Infrared studies of sub-monolayer methylamine and trimethylamine adsorption on Ni(111)
The adsorption of monomethylamine and trimethylamine on Ni(111) has been studied using reflection absorption infra-red spectroscopy (RAIRS). At 110 K, both molecules are found to chemisorb molecularly and to retain their gas-phase symmetries at the surface. Methylamine possesses an adsorption site s...
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Published in | Surface science Vol. 427; pp. 282 - 287 |
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Main Authors | , , |
Format | Journal Article Conference Proceeding |
Language | English |
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Elsevier B.V
01.06.1999
Amsterdam Elsevier Science New York, NY |
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Abstract | The adsorption of monomethylamine and trimethylamine on Ni(111) has been studied using reflection absorption infra-red spectroscopy (RAIRS). At 110
K, both molecules are found to chemisorb molecularly and to retain their gas-phase symmetries at the surface. Methylamine possesses an adsorption site symmetry of
C
s in which the NH
2 unit is held parallel to the surface plane and the methyl group is tilted with respect to the surface normal. Trimethylamine possesses
C
3v symmetry upon adsorption, with the
c
3 axis aligned along the surface normal. The high sensitivity RAIR data allow a peculiar feature of methylamines to be probed: the lone pair on the nitrogen gives rise to inequivalence in the CH bonds of the methyl unit, leading to the creation of one much weaker C–H bond that produces a decoupled vibration at an unusually low stretching frequency. |
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AbstractList | The adsorption of monomethylamine and trimethylamine on Ni(111) has been studied using reflection absorption infra-red spectroscopy (RAIRS). At 110
K, both molecules are found to chemisorb molecularly and to retain their gas-phase symmetries at the surface. Methylamine possesses an adsorption site symmetry of
C
s in which the NH
2 unit is held parallel to the surface plane and the methyl group is tilted with respect to the surface normal. Trimethylamine possesses
C
3v symmetry upon adsorption, with the
c
3 axis aligned along the surface normal. The high sensitivity RAIR data allow a peculiar feature of methylamines to be probed: the lone pair on the nitrogen gives rise to inequivalence in the CH bonds of the methyl unit, leading to the creation of one much weaker C–H bond that produces a decoupled vibration at an unusually low stretching frequency. |
Author | Nunney, T.S. Birtill, J.J. Raval, R. |
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Keywords | Chemisorption Methylamines Nickel Single crystal surfaces Reflection absorption IR spectroscopy Vibrations of adsorbed molecules Gas solid adsorption Amine Organic adsorbate Gas solid interface Metallic adsorbent Transition metal Infrared spectrum Experimental study Vibrational mode |
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Snippet | The adsorption of monomethylamine and trimethylamine on Ni(111) has been studied using reflection absorption infra-red spectroscopy (RAIRS). At 110
K, both... |
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SubjectTerms | Chemisorption Chemistry Condensed matter: structure, mechanical and thermal properties Dynamics; vibrations Exact sciences and technology General and physical chemistry Methylamines Nickel Physics Reflection absorption IR spectroscopy Single crystal surfaces Solid-fluid interfaces Solid-gas interface Surface and interface dynamics and vibrations Surface physical chemistry Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties) Vibrations of adsorbed molecules |
Title | Infrared studies of sub-monolayer methylamine and trimethylamine adsorption on Ni(111) |
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