A novel Z-scheme heterojunction photocatalyst CeO2@WO3 nanocomposite with enhanced visible-light photocatalytic performance for wastewater treatment by cephalexin antibiotic degradation: Process optimization

[Display omitted] Considering growing global environmental concerns, there is a heightened focus on expediting the synthesis of highly efficient catalytic materials to address these challenges effectively. Herein, a novel CeO2@WO3 heterojunction photocatalyst was synthesized using an ultrasonic-assi...

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Published inJournal of industrial and engineering chemistry (Seoul, Korea) Vol. 135; pp. 213 - 231
Main Authors Wang, Shuaibing, Liu, Junhong, Albaijan, Ibrahim, Shawabkeh, Ali, Lin, Haitao, Ahmad, Irfan, Rab, Safia Obaidur, Alshahrani, Mohammad Y.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 25.07.2024
한국공업화학회
Subjects
Non-biodegradable Cephalexin
Photocatalysis
Process optimization
Wastewater treatment
화학공학
Process optimization
Wastewater treatment
Non-biodegradable Cephalexin
Photocatalysis
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Abstract [Display omitted] Considering growing global environmental concerns, there is a heightened focus on expediting the synthesis of highly efficient catalytic materials to address these challenges effectively. Herein, a novel CeO2@WO3 heterojunction photocatalyst was synthesized using an ultrasonic-assisted method for the environmentally friendly degradation of cephalexin (CPX) under visible light. The optimized photocatalyst synthesis condition was achieved by assessing the influence of effective parameters, including the CeO2 content (5–25 wt%) and calcination temperature (300–600 °C), employing the RSM method. The synthesized photocatalysts were comprehensively characterized through XRD, SEM, TEM, EDS-mapping, BET, FTIR, and UV–Vis band gap analysis. Using optimal photocatalyst (CeO2 content: 15.78 %, calcination temperature: 440.59 °C, and ultrasonic power: 80 W), the influence of four critical variables on CPX degradation was thoroughly investigated via RSM-CCD. The maximum CPX degradation efficiency of 98.8 % was attained under the following optimal conditions: CPX concentration: 20.00 mg/L, solution pH: 6.79, photocatalyst dosage: 0.019 g/L, and visible light time: 94.82 min. Statistical analysis confirmed the accuracy of the regression model based on empirical data. The CeO2@WO3 heterojunction demonstrated substantial Chemical Oxygen Demand (COD) removal, reaching 73.26 % during the mineralization of CPX, surpassing the outcomes of previous studies. Trapping experiments and EPR analysis indicated the crucial involvement of hydroxyl radicals and superoxide radicals as highly active species due to their non-selective oxidation capabilities. Furthermore, a Z-scheme charge transfer mechanism was proposed to elucidate the enhanced photocatalytic activity. Identifying degradation intermediates was accomplished through HPLC-MS analysis, leading to a plausible pathway for CPX degradation. Overall, CeO2@WO3 exhibited excellent stability and could endure five cycles with minimal cerium leaching, highlighting its effectiveness in decomposing organic contaminants.
AbstractList Considering growing global environmental concerns, there is a heightened focus on expediting the synthesis ofhighly efficient catalytic materials to address these challenges effectively. Herein, a novel CeO2@WO3 heterojunctionphotocatalyst was synthesized using an ultrasonic-assisted method for the environmentally friendlydegradation of cephalexin (CPX) under visible light. The optimized photocatalyst synthesis condition was achievedby assessing the influence of effective parameters, including the CeO2 content (5–25 wt%) and calcinationtemperature (300–600 ◦C), employing the RSM method. The synthesized photocatalysts were comprehensivelycharacterized through XRD, SEM, TEM, EDS-mapping, BET, FTIR, and UV–Vis band gap analysis. Using optimalphotocatalyst (CeO2 content: 15.78 %, calcination temperature: 440.59 ◦C, and ultrasonic power: 80 W), theinfluence of four critical variables on CPX degradation was thoroughly investigated via RSM-CCD. The maximumCPX degradation efficiency of 98.8 % was attained under the following optimal conditions: CPX concentration:20.00 mg/L, solution pH: 6.79, photocatalyst dosage: 0.019 g/L, and visible light time: 94.82 min. Statisticalanalysis confirmed the accuracy of the regression model based on empirical data. The CeO2@WO3 heterojunctiondemonstrated substantial Chemical Oxygen Demand (COD) removal, reaching 73.26 % during the mineralizationof CPX, surpassing the outcomes of previous studies. Trapping experiments and EPR analysis indicated the crucialinvolvement of hydroxyl radicals and superoxide radicals as highly active species due to their non-selectiveoxidation capabilities. Furthermore, a Z-scheme charge transfer mechanism was proposed to elucidate theenhanced photocatalytic activity. Identifying degradation intermediates was accomplished through HPLC-MSanalysis, leading to a plausible pathway for CPX degradation. Overall, CeO2@WO3 exhibited excellent stabilityand could endure five cycles with minimal cerium leaching, highlighting its effectiveness in decomposingorganic contaminants. KCI Citation Count: 0
