Freeze‐dried graphene oxide modified with trimethylhexamethylene in the mix solvent for improved anti‐corrosion property of epoxy

Graphene oxide (GO) reinforcement to enhance the property of epoxy has been reported many times; with most of the papers focusing on how to modify GO with different functional groups to achieve better dispersion. Here, the importance of the preparation route on the coating systems performance was in...

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Published inJournal of applied polymer science Vol. 137; no. 38
Main Authors Hou, Weixin, Gao, Ya, Wang, John, Blackwood, Daniel J., Teo, Serena
Format Journal Article
LanguageEnglish
Published Hoboken, USA John Wiley & Sons, Inc 10.10.2020
Wiley Subscription Services, Inc
Subjects
adhesives
Coatings
composites
Corrosion
Curing agents
Diamines
Dispersion
Functional groups
glass transition
Graphene
Hydrophobicity
Materials science
Polymers
Solvents
thermogravimetric analysis
Xylene
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Abstract Graphene oxide (GO) reinforcement to enhance the property of epoxy has been reported many times; with most of the papers focusing on how to modify GO with different functional groups to achieve better dispersion. Here, the importance of the preparation route on the coating systems performance was investigated. It was found that a mixed polar/nonpolar solvent BuOH/xylene (3/1 vol/vol) was the best choice for forming the epoxy/GO coatings. Furthermore, it was found that when the freeze‐dried GO sonicated with the curing agent trimethylhexamethylene diamine in the mix solvent, the as‐prepared coating exhibited best performance, including better GO dispersion and hydrophobicity, higher adhesion, and anti‐corrosion property. Without any additional chemical to modify the GO, this optimized preparation route for epoxy/GO coatings will provide a guide for future similar research works, especially for the GO dispersion in nonaqueous systems. GO dispersion in epoxy/GO coatings prepared by different routes.
AbstractList Abstract Graphene oxide (GO) reinforcement to enhance the property of epoxy has been reported many times; with most of the papers focusing on how to modify GO with different functional groups to achieve better dispersion. Here, the importance of the preparation route on the coating systems performance was investigated. It was found that a mixed polar/nonpolar solvent BuOH/xylene (3/1 vol/vol) was the best choice for forming the epoxy/GO coatings. Furthermore, it was found that when the freeze‐dried GO sonicated with the curing agent trimethylhexamethylene diamine in the mix solvent, the as‐prepared coating exhibited best performance, including better GO dispersion and hydrophobicity, higher adhesion, and anti‐corrosion property. Without any additional chemical to modify the GO, this optimized preparation route for epoxy/GO coatings will provide a guide for future similar research works, especially for the GO dispersion in nonaqueous systems.
Graphene oxide (GO) reinforcement to enhance the property of epoxy has been reported many times; with most of the papers focusing on how to modify GO with different functional groups to achieve better dispersion. Here, the importance of the preparation route on the coating systems performance was investigated. It was found that a mixed polar/nonpolar solvent BuOH/xylene (3/1 vol/vol) was the best choice for forming the epoxy/GO coatings. Furthermore, it was found that when the freeze‐dried GO sonicated with the curing agent trimethylhexamethylene diamine in the mix solvent, the as‐prepared coating exhibited best performance, including better GO dispersion and hydrophobicity, higher adhesion, and anti‐corrosion property. Without any additional chemical to modify the GO, this optimized preparation route for epoxy/GO coatings will provide a guide for future similar research works, especially for the GO dispersion in nonaqueous systems. GO dispersion in epoxy/GO coatings prepared by different routes.
Graphene oxide (GO) reinforcement to enhance the property of epoxy has been reported many times; with most of the papers focusing on how to modify GO with different functional groups to achieve better dispersion. Here, the importance of the preparation route on the coating systems performance was investigated. It was found that a mixed polar/nonpolar solvent BuOH/xylene (3/1 vol/vol) was the best choice for forming the epoxy/GO coatings. Furthermore, it was found that when the freeze‐dried GO sonicated with the curing agent trimethylhexamethylene diamine in the mix solvent, the as‐prepared coating exhibited best performance, including better GO dispersion and hydrophobicity, higher adhesion, and anti‐corrosion property. Without any additional chemical to modify the GO, this optimized preparation route for epoxy/GO coatings will provide a guide for future similar research works, especially for the GO dispersion in nonaqueous systems.
Author Gao, Ya
Wang, John
Teo, Serena
Blackwood, Daniel J.
Hou, Weixin
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Snippet Graphene oxide (GO) reinforcement to enhance the property of epoxy has been reported many times; with most of the papers focusing on how to modify GO with...
Abstract Graphene oxide (GO) reinforcement to enhance the property of epoxy has been reported many times; with most of the papers focusing on how to modify GO...
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SubjectTerms adhesives
Coatings
composites
Corrosion
Curing agents
Diamines
Dispersion
Functional groups
glass transition
Graphene
Hydrophobicity
Materials science
Polymers
Solvents
thermogravimetric analysis
Xylene
Title Freeze‐dried graphene oxide modified with trimethylhexamethylene in the mix solvent for improved anti‐corrosion property of epoxy
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fapp.49139
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