Preparation of PVA/PAA nanofibers containing thiol-modified silica particles by electrospinning as an eco-friendly Cu (II) adsorbent

[Display omitted] •Surface of silica nanoparticles was modified with thiol groups through sol–gel method.•Modified silica particles were incorporated into PVA/PAA nanofibers by eco-friendly electrospinning process.•Adsorption capacity of Cu (II) ions onto PVA/PAA nanofibers dramatically increased by...

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Published inJournal of industrial and engineering chemistry (Seoul, Korea) Vol. 77; pp. 273 - 279
Main Authors Kim, Jinyeong, Kang, Taeho, Kim, Hyewon, Shin, Hong Ju, Oh, Seong-Geun
Format Journal Article
LanguageEnglish
Published Elsevier B.V 25.09.2019
한국공업화학회
Subjects
Copper adsorption
Eco-friendly electrospinning
Nanofiber
Silica nanoparticles
Thiol-modification
화학공학
Eco-friendly electrospinning
Silica nanoparticles
Copper adsorption
Nanofiber
Thiol-modification
Online AccessGet full text
ISSN1226-086X
1876-794X
DOI10.1016/j.jiec.2019.04.048

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Abstract [Display omitted] •Surface of silica nanoparticles was modified with thiol groups through sol–gel method.•Modified silica particles were incorporated into PVA/PAA nanofibers by eco-friendly electrospinning process.•Adsorption capacity of Cu (II) ions onto PVA/PAA nanofibers dramatically increased by incorporation of thiol-modified silica.•Adsorption behavior was rather chemisorption due to strong interaction between Cu (II) ions and thiol groups. Using an electrospinning technique, thiol-modified silica nanoparticles were incorporated into poly(vinyl alcohol) (PVA) and poly(acrylic acid) (PAA) hybrid nanofibers to fabricate an eco-friendly adsorbent with enhanced Cu (II) adsorption capacity. The hybrid nanofibers were successfully crosslinked through heat treatment. Cu (II) adsorption characteristics of nanofibers were investigated including silica quantity, surface modification, and pH. Adsorption isotherms and kinetics fit a Langmuir isotherm model and pseudo-second-order model, respectively, implying Cu (II) ion monolayer chemisorption onto the nanofibers. The resultant hybrid fibers exhibited a maximum Cu (II) adsorption capacity of 125.47 mg/g.
AbstractList Using an electrospinning technique, thiol-modified silica nanoparticles were incorporated into poly(vinyl alcohol) (PVA) and poly(acrylic acid) (PAA) hybrid nanofibers to fabricate an eco-friendly adsorbentwith enhanced Cu (II) adsorption capacity. The hybrid nanofibers were successfully crosslinked throughheat treatment. Cu (II) adsorption characteristics of nanofibers were investigated including silicaquantity, surface modification, and pH. Adsorption isotherms and kineticsfit a Langmuir isotherm modeland pseudo-second-order model, respectively, implying Cu (II) ion monolayer chemisorption onto thenanofibers. The resultant hybridfibers exhibited a maximum Cu (II) adsorption capacity of 125.47 mg/g. KCI Citation Count: 21
[Display omitted] •Surface of silica nanoparticles was modified with thiol groups through sol–gel method.•Modified silica particles were incorporated into PVA/PAA nanofibers by eco-friendly electrospinning process.•Adsorption capacity of Cu (II) ions onto PVA/PAA nanofibers dramatically increased by incorporation of thiol-modified silica.•Adsorption behavior was rather chemisorption due to strong interaction between Cu (II) ions and thiol groups. Using an electrospinning technique, thiol-modified silica nanoparticles were incorporated into poly(vinyl alcohol) (PVA) and poly(acrylic acid) (PAA) hybrid nanofibers to fabricate an eco-friendly adsorbent with enhanced Cu (II) adsorption capacity. The hybrid nanofibers were successfully crosslinked through heat treatment. Cu (II) adsorption characteristics of nanofibers were investigated including silica quantity, surface modification, and pH. Adsorption isotherms and kinetics fit a Langmuir isotherm model and pseudo-second-order model, respectively, implying Cu (II) ion monolayer chemisorption onto the nanofibers. The resultant hybrid fibers exhibited a maximum Cu (II) adsorption capacity of 125.47 mg/g.
Author Kim, Jinyeong
Oh, Seong-Geun
Kang, Taeho
Kim, Hyewon
Shin, Hong Ju
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  surname: Kim
  fullname: Kim, Jinyeong
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  givenname: Taeho
  surname: Kang
  fullname: Kang, Taeho
  organization: Department of Chemical Engineering, Hanyang University, Seoul 04763, South Korea
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  givenname: Hyewon
  surname: Kim
  fullname: Kim, Hyewon
  organization: Department of Chemical Engineering, Hanyang University, Seoul 04763, South Korea
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  givenname: Hong Ju
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  givenname: Seong-Geun
  surname: Oh
  fullname: Oh, Seong-Geun
  email: seongoh@hanyang.ac.kr
  organization: Department of Chemical Engineering, Hanyang University, Seoul 04763, South Korea
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Keywords Eco-friendly electrospinning
Silica nanoparticles
Copper adsorption
Nanofiber
Thiol-modification
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한국공업화학회
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Snippet [Display omitted] •Surface of silica nanoparticles was modified with thiol groups through sol–gel method.•Modified silica particles were incorporated into...
Using an electrospinning technique, thiol-modified silica nanoparticles were incorporated into poly(vinyl alcohol) (PVA) and poly(acrylic acid) (PAA) hybrid...
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SubjectTerms Copper adsorption
Eco-friendly electrospinning
Nanofiber
Silica nanoparticles
Thiol-modification
화학공학
Title Preparation of PVA/PAA nanofibers containing thiol-modified silica particles by electrospinning as an eco-friendly Cu (II) adsorbent
URI https://dx.doi.org/10.1016/j.jiec.2019.04.048
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