Electronic, crystal structure and morphological properties of the Sr2DyRuO6 double perovskite
Electronic, crystal structure and the surface morphology of the Sr2DyRuO6 double perovskite, has been investigated. Measurements of X-ray diffraction and Rietveld analysis show that this compound crystallizes in a perovskite monoclinic structure which belongs to the P21/n (#14) space group and 1:1 o...
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Published in | Materials letters Vol. 82; pp. 116 - 119 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.09.2012
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Abstract | Electronic, crystal structure and the surface morphology of the Sr2DyRuO6 double perovskite, has been investigated. Measurements of X-ray diffraction and Rietveld analysis show that this compound crystallizes in a perovskite monoclinic structure which belongs to the P21/n (#14) space group and 1:1 ordered arrangement of the Ru5+ and Dy3+-cations over the six-coordinate M′ sites, with lattice parameters a=5.7774(2)Å, b=5.7948(2)Å, c=8.1848(2)Å, angle β=90.181(3)° and V=276.88(1)Å3. A morphological characterization of material was performed by Scanning Electron Microscopy (SEM). Results show the granular feature of compound with particle size D=37.2nm. Semi-quantitative compositional studies were carried out from Energy Dispersive X-ray experiments (EDX), and calculations of electronic structure were performed by Density Functional Theory (DFT). Density of states (DOS) study was carried out considering the two spin polarizations, and spin-polarized DOS was obtained from the experimental lattice constants. Results show that the Ru5+ and Dy3+ are responsible of magnetic character of the Sr2DyRuO6.
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► Study of Electronic, crystal structure and morphology of Sr2DyRuO6 double perovskite. ► X-ray diffraction pattern of Sr2DyRuO6 corresponds to monoclinic P21/n space group. ► Scanning Electron Microscopy and the Scherrer equation show particle size D=37.2nm. ► The Ru5+ and Dy3+ ions are responsible for magnetic character of Sr2DyRuO6 perovskite. ► The Sr2DyRuO6 is conductor for spin-up and semiconductor for spin-down polarizations. |
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AbstractList | Electronic, crystal structure and the surface morphology of the Sr2DyRuO6 double perovskite, has been investigated. Measurements of X-ray diffraction and Rietveld analysis show that this compound crystallizes in a perovskite monoclinic structure which belongs to the P21/n (#14) space group and 1:1 ordered arrangement of the Ru5+ and Dy3+-cations over the six-coordinate M′ sites, with lattice parameters a=5.7774(2)Å, b=5.7948(2)Å, c=8.1848(2)Å, angle β=90.181(3)° and V=276.88(1)Å3. A morphological characterization of material was performed by Scanning Electron Microscopy (SEM). Results show the granular feature of compound with particle size D=37.2nm. Semi-quantitative compositional studies were carried out from Energy Dispersive X-ray experiments (EDX), and calculations of electronic structure were performed by Density Functional Theory (DFT). Density of states (DOS) study was carried out considering the two spin polarizations, and spin-polarized DOS was obtained from the experimental lattice constants. Results show that the Ru5+ and Dy3+ are responsible of magnetic character of the Sr2DyRuO6.
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► Study of Electronic, crystal structure and morphology of Sr2DyRuO6 double perovskite. ► X-ray diffraction pattern of Sr2DyRuO6 corresponds to monoclinic P21/n space group. ► Scanning Electron Microscopy and the Scherrer equation show particle size D=37.2nm. ► The Ru5+ and Dy3+ ions are responsible for magnetic character of Sr2DyRuO6 perovskite. ► The Sr2DyRuO6 is conductor for spin-up and semiconductor for spin-down polarizations. Electronic, crystal structure and the surface morphology of the Sr2DyRuO6 double perovskite, has been investigated. Measurements of X-ray diffraction and Rietveld analysis show that this compound crystallizes in a perovskite monoclinic structure which belongs to the P21/n(#14) space group and 1:1 ordered arrangement of the Ru5+ and Dy3+-cations over the six-coordinate M' sites, with lattice parameters a=5.7774(2)Aa, b=5.7948(2)Aa, c=8.1848(2)Aa, angle beta =90.181(3) degree and V=276.88(1)Aa3. A morphological characterization of material was performed by Scanning Electron Microscopy (SEM). Results show the granular feature of compound with particle size D=37.2nm. Semi-quantitative compositional studies were carried out from Energy Dispersive X-ray experiments (EDX), and calculations of electronic structure were performed by Density Functional Theory (DFT). Density of states (DOS) study was carried out considering the two spin polarizations, and spin-polarized DOS was obtained from the experimental lattice constants. Results show that the Ru5+ and Dy3+ are responsible of magnetic character of the Sr2DyRuO6. |
Author | Triana, C.A. Téllez, D.A. Landínez Rodríguez, J. Arbey Fajardo, F. Roa-Rojas, J. |
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SubjectTerms | Crystal structure Density functional theory Density of states Double perovskite Electron microscopy Electronics Lattice parameters Oxides Perovskites Scanning electron microscopy X-ray techniques X-rays |
Title | Electronic, crystal structure and morphological properties of the Sr2DyRuO6 double perovskite |
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