Cd( ii )/Zn( ii )-based luminescent sensors for detecting HA in simulated urine.
Three novel Cd( ii )/Zn( ii ) coordination polymers (CPs), namely [Cd(L)(BPDC) 0.5 H 2 O]·0.5H 2 O ( 1 ), [Zn 2 (L) 2 (BPDC)]·2H 2 O ( 2 ) and [Cd 2 (L)(BTC)H 2 O]·3H 2 O ( 3 ) (L = 4-(tetrazol-5-yl)phenyl-4,2′:6′,4′′-terpyridine, H 2 BPDC = 4,4′-biphenyldicarboxylic acid, and H 3 BTC = 1,3,5-benzenetricarboxylic acid), have been successfully synthesized and characterized. CP 1 and CP 2 display new two-dimensional double-layered honeycomb frameworks containing uncoordinated nitrogen atoms from pyridine and tetrazole rings, which can easily form hydrogen bonds with various analytes. CP 3 exhibits a 3D framework also with uncoordinated nitrogen atoms from pyridine and tetrazole rings. The fluorescence explorations indicate that CPs 1-3 exhibit strong blue luminescence and excellent chemical stability under a relatively wide range of pH conditions. It is worth noting that CPs 1-3 can quantitatively detect hippuric acid (HA), which is a metabolite of toluene in human urine, with high selectivity, sensitivity, fast response and relatively low detection limits. Moreover, the sensing mechanism of CPs 1-3 for HA can mainly be ascribed to fluorescence resonance energy transfer (FRET). CPs 1-3 could be ideal candidates as HA sensors in human urine samples for practical applications. Notably, to the best of our knowledge, we report for the first time Cd( ii )/Zn( ii )-based luminescent sensors for detecting HA in simulated urine. Water stable Cd( ii )/Zn( ii ) coordination polymers exhibit rapid, sensitive, selective and recyclable detection towards hippuric acid in simulated urine for indexing toluene exposure.
Three novel Cd(ii)/Zn(ii) coordination polymers (CPs), namely [Cd(L)(BPDC) H O]·0.5H O (1), [Zn (L) (BPDC)]·2H O (2) and [Cd (L)(BTC)H O]·3H O (3) (L = 4-(tetrazol-5-yl)phenyl-4,2':6',4''-terpyridine, H BPDC = 4,4'-biphenyldicarboxylic acid, and H BTC = 1,3,5-benzenetricarboxylic acid), have been successfully synthesized and characterized. CP 1 and CP 2 display new two-dimensional double-layered honeycomb frameworks containing uncoordinated nitrogen atoms from pyridine and tetrazole rings, which can easily form hydrogen bonds with various analytes. CP 3 exhibits a 3D framework also with uncoordinated nitrogen atoms from pyridine and tetrazole rings. The fluorescence explorations indicate that CPs 1-3 exhibit strong blue luminescence and excellent chemical stability under a relatively wide range of pH conditions. It is worth noting that CPs 1-3 can quantitatively detect hippuric acid (HA), which is a metabolite of toluene in human urine, with high selectivity, sensitivity, fast response and relatively low detection limits. Moreover, the sensing mechanism of CPs 1-3 for HA can mainly be ascribed to fluorescence resonance energy transfer (FRET). CPs 1-3 could be ideal candidates as HA sensors in human urine samples for practical applications. Notably, to the best of our knowledge, we report for the first time Cd(ii)/Zn(ii)-based luminescent sensors for detecting HA in simulated urine.
Three novel Cd(ii)/Zn(ii) coordination polymers (CPs), namely [Cd(L)(BPDC)0.5H2O]·0.5H2O (1), [Zn2(L)2(BPDC)]·2H2O (2) and [Cd2(L)(BTC)H2O]·3H2O (3) (L = 4-(tetrazol-5-yl)phenyl-4,2′:6′,4′′-terpyridine, H2BPDC = 4,4′-biphenyldicarboxylic acid, and H3BTC = 1,3,5-benzenetricarboxylic acid), have been successfully synthesized and characterized. CP 1 and CP 2 display new two-dimensional double-layered honeycomb frameworks containing uncoordinated nitrogen atoms from pyridine and tetrazole rings, which can easily form hydrogen bonds with various analytes. CP 3 exhibits a 3D framework also with uncoordinated nitrogen atoms from pyridine and tetrazole rings. The fluorescence explorations indicate that CPs 1–3 exhibit strong blue luminescence and excellent chemical stability under a relatively wide range of pH conditions. It is worth noting that CPs 1–3 can quantitatively detect hippuric acid (HA), which is a metabolite of toluene in human urine, with high selectivity, sensitivity, fast response and relatively low detection limits. Moreover, the sensing mechanism of CPs 1–3 for HA can mainly be ascribed to fluorescence resonance energy transfer (FRET). CPs 1–3 could be ideal candidates as HA sensors in human urine samples for practical applications. Notably, to the best of our knowledge, we report for the first time Cd(ii)/Zn(ii)-based luminescent sensors for detecting HA in simulated urine.
Author Zhao, Jiao-Jiao
Liu, Peng-Yu
Liu, Zhi-Liang
Zhang, Lei
Wang, Yan-Qin
Chen, Wei-Zhe
AuthorAffiliation Inner Mongolia Key Laboratory of Chemistry and Physics of Rare Earth Materials
Inner Mongolia University
College of Chemistry and Chemical Engineering
AuthorAffiliation_xml – name: College of Chemistry and Chemical Engineering
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– name: Inner Mongolia University
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  givenname: Jiao-Jiao
  surname: Zhao
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BackLink https://www.ncbi.nlm.nih.gov/pubmed/33350995$$D View this record in MEDLINE/PubMed
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Snippet Three novel Cd( ii )/Zn( ii ) coordination polymers (CPs), namely [Cd(L)(BPDC) 0.5 H 2 O]·0.5H 2 O ( 1 ), [Zn 2 (L) 2 (BPDC)]·2H 2 O ( 2 ) and [Cd 2 (L)(BTC)H...
Three novel Cd(ii)/Zn(ii) coordination polymers (CPs), namely [Cd(L)(BPDC) H O]·0.5H O (1), [Zn (L) (BPDC)]·2H O (2) and [Cd (L)(BTC)H O]·3H O (3) (L =...
Three novel Cd(ii)/Zn(ii) coordination polymers (CPs), namely [Cd(L)(BPDC)0.5H2O]·0.5H2O (1), [Zn2(L)2(BPDC)]·2H2O (2) and [Cd2(L)(BTC)H2O]·3H2O (3) (L =...
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SubjectTerms Acids
Cadmium
Cadmium - chemistry
Cadmium - urine
Coordination Complexes - chemical synthesis
Coordination Complexes - chemistry
Coordination polymers
Crystallography
Energy transfer
Fluorescence
Hippurates - chemistry
Hippurates - urine
Hippuric acid
Humans
Hydrogen bonds
Limit of Detection
Metabolites
Nitrogen atoms
Polymers - chemistry
Selectivity
Sensitivity
Sensors
Tetrazoles
Toluene
Toluene - chemistry
Urine
Water - chemistry
Zinc - chemistry
Zinc - urine
Title Water-stable Cd()/Zn() coordination polymers as recyclable luminescent sensors for detecting hippuric acid in simulated urine for indexing toluene exposure with high selectivity, sensitivity and fast response
URI https://www.ncbi.nlm.nih.gov/pubmed/33350995
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