Synthesis and characterization of copper(II) complexes of 1,5-bis(quinoline-8′-yl)-1,5- dithiapentane. crystal and molecular structure of [Cu(BQDTP)(NO 3)(OH 2)](NO 3)
Four new copper(II) complexes of formula [Cu(BQDTP)Cl 2] · 2H 2O ( I), [Cu(BQDTP)Br 2] · 2H 2O ( II), [Cu(BQDTP)(OH 2) 2] (ClO 4) 2 ( III) and [Cu(BQDTP)(NO 3) (OH 2)](NO 3) ( IV, where BQDTP is 1,5-bis(quinoline-8′-yl)-1.5-dithiapentane, have been synthesized and characterized by elemental analysis...
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| Published in | Polyhedron Vol. 10; no. 13; pp. 1579 - 1585 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Oxford
Elsevier Ltd
1991
New York, NY Elsevier Science |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Four new copper(II) complexes of formula [Cu(BQDTP)Cl
2] · 2H
2O (
I), [Cu(BQDTP)Br
2] · 2H
2O (
II), [Cu(BQDTP)(OH
2)
2] (ClO
4)
2 (
III) and [Cu(BQDTP)(NO
3) (OH
2)](NO
3) (
IV, where BQDTP is 1,5-bis(quinoline-8′-yl)-1.5-dithiapentane, have been synthesized and characterized by elemental analysis, conductivity measurements, IR and ligand-field spectral studies and magnetic susceptibility measurements. The X-ray crystal structure of
IV has been solved at 293 K by single-crystal X-ray analysis. It consists of [Cu(BQDTP)(NO
3)(OH
2)]
+ cations and nitrate ions, which are connected by hydrogen bonds to a water molecule. The coordination geometry about the copper atom is an elongated octahedron. The measured bond distances are: CuS = 2.343(3) and 2.507(3) Å, CuN = 1.986(7) and 1.993(7) Å, CuO
(water) = 2.030(6) Å and CuO
)nitrate) = 2.677(7) Å. The IR and electronic spectroscopic data, conductivity and magnetic susceptibility are in agreement with the observed structure. |
|---|---|
| AbstractList | Four new copper(II) complexes of formula [Cu(BQDTP)Cl
2] · 2H
2O (
I), [Cu(BQDTP)Br
2] · 2H
2O (
II), [Cu(BQDTP)(OH
2)
2] (ClO
4)
2 (
III) and [Cu(BQDTP)(NO
3) (OH
2)](NO
3) (
IV, where BQDTP is 1,5-bis(quinoline-8′-yl)-1.5-dithiapentane, have been synthesized and characterized by elemental analysis, conductivity measurements, IR and ligand-field spectral studies and magnetic susceptibility measurements. The X-ray crystal structure of
IV has been solved at 293 K by single-crystal X-ray analysis. It consists of [Cu(BQDTP)(NO
3)(OH
2)]
+ cations and nitrate ions, which are connected by hydrogen bonds to a water molecule. The coordination geometry about the copper atom is an elongated octahedron. The measured bond distances are: CuS = 2.343(3) and 2.507(3) Å, CuN = 1.986(7) and 1.993(7) Å, CuO
(water) = 2.030(6) Å and CuO
)nitrate) = 2.677(7) Å. The IR and electronic spectroscopic data, conductivity and magnetic susceptibility are in agreement with the observed structure. |
| Author | Bermejo, E. Castiñeiras, A. Lombao, A. Hiller, W. Carballo, R. Strähle, J. |
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| Cites_doi | 10.1021/ja01510a035 10.1039/qr9712500289 10.1246/bcsj.48.707 10.1021/ja01504a001 10.1016/S0277-5387(00)83878-4 10.1063/1.1699158 10.1039/j19710002801 10.1021/ic00131a064 10.1016/0022-1902(78)80420-5 10.1021/ic50192a018 10.1016/S0277-5387(00)81093-1 10.1107/S0365110X63002991 10.1063/1.1723943 10.1016/0371-1951(66)80040-1 10.1246/bcsj.45.956 10.1021/ic00137a021 10.1246/bcsj.44.2127 10.1107/S0108767383000252 10.1021/ic00164a009 10.1515/znb-1990-0908 10.1063/1.1696110 10.1021/ja00270a064 10.1002/zaac.19713840110 10.1021/ic00231a017 10.1016/S0010-8545(00)80009-0 10.1021/ja00905a015 10.1016/S0020-1693(00)90346-3 10.1002/ijch.198100003 10.1039/j19700003095 10.1039/qr9591300353 10.1524/zkri.1990.193.3-4.251 10.1016/S0277-5387(00)84218-7 10.1039/DT9880001337 10.1246/bcsj.44.2130 10.1080/00945718608055930 10.1021/ic00134a024 10.1016/S0020-1693(00)87957-8 10.1016/S0010-8545(00)80135-6 10.1002/recl.19881070311 |
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| Issue | 13 |
| Keywords | Cationic complex Divalent metal Complexes Molecular structure Nitrogen heterocycle Organic ligand Transition metal Complexes Acido complex Experimental study X ray diffraction Aqua complex Copper II Complexes Aromatic compound Infrared spectrum Crystalline structure |
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| Snippet | Four new copper(II) complexes of formula [Cu(BQDTP)Cl
2] · 2H
2O (
I), [Cu(BQDTP)Br
2] · 2H
2O (
II), [Cu(BQDTP)(OH
2)
2] (ClO
4)
2 (
III) and [Cu(BQDTP)(NO
3)... |
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| SubjectTerms | Chemistry Condensed matter: structure, mechanical and thermal properties Coordination compounds Exact sciences and technology Inorganic chemistry and origins of life Inorganic compounds Metal complexes Physics Preparations and properties Structure of solids and liquids; crystallography Structure of specific crystalline solids |
| Title | Synthesis and characterization of copper(II) complexes of 1,5-bis(quinoline-8′-yl)-1,5- dithiapentane. crystal and molecular structure of [Cu(BQDTP)(NO 3)(OH 2)](NO 3) |
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