Metal organic framework-derived CoMn2O4 catalyst for heterogeneous activation of peroxymonosulfate and sulfanilamide degradation
[Display omitted] •Plate-shaped CoMn2O4 was synthesized using MOFs as precursor.•The catalyst showed large specific surface area and abundant active sites.•It had much higher catalytic activity than previously-reported CoMn2O4 catalyst.•The Co-Mn synergy in heterogeneous catalysis were elucidated.•T...
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| Published in | Chemical engineering journal (Lausanne, Switzerland : 1996) Vol. 337; pp. 101 - 109 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.04.2018
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Plate-shaped CoMn2O4 was synthesized using MOFs as precursor.•The catalyst showed large specific surface area and abundant active sites.•It had much higher catalytic activity than previously-reported CoMn2O4 catalyst.•The Co-Mn synergy in heterogeneous catalysis were elucidated.•The material showed good stability and reusability for SA removal.
Spinel-type CoMn2O4 materials are promising catalyst for heterogeneous activation of peroxymonosulfate (PMS), but the catalytic activity still need considerable improvements for practical environmental application and the underlying Co-Mn synergy is unclear. In this work, we synthesized CoMn2O4 microplates by using CoMn2-perylene-3,4,9,10-tetracarboxylic dianhydride (ptcda) metal organic frameworks (MOFs) as the precursor. The resulting material showed significantly higher catalytic activity for the PMS activation and sulfanilamide (SA) degradation than the CoMn2O4 obtained by conventional solvothermal synthesis methods, due to its much higher specific surface area and abundant surface hydroxyl groups as the active sites. In addition, the Co-Mn synergy in the synthesized material for the efficient heterogeneous catalysis was elucidated. The catalyst stability was also evaluated. Our work may lay the foundation for optimized design of highly-efficient heterogeneous catalyst for environmental application. |
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| AbstractList | [Display omitted]
•Plate-shaped CoMn2O4 was synthesized using MOFs as precursor.•The catalyst showed large specific surface area and abundant active sites.•It had much higher catalytic activity than previously-reported CoMn2O4 catalyst.•The Co-Mn synergy in heterogeneous catalysis were elucidated.•The material showed good stability and reusability for SA removal.
Spinel-type CoMn2O4 materials are promising catalyst for heterogeneous activation of peroxymonosulfate (PMS), but the catalytic activity still need considerable improvements for practical environmental application and the underlying Co-Mn synergy is unclear. In this work, we synthesized CoMn2O4 microplates by using CoMn2-perylene-3,4,9,10-tetracarboxylic dianhydride (ptcda) metal organic frameworks (MOFs) as the precursor. The resulting material showed significantly higher catalytic activity for the PMS activation and sulfanilamide (SA) degradation than the CoMn2O4 obtained by conventional solvothermal synthesis methods, due to its much higher specific surface area and abundant surface hydroxyl groups as the active sites. In addition, the Co-Mn synergy in the synthesized material for the efficient heterogeneous catalysis was elucidated. The catalyst stability was also evaluated. Our work may lay the foundation for optimized design of highly-efficient heterogeneous catalyst for environmental application. |
| Author | Chen, Chang-Bin Li, Wen-Wei Liu, Hou-Qi Li, Jie Li, Chen-Xuan Cui, Shuo Lu, Jia-Yuan Zhang, Feng |
| Author_xml | – sequence: 1 givenname: Chen-Xuan surname: Li fullname: Li, Chen-Xuan organization: Department of Chemistry, University of Science & Technology of China, Hefei 230026, China – sequence: 2 givenname: Chang-Bin surname: Chen fullname: Chen, Chang-Bin organization: Department of Chemistry, University of Science & Technology of China, Hefei 230026, China – sequence: 3 givenname: Jia-Yuan surname: Lu fullname: Lu, Jia-Yuan organization: Department of Chemistry, University of Science & Technology of China, Hefei 230026, China – sequence: 4 givenname: Shuo surname: Cui fullname: Cui, Shuo organization: Department of Chemistry, University of Science & Technology of China, Hefei 230026, China – sequence: 5 givenname: Jie surname: Li fullname: Li, Jie organization: Department of Chemistry, University of Science & Technology of China, Hefei 230026, China – sequence: 6 givenname: Hou-Qi surname: Liu fullname: Liu, Hou-Qi organization: Department of Chemistry, University of Science & Technology of China, Hefei 230026, China – sequence: 7 givenname: Wen-Wei orcidid: 0000-0001-9280-0045 surname: Li fullname: Li, Wen-Wei email: wwli@ustc.edu.cn organization: Department of Chemistry, University of Science & Technology of China, Hefei 230026, China – sequence: 8 givenname: Feng surname: Zhang fullname: Zhang, Feng email: zfeng3@ustc.edu.cn organization: Department of Chemistry, University of Science & Technology of China, Hefei 230026, China |
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•Plate-shaped CoMn2O4 was synthesized using MOFs as precursor.•The catalyst showed large specific surface area and abundant active sites.•It... |
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| SubjectTerms | CoMn2O4 Metal–organic frameworks (MOFs) Peroxymonosulfate (PMS) Sulfanilamide Synergy |
| Title | Metal organic framework-derived CoMn2O4 catalyst for heterogeneous activation of peroxymonosulfate and sulfanilamide degradation |
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