Preparation of a porous boron-doped diamond/Ta electrode for the electrocatalytic degradation of organic pollutants
Polycrystalline boron-doped diamond (BDD) was grown on a Ta substrate by electron-assisted hot filament chemical vapor deposition, and porous BDD/Ta multilayer films were constructed by Ni-nanoparticle-assisted plasma etching. The etching process and the formation mechanism of the porous nanostructu...
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Published in | Carbon (New York) Vol. 129; pp. 543 - 551 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
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New York
Elsevier Ltd
01.04.2018
Elsevier BV |
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Abstract | Polycrystalline boron-doped diamond (BDD) was grown on a Ta substrate by electron-assisted hot filament chemical vapor deposition, and porous BDD/Ta multilayer films were constructed by Ni-nanoparticle-assisted plasma etching. The etching process and the formation mechanism of the porous nanostructure on the BDD were investigated by changing the Ni sputtering time and the BDD etching time. Under optimal etching conditions, differently shaped nanoholes appeared on the different crystal planes of the diamond crystallites, including square and triangular (or hexagonal) holes. In addition, changes in the elemental composition, crystal, and chemical-bonding structures were analyzed; the effective electroactive surface area and charge transfer capability at the liquid-solid interface were found to be improved in the etched crystallites. Therefore, we believe that the electrocatalytic performance of a porous BDD/Ta electrode would also be improved, as electrocatalytic performance is strongly affected by the porous nanostructures of BDD films. The porous BDD/Ta electrode acted as the anode for the rapid degradation of methylene blue through the electro-Fenton process.
An etched BDD/Ta film with a nanoporous surface exhibits excellent electrocatalytic behavior. [Display omitted] |
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AbstractList | Polycrystalline boron-doped diamond (BDD) was grown on a Ta substrate by electron-assisted hot filament chemical vapor deposition, and porous BDD/Ta multilayer films were constructed by Ni-nanoparticle-assisted plasma etching. The etching process and the formation mechanism of the porous nanostructure on the BDD were investigated by changing the Ni sputtering time and the BDD etching time. Under optimal etching conditions, differently shaped nanoholes appeared on the different crystal planes of the diamond crystallites, including square and triangular (or hexagonal) holes. In addition, changes in the elemental composition, crystal, and chemical-bonding structures were analyzed; the effective electroactive surface area and charge transfer capability at the liquid-solid interface were found to be improved in the etched crystallites. Therefore, we believe that the electrocatalytic performance of a porous BDD/Ta electrode would also be improved, as electrocatalytic performance is strongly affected by the porous nanostructures of BDD films. The porous BDD/Ta electrode acted as the anode for the rapid degradation of methylene blue through the electro-Fenton process.
An etched BDD/Ta film with a nanoporous surface exhibits excellent electrocatalytic behavior. [Display omitted] Polycrystalline boron-doped diamond (BDD) was grown on a Ta substrate by electron-assisted hot filament chemical vapor deposition, and porous BDD/Ta multilayer films were constructed by Ni-nanoparticle-assisted plasma etching. The etching process and the formation mechanism of the porous nanostructure on the BDD were investigated by changing the Ni sputtering time and the BDD etching time. Under optimal etching conditions, differently shaped nanoholes appeared on the different crystal planes of the diamond crystallites, including square and triangular (or hexagonal) holes. In addition, changes in the elemental composition, crystal, and chemical-bonding structures were analyzed; the effective electroactive surface area and charge transfer capability at the liquid-solid interface were found to be improved in the etched crystallites. Therefore, we believe that the electrocatalytic performance of a porous BDD/Ta electrode would also be improved, as electrocatalytic performance is strongly affected by the porous nanostructures of BDD films. The porous BDD/Ta electrode acted as the anode for the rapid degradation of methylene blue through the electro-Fenton process. |
Author | Li, Hongji Li, Cuiping Yang, Baohe Lei, Yingjie Li, Xiaojie Li, Mingji Sun, Dazhi |
Author_xml | – sequence: 1 givenname: Xiaojie surname: Li fullname: Li, Xiaojie organization: Tianjin Key Laboratory of Film Electronic and Communicate Devices, School of Electrical and Electronic Engineering, Tianjin University of Technology, Tianjin 300384, PR China – sequence: 2 givenname: Hongji surname: Li fullname: Li, Hongji email: hongjili@yeah.net organization: Tianjin Key Laboratory of Organic Solar Cells and Photochemical Conversion, School of Chemistry & Chemical Engineering, Tianjin University of Technology, Tianjin 300384, PR China – sequence: 3 givenname: Mingji surname: Li fullname: Li, Mingji email: limingji@163.com organization: Tianjin Key Laboratory of Film Electronic and Communicate Devices, School of Electrical and Electronic Engineering, Tianjin University of Technology, Tianjin 300384, PR China – sequence: 4 givenname: Cuiping surname: Li fullname: Li, Cuiping organization: Tianjin Key Laboratory of Film Electronic and Communicate Devices, School of Electrical and Electronic Engineering, Tianjin University of Technology, Tianjin 300384, PR China – sequence: 5 givenname: Dazhi surname: Sun fullname: Sun, Dazhi organization: Tianjin Key Laboratory of Film Electronic and Communicate Devices, School of Electrical and Electronic Engineering, Tianjin University of Technology, Tianjin 300384, PR China – sequence: 6 givenname: Yingjie surname: Lei fullname: Lei, Yingjie organization: Tianjin Key Laboratory of Organic Solar Cells and Photochemical Conversion, School of Chemistry & Chemical Engineering, Tianjin University of Technology, Tianjin 300384, PR China – sequence: 7 givenname: Baohe surname: Yang fullname: Yang, Baohe organization: Tianjin Key Laboratory of Film Electronic and Communicate Devices, School of Electrical and Electronic Engineering, Tianjin University of Technology, Tianjin 300384, PR China |
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Snippet | Polycrystalline boron-doped diamond (BDD) was grown on a Ta substrate by electron-assisted hot filament chemical vapor deposition, and porous BDD/Ta multilayer... |
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SubjectTerms | Boron Boron-doped diamond Charge transfer Chemical bonds Chemical vapor deposition Crystal structure Crystallites Degradation Diamonds Electro catalysis Electrocatalysis Electrode Electrodes Etching Liquid-solid interfaces Methylene blue Nanostructure Plasma etching Pollutants Porous structure Substrates |
Title | Preparation of a porous boron-doped diamond/Ta electrode for the electrocatalytic degradation of organic pollutants |
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