Synthesis and surface active properties of novel anionic surfactants with two short fluoroalkyl groups
[Display omitted] Fluorinated surfactants, especially perfluorooctanoic acid (PFOA) and its derivatives, are frequently used in many industries. However, they are harmful to human health and the environment. While surfactants with only short fluorocarbon chains have lower toxicity, their physical pr...
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| Published in | Journal of industrial and engineering chemistry (Seoul, Korea) Vol. 61; pp. 216 - 226 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
25.05.2018
한국공업화학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1226-086X 1876-794X |
| DOI | 10.1016/j.jiec.2017.12.019 |
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| Abstract | [Display omitted]
Fluorinated surfactants, especially perfluorooctanoic acid (PFOA) and its derivatives, are frequently used in many industries. However, they are harmful to human health and the environment. While surfactants with only short fluorocarbon chains have lower toxicity, their physical properties need improvement. In this study, we synthesized novel anionic fluorinated surfactants with two short fluorocarbon chains per molecule, using the condensation reaction of fluoroalcohol and fluoroalkyl glycidyl ether in two-step reactions, which are carried out under mild conditions with easy work-up procedures and high yield (>80%). The products were structurally characterized, and their performance as surfactants were systematically analyzed. The critical micelle concentrations of the final products were found to be low (0.31–1.15mmol/L), and their surface tension in 1% aqueous solution was within the range of 15.7–22.8mN/m. These results suggest that despite their short fluorocarbon chains, these new surfactants are valuable alternatives to PFOA and its derivatives. |
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| AbstractList | [Display omitted]
Fluorinated surfactants, especially perfluorooctanoic acid (PFOA) and its derivatives, are frequently used in many industries. However, they are harmful to human health and the environment. While surfactants with only short fluorocarbon chains have lower toxicity, their physical properties need improvement. In this study, we synthesized novel anionic fluorinated surfactants with two short fluorocarbon chains per molecule, using the condensation reaction of fluoroalcohol and fluoroalkyl glycidyl ether in two-step reactions, which are carried out under mild conditions with easy work-up procedures and high yield (>80%). The products were structurally characterized, and their performance as surfactants were systematically analyzed. The critical micelle concentrations of the final products were found to be low (0.31–1.15mmol/L), and their surface tension in 1% aqueous solution was within the range of 15.7–22.8mN/m. These results suggest that despite their short fluorocarbon chains, these new surfactants are valuable alternatives to PFOA and its derivatives. Fluorinated surfactants, especially perfluorooctanoic acid (PFOA) and its derivatives, are frequently used in many industries. However, they are harmful to human health and the environment. While surfactants with only short fluorocarbon chains have lower toxicity, their physical properties need improvement. In this study, we synthesized novel anionic fluorinated surfactants with two short fluorocarbon chains per molecule, using the condensation reaction of fluoroalcohol and fluoroalkyl glycidyl ether in two-step reactions, which are carried out under mild conditions with easy work-up procedures and high yield (>80%). The products were structurally characterized, and their performance as surfactants were systematically analyzed. The critical micelle concentrations of the final products were found to be low (0.31–1.15 mmol/L), and their surface tension in 1% aqueous solution was within the range of 15.7–22.8 mN/m. These results suggest that despite their short fluorocarbon chains, these new surfactants are valuable alternatives to PFOA and its derivatives. KCI Citation Count: 6 |
| Author | Jung, Seon Hwa Lee, Byung Min Kang, Eun-kyung Jung, Ga Young |
| Author_xml | – sequence: 1 givenname: Eun-kyung surname: Kang fullname: Kang, Eun-kyung organization: Advanced Materials and Chemical Engineering, University of Science and Technology, 217, Gajeong-ro, Yuseong-gu, Daejeon 34113, Republic of Korea – sequence: 2 givenname: Ga Young surname: Jung fullname: Jung, Ga Young organization: Advanced Materials and Chemical Engineering, University of Science and Technology, 217, Gajeong-ro, Yuseong-gu, Daejeon 34113, Republic of Korea – sequence: 3 givenname: Seon Hwa surname: Jung fullname: Jung, Seon Hwa organization: Center for Interface Chemistry and Engineering, Korea Research Institute of Chemical Technology, 141, Gajeong-ro, Yuseong-gu, Daejeon 34114, Republic of Korea – sequence: 4 givenname: Byung Min surname: Lee fullname: Lee, Byung Min email: bmlee@krict.re.kr, surfagent@hanmail.net organization: Advanced Materials and Chemical Engineering, University of Science and Technology, 217, Gajeong-ro, Yuseong-gu, Daejeon 34113, Republic of Korea |
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Fluorinated surfactants, especially perfluorooctanoic acid (PFOA) and its derivatives, are frequently used in many industries. However, they... Fluorinated surfactants, especially perfluorooctanoic acid (PFOA) and its derivatives, are frequently used in many industries. However, they are harmful to... |
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| Title | Synthesis and surface active properties of novel anionic surfactants with two short fluoroalkyl groups |
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