[Display omitted] Considering growing global environmental concerns, there is a heightened focus on expediting the synthesis of highly efficient catalytic materials to address these challenges effectively. Herein, a novel CeO2@WO3 heterojunction photocatalyst was synthesized using an ultrasonic-assisted method for the environmentally friendly degradation of cephalexin (CPX) under visible light. The optimized photocatalyst synthesis condition was achieved by assessing the influence of effective parameters, including the CeO2 content (5–25 wt%) and calcination temperature (300–600 °C), employing the RSM method. The synthesized photocatalysts were comprehensively characterized through XRD, SEM, TEM, EDS-mapping, BET, FTIR, and UV–Vis band gap analysis. Using optimal photocatalyst (CeO2 content: 15.78 %, calcination temperature: 440.59 °C, and ultrasonic power: 80 W), the influence of four critical variables on CPX degradation was thoroughly investigated via RSM-CCD. The maximum CPX degradation efficiency of 98.8 % was attained under the following optimal conditions: CPX concentration: 20.00 mg/L, solution pH: 6.79, photocatalyst dosage: 0.019 g/L, and visible light time: 94.82 min. Statistical analysis confirmed the accuracy of the regression model based on empirical data. The CeO2@WO3 heterojunction demonstrated substantial Chemical Oxygen Demand (COD) removal, reaching 73.26 % during the mineralization of CPX, surpassing the outcomes of previous studies. Trapping experiments and EPR analysis indicated the crucial involvement of hydroxyl radicals and superoxide radicals as highly active species due to their non-selective oxidation capabilities. Furthermore, a Z-scheme charge transfer mechanism was proposed to elucidate the enhanced photocatalytic activity. Identifying degradation intermediates was accomplished through HPLC-MS analysis, leading to a plausible pathway for CPX degradation. Overall, CeO2@WO3 exhibited excellent stability and could endure five cycles with minimal cerium leaching, highlighting its effectiveness in decomposing organic contaminants.
Author Liu, Junhong
Rab, Safia Obaidur
Shawabkeh, Ali
Alshahrani, Mohammad Y.
Lin, Haitao
Albaijan, Ibrahim
Wang, Shuaibing
Ahmad, Irfan
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  givenname: Junhong
  surname: Liu
  fullname: Liu, Junhong
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  givenname: Ibrahim
  surname: Albaijan
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  organization: Mechanical Engineering Department, College of Engineering at Al-Kharj, Prince Sattam Bin Abdulaziz University, Al Kharj 16273, Saudi Arabia
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  givenname: Ali
  surname: Shawabkeh
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  email: Ali.Shawabkeh@aum.edu.kw
  organization: College of Engineering and Technology, American University of the Middle East, Kuwait
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  organization: Yuxi Normal University, 653100 Yuxi, Yunnan, China
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  givenname: Irfan
  surname: Ahmad
  fullname: Ahmad, Irfan
  organization: Department of Clinical Laboratory Sciences, College of Applied Medical Sciences, King Khalid University, Abha, Saudi Arabia
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  givenname: Safia Obaidur
  surname: Rab
  fullname: Rab, Safia Obaidur
  organization: Department of Clinical Laboratory Sciences, College of Applied Medical Sciences, King Khalid University, Abha, Saudi Arabia
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  givenname: Mohammad Y.
  surname: Alshahrani
  fullname: Alshahrani, Mohammad Y.
  organization: Department of Clinical Laboratory Sciences, College of Applied Medical Sciences, King Khalid University, Abha, Saudi Arabia
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Keywords Process optimization
Wastewater treatment
Non-biodegradable Cephalexin
Photocatalysis
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한국공업화학회
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Snippet [Display omitted] Considering growing global environmental concerns, there is a heightened focus on expediting the synthesis of highly efficient catalytic...
Considering growing global environmental concerns, there is a heightened focus on expediting the synthesis ofhighly efficient catalytic materials to address...
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SubjectTerms Non-biodegradable Cephalexin
Photocatalysis
Process optimization
Wastewater treatment
화학공학
Title A novel Z-scheme heterojunction photocatalyst CeO2@WO3 nanocomposite with enhanced visible-light photocatalytic performance for wastewater treatment by cephalexin antibiotic degradation: Process optimization
URI https://dx.doi.org/10.1016/j.jiec.2024.01.033
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