Determination of structural parameters of uranyl ions complexed with organic acids using EXAFS
Two compounds of known crystal structure, sodium triacetatodioxouranium(VI), Na[UO 2(CH 3COO) 3], and dibenzoatodioxouranium(VI), UO 2[C 6H 5(COO)] 2, were studied by uranium L III-edge extended X-ray absorption fine structure, EXAFS, spectroscopy to differentiate between bidentate and monodentate c...
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| Published in | Journal of alloys and compounds Vol. 271; pp. 123 - 127 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
Elsevier B.V
12.06.1998
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| Abstract | Two compounds of known crystal structure, sodium triacetatodioxouranium(VI), Na[UO
2(CH
3COO)
3], and dibenzoatodioxouranium(VI), UO
2[C
6H
5(COO)]
2, were studied by uranium L
III-edge extended X-ray absorption fine structure, EXAFS, spectroscopy to differentiate between bidentate and monodentate coordination of carboxylate ions on the basis of the uranium–equatorial oxygen, O
eq, bond lengths. Bidentate coordination can be verified by detecting carboxyl carbon atoms and the neighboring distal carbon atom of the organic rest. In contrast, EXAFS spectra for monodentate carboxylate complexes show no evidence of carbon atoms beyond the O
eq coordination shell. The mode of coordination was determined by EXAFS analysis for solid uranyl complexes with humic, methoxybenzoic, and salicylic acids. A correlation between the U L
III-edge X-ray absorption near-edge structure, XANES, and the U–O
eq bond distance according to the relationship Δ
E·
R(O
eq)
2=constant was observed. For the samples studied, the constant was determined to be 197±8 eV Å
2. |
|---|---|
| AbstractList | Two compounds of known crystal structure, sodium triacetatodioxouranium(VI), Na[UO
2(CH
3COO)
3], and dibenzoatodioxouranium(VI), UO
2[C
6H
5(COO)]
2, were studied by uranium L
III-edge extended X-ray absorption fine structure, EXAFS, spectroscopy to differentiate between bidentate and monodentate coordination of carboxylate ions on the basis of the uranium–equatorial oxygen, O
eq, bond lengths. Bidentate coordination can be verified by detecting carboxyl carbon atoms and the neighboring distal carbon atom of the organic rest. In contrast, EXAFS spectra for monodentate carboxylate complexes show no evidence of carbon atoms beyond the O
eq coordination shell. The mode of coordination was determined by EXAFS analysis for solid uranyl complexes with humic, methoxybenzoic, and salicylic acids. A correlation between the U L
III-edge X-ray absorption near-edge structure, XANES, and the U–O
eq bond distance according to the relationship Δ
E·
R(O
eq)
2=constant was observed. For the samples studied, the constant was determined to be 197±8 eV Å
2. |
| Author | Reich, T Nitsche, H Allen, P.G Shuh, D.K Bubner, M Pompe, S Heise, K.H Denecke, M.A Edelstein, N.M Bucher, J.J |
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| Cites_doi | 10.1103/PhysRevB.54.156 10.1103/PhysRevB.34.7350 10.1039/dt9760002243 10.1107/S0567739482000114 10.1524/ract.1995.7071.special-issue.377 10.1016/0022-1902(75)80918-3 10.1016/0016-7037(92)90158-F 10.1524/ract.1997.79.3.151 10.1021/ic9508536 10.1103/PhysRevB.52.2995 |
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| Copyright | 1998 Elsevier Science S.A. |
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| Keywords | Bidentate coordination Monodentate coordination Extended X-ray absorption fine structure spectroscopy Carboxylate ions Dibenzoatodioxouranium(VI) Sodium triacetatodioxouranium(VI) |
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| References_xml | – volume: 35 start-page: 784 year: 1996 ident: BIB14 publication-title: Inorg. Chem. contributor: fullname: Nitsche – volume: 79 start-page: 151 year: 1997 ident: BIB8 publication-title: Radiochim. Acta contributor: fullname: Nitsche – volume: B32 start-page: 4292 year: 1984 ident: BIB17 publication-title: Phys. Rev. contributor: fullname: Petieau – volume: 82 start-page: 44 year: 1996 ident: BIB1 publication-title: Structure Bonding contributor: fullname: Kemp – volume: 7 start-page: C2 year: 1997 end-page: 637 ident: BIB2 publication-title: J. Physique IV contributor: fullname: Shuh – volume: 70, 71 start-page: 377 year: 1995 ident: BIB6 publication-title: Radiochim. Acta contributor: fullname: Nitsche – volume: B34 start-page: 7350 year: 1986 ident: BIB18 publication-title: Phys. Rev. contributor: