High-temperature CMAS resistance performance of Ti2AlC oxide scales

•Bi-layered oxide scales were developed by pre-oxidizing Ti2AlC bulk at different temperatures.•Molten CMAS corrosion behavior on scales at 1523 K was studied though a sessile-drop method.•CaTiO3 phase could help increase CMAS droplet viscosity and reduce spreading rate.•Glassy CMAS on Al2TiO5 layer...

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Published inCorrosion science Vol. 174; p. 108832
Main Authors Jing, Jing, Li, Jimeng, He, Zhe, He, Jian, Guo, Hongbo
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier Ltd 01.09.2020
Elsevier BV
Subjects
Aluminum titanates
Calcium magnesium silicates
Calcium-magnesium-aluminium-silicate (CMAS)
Contact angle
Diffusion layers
Diffusion rate
High temperature
Oxidation
Oxidation resistance
Scale (corrosion)
Sessile drop method
Thermal barrier coatings
Thermal barrier coatings (TBCs)
Ti2AlC
Wettability
Wetting
Oxidation
Thermal barrier coatings (TBCs)
Wetting
Calcium-magnesium-aluminium-silicate (CMAS)
Ti2AlC
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Abstract •Bi-layered oxide scales were developed by pre-oxidizing Ti2AlC bulk at different temperatures.•Molten CMAS corrosion behavior on scales at 1523 K was studied though a sessile-drop method.•CaTiO3 phase could help increase CMAS droplet viscosity and reduce spreading rate.•Glassy CMAS on Al2TiO5 layer shows the slowest spreading rate and the largest equilibrium contact angle among all. Failure of thermal barrier coatings (TBCs) caused by glassy deposits mostly composed of calcium-magnesium-aluminium-silicate (CMAS) has become an urgent issue. The addition of Al and Ti elements in TBCs is beneficial to improve the CMAS resistance. In this paper, bi-layered oxide scales were formed through pre-oxidation of Ti2AlC (POTAC) bulks at high temperatures. The wettability and spreading behaviors of CMAS on the oxide scales, as well as the interaction between them were investigated by a sessile-drop method. The glassy CMAS deposit on the Al2TiO5 layer revealed the largest equilibrium contact angle and slowest diffusion-limited spreading rate among all the samples.
AbstractList Failure of thermal barrier coatings (TBCs) caused by glassy deposits mostly composed of calcium-magnesium-aluminium-silicate (CMAS) has become an urgent issue. The addition of Al and Ti elements in TBCs is beneficial to improve the CMAS resistance. In this paper, bi-layered oxide scales were formed through pre-oxidation of Ti2AlC (POTAC) bulks at high temperatures. The wettability and spreading behaviors of CMAS on the oxide scales, as well as the interaction between them were investigated by a sessile-drop method. The glassy CMAS deposit on the Al2TiO5 layer revealed the largest equilibrium contact angle and slowest diffusion-limited spreading rate among all the samples.
•Bi-layered oxide scales were developed by pre-oxidizing Ti2AlC bulk at different temperatures.•Molten CMAS corrosion behavior on scales at 1523 K was studied though a sessile-drop method.•CaTiO3 phase could help increase CMAS droplet viscosity and reduce spreading rate.•Glassy CMAS on Al2TiO5 layer shows the slowest spreading rate and the largest equilibrium contact angle among all. Failure of thermal barrier coatings (TBCs) caused by glassy deposits mostly composed of calcium-magnesium-aluminium-silicate (CMAS) has become an urgent issue. The addition of Al and Ti elements in TBCs is beneficial to improve the CMAS resistance. In this paper, bi-layered oxide scales were formed through pre-oxidation of Ti2AlC (POTAC) bulks at high temperatures. The wettability and spreading behaviors of CMAS on the oxide scales, as well as the interaction between them were investigated by a sessile-drop method. The glassy CMAS deposit on the Al2TiO5 layer revealed the largest equilibrium contact angle and slowest diffusion-limited spreading rate among all the samples.
ArticleNumber 108832
Author He, Zhe
Guo, Hongbo
He, Jian
Li, Jimeng
Jing, Jing
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  givenname: Jian
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  givenname: Hongbo
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Keywords Oxidation
Thermal barrier coatings (TBCs)
Wetting
Calcium-magnesium-aluminium-silicate (CMAS)
Ti2AlC
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Snippet •Bi-layered oxide scales were developed by pre-oxidizing Ti2AlC bulk at different temperatures.•Molten CMAS corrosion behavior on scales at 1523 K was studied...
Failure of thermal barrier coatings (TBCs) caused by glassy deposits mostly composed of calcium-magnesium-aluminium-silicate (CMAS) has become an urgent issue....
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SubjectTerms Aluminum titanates
Calcium magnesium silicates
Calcium-magnesium-aluminium-silicate (CMAS)
Contact angle
Diffusion layers
Diffusion rate
High temperature
Oxidation
Oxidation resistance
Scale (corrosion)
Sessile drop method
Thermal barrier coatings
Thermal barrier coatings (TBCs)
Ti2AlC
Wettability
Wetting
Title High-temperature CMAS resistance performance of Ti2AlC oxide scales
URI https://dx.doi.org/10.1016/j.corsci.2020.108832
https://www.proquest.com/docview/2449987015
Volume 174
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