Effect of comburent ratios on combustion synthesis of Eu-doped β-SiAlON green phosphors
SiAlON phosphors doped with rare earths have attracted much attention on the application of light emitting diode（LEDs） benefitting from their outstanding thermal stability, chemical stability and broad emission band properties. In this work, Eu-doped β-SiAlON green phosphors with composition Si（5.5）...
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| Published in | Journal of rare earths Vol. 35; no. 5; pp. 430 - 435 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.05.2017
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(17)60928-1 |
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| Abstract | SiAlON phosphors doped with rare earths have attracted much attention on the application of light emitting diode（LEDs） benefitting from their outstanding thermal stability, chemical stability and broad emission band properties. In this work, Eu-doped β-SiAlON green phosphors with composition Si（5.5）Al（0.5）O（0.5）N（7.5）：0.035Eu^2＋ were prepared by a highly efficient combustion synthesis（CS） method. The effect of comburent ratios（i.e., Si ＆ Al） were systematically investigated by adjusting the starting compositions of reactants. It was confirmed that the ratios of Si and Al reactants had an intense influence on the phase composition, microstructure and photoluminescence properties of as-synthesized phosphors by directly determining the systematic energy in CS. The as-prepared β-SiAlON：Eu^2＋ phosphors featured with high phase purity, uniform particle size of 3–5 μm, well-crystalline morphology and outstanding luminescent properties of green emission under UV or blue excitation were synthesized with 67.5 wt.% ratio of Si and no Al comburent. |
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| AbstractList | SiAlON phosphors doped with rare earths have attracted much attention on the application of light emitting diode（LEDs） benefitting from their outstanding thermal stability, chemical stability and broad emission band properties. In this work, Eu-doped β-SiAlON green phosphors with composition Si（5.5）Al（0.5）O（0.5）N（7.5）：0.035Eu^2＋ were prepared by a highly efficient combustion synthesis（CS） method. The effect of comburent ratios（i.e., Si ＆ Al） were systematically investigated by adjusting the starting compositions of reactants. It was confirmed that the ratios of Si and Al reactants had an intense influence on the phase composition, microstructure and photoluminescence properties of as-synthesized phosphors by directly determining the systematic energy in CS. The as-prepared β-SiAlON：Eu^2＋ phosphors featured with high phase purity, uniform particle size of 3–5 μm, well-crystalline morphology and outstanding luminescent properties of green emission under UV or blue excitation were synthesized with 67.5 wt.% ratio of Si and no Al comburent. SiAlON phosphors doped with rare earths have attracted much attention on the application of light emitting diode (LEDs) benefitting from their outstanding thermal stability, chemical stability and broad emission band properties. In this work, Eu-doped β-SiAlON green phosphors with composition Si5.5Al0.5O0.5N7.5:0.035Eu2+ were prepared by a highly efficient combustion synthesis (CS) method. The effect of comburent ratios (i.e., Si & Al) were systematically investigated by adjusting the starting compositions of reactants. It was confirmed that the ratios of Si and Al reactants had an intense influence on the phase composition, microstructure and photoluminescence properties of as-synthesized phosphors by directly determining the systematic energy in CS. The as-prepared β-SiAlON:Eu2+ phosphors featured with high phase purity, uniform particle size of 3–5 μm, well-crystalline morphology and outstanding luminescent properties of green emission under UV or blue excitation were synthesized with 67.5 wt.% ratio of Si and no Al comburent. Excitation spectra (542 nm) (a) and emission spectra (300 nm) (b) of samples synthesized with various proportions of comburents as indicated |
| Author | 葛一瑶 田兆波 陈莹 孙思源 张杰 谢志鹏 |
| AuthorAffiliation | State Key Laboratory of New Ceramics and Fine Processing, Department of Materials Science and Engineering, Tsinghua University, Beijing 100084, China |
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| CitedBy_id | crossref_primary_10_1016_j_jre_2017_05_013 crossref_primary_10_30987_2782_5957_2023_3_4_13 crossref_primary_10_1016_j_jre_2018_01_003 crossref_primary_10_1007_s11664_020_07990_6 crossref_primary_10_1016_j_jallcom_2024_176407 crossref_primary_10_1007_s12613_019_1934_2 crossref_primary_10_1007_s10971_022_05860_7 crossref_primary_10_1016_j_ceramint_2018_09_119 crossref_primary_10_1149_2162_8777_ac0a53 crossref_primary_10_1016_j_jallcom_2021_160745 crossref_primary_10_17073_1683_4518_2023_1_26_30 crossref_primary_10_1016_j_jre_2017_06_014 crossref_primary_10_1016_j_jre_2018_04_018 |
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| Keywords | β-SiAlON Eu2+ doped combustion synthesis phosphor comburent Si/Al ratio rare earths |
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| Notes | SiAlON phosphors doped with rare earths have attracted much attention on the application of light emitting diode（LEDs） benefitting from their outstanding thermal stability, chemical stability and broad emission band properties. In this work, Eu-doped β-SiAlON green phosphors with composition Si（5.5）Al（0.5）O（0.5）N（7.5）：0.035Eu^2＋ were prepared by a highly efficient combustion synthesis（CS） method. The effect of comburent ratios（i.e., Si ＆ Al） were systematically investigated by adjusting the starting compositions of reactants. It was confirmed that the ratios of Si and Al reactants had an intense influence on the phase composition, microstructure and photoluminescence properties of as-synthesized phosphors by directly determining the systematic energy in CS. The as-prepared β-SiAlON：Eu^2＋ phosphors featured with high phase purity, uniform particle size of 3–5 μm, well-crystalline morphology and outstanding luminescent properties of green emission under UV or blue excitation were synthesized with 67.5 wt.% ratio of Si and no Al comburent. 11-2788/TF GE Yiyao , TIAN Zhaobo, CHEN Ying, SUN Siyuan, ZHANG Jie , XIE Zhipeng （State Key Laboratory of New Ceramics and Fine Processing Department of Materials Science and Engineering Tsinghua University, geijing 100084, China） combustion systematically crystalline luminescent outstanding excitation determining starting featured adjusting |
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| Snippet | SiAlON phosphors doped with rare earths have attracted much attention on the application of light emitting diode（LEDs） benefitting from their outstanding... SiAlON phosphors doped with rare earths have attracted much attention on the application of light emitting diode (LEDs) benefitting from their outstanding... |
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| SubjectTerms | comburent combustion synthesis Eu2+ doped phosphor rare earths Si/Al ratio β-SiAlON |
| Title | Effect of comburent ratios on combustion synthesis of Eu-doped β-SiAlON green phosphors |
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