fullname: Marcelli – volume: B54 start-page: 156 year: 1996 ident: BIB3 publication-title: Phys. Rev. contributor: fullname: Reich – volume: 4-5 start-page: 149 year: 1997 ident: BIB13 publication-title: Poverkhnost contributor: fullname: Nitsche – volume: 56 start-page: 3627 year: 1992 ident: BIB7 publication-title: Geochim. Cosmochim. Acta contributor: fullname: Hurley – volume: C41 start-page: 1439 year: 1985 ident: BIB4 publication-title: Acta Crystallogr. contributor: fullname: Templeton – volume: B52 start-page: 2995 year: 1995 ident: BIB11 publication-title: Phys. Rev. contributor: fullname: Eller – volume: C46 start-page: 2316 year: 1990 ident: BIB5 publication-title: Acta Crystallogr. contributor: fullname: Rizkalla – volume: A38 start-page: 62 year: 1982 ident: BIB16 publication-title: Acta Crystallogr. contributor: fullname: Templeton – volume: 37 start-page: 1933 year: 1975 ident: BIB12 publication-title: J. Inorg. Nucl. Chem. contributor: fullname: Morosin – volume: B54 start-page: 156 year: 1996 ident: 10.1016/S0925-8388(98)00038-3_BIB3 publication-title: Phys. Rev. doi: 10.1103/PhysRevB.54.156 contributor: fullname: Hudson – volume: B34 start-page: 7350 year: 1986 ident: 10.1016/S0925-8388(98)00038-3_BIB18 publication-title: Phys. Rev. doi: 10.1103/PhysRevB.34.7350 contributor: fullname: Petieau – volume: B32 start-page: 4292 year: 1984 ident: 10.1016/S0925-8388(98)00038-3_BIB17 publication-title: Phys. Rev. contributor: fullname: Bianconi – ident: 10.1016/S0925-8388(98)00038-3_BIB15 doi: 10.1039/dt9760002243 – volume: A38 start-page: 62 year: 1982 ident: 10.1016/S0925-8388(98)00038-3_BIB16 publication-title: Acta Crystallogr. doi: 10.1107/S0567739482000114 contributor: fullname: Templeton – ident: 10.1016/S0925-8388(98)00038-3_BIB10 – volume: 82 start-page: 44 year: 1996 ident: 10.1016/S0925-8388(98)00038-3_BIB1 publication-title: Structure Bonding contributor: fullname: Leciejewicz – volume: 7 start-page: C2 year: 1997 ident: 10.1016/S0925-8388(98)00038-3_BIB2 publication-title: J. Physique IV contributor: fullname: Denecke – volume: C46 start-page: 2316 year: 1990 ident: 10.1016/S0925-8388(98)00038-3_BIB5 publication-title: Acta Crystallogr. contributor: fullname: Cousson – volume: 70, 71 start-page: 377 year: 1995 ident: 10.1016/S0925-8388(98)00038-3_BIB6 publication-title: Radiochim. Acta doi: 10.1524/ract.1995.7071.special-issue.377 contributor: fullname: Silva – volume: C41 start-page: 1439 year: 1985 ident: 10.1016/S0925-8388(98)00038-3_BIB4 publication-title: Acta Crystallogr. contributor: fullname: Templeton – volume: 37 start-page: 1933 year: 1975 ident: 10.1016/S0925-8388(98)00038-3_BIB12 publication-title: J. Inorg. Nucl. Chem. doi: 10.1016/0022-1902(75)80918-3 contributor: fullname: Howatson – volume: 56 start-page: 3627 year: 1992 ident: 10.1016/S0925-8388(98)00038-3_BIB7 publication-title: Geochim. Cosmochim. Acta doi: 10.1016/0016-7037(92)90158-F contributor: fullname: Tipping – volume: 79 start-page: 151 year: 1997 ident: 10.1016/S0925-8388(98)00038-3_BIB8 publication-title: Radiochim. Acta doi: 10.1524/ract.1997.79.3.151 contributor: fullname: Denecke – volume: 35 start-page: 784 year: 1996 ident: 10.1016/S0925-8388(98)00038-3_BIB14 publication-title: Inorg. Chem. doi: 10.1021/ic9508536 contributor: fullname: Allen – volume: 4-5 start-page: 149 year: 1997 ident: 10.1016/S0925-8388(98)00038-3_BIB13 publication-title: Poverkhnost contributor: fullname: Reich – ident: 10.1016/S0925-8388(98)00038-3_BIB9 – volume: B52 start-page: 2995 year: 1995 ident: 10.1016/S0925-8388(98)00038-3_BIB11 publication-title: Phys. Rev. doi: 10.1103/PhysRevB.52.2995 contributor: fullname: Zabinsky |
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| Snippet | Two compounds of known crystal structure, sodium triacetatodioxouranium(VI), Na[UO
2(CH
3COO)
3], and dibenzoatodioxouranium(VI), UO
2[C
6H
5(COO)]
2, were... |
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| SubjectTerms | ABSORPTION SPECTROSCOPY Bidentate coordination Carboxylate ions Dibenzoatodioxouranium(VI) Extended X-ray absorption fine structure spectroscopy MOLECULAR STRUCTURE Monodentate coordination ORGANIC ACIDS RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEAR CHEMISTRY Sodium triacetatodioxouranium(VI) URANYL COMPLEXES X-RAY SPECTROSCOPY |
| Title | Determination of structural parameters of uranyl ions complexed with organic acids using EXAFS |
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