Effect of hydrolysis on the colloidal stability of fine alumina suspensions
This paper investigates the effect of hydrolysis and the formation of hydrated polycations on the colloidal stability and rheological properties of fine alumina suspensions. This is an important phenomenon in colloidal processing of advanced ceramic materials and nanocomposite materials from fine pa...
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Published in | Materials science & engineering. A, Structural materials : properties, microstructure and processing Vol. 204; no. 1; pp. 169 - 175 |
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Main Authors | , , , , , |
Format | Journal Article Conference Proceeding |
Language | English |
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Amsterdam
Elsevier B.V
01.12.1995
Elsevier |
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Abstract | This paper investigates the effect of hydrolysis and the formation of hydrated polycations on the colloidal stability and rheological properties of fine alumina suspensions. This is an important phenomenon in colloidal processing of advanced ceramic materials and nanocomposite materials from fine particles. The aging process and the formation of large polycations in the solution are monitored by nuclear magnetic resonance, and the aggregation rate and viscosity of the suspension are measured under similar conditions. It is observed that aging under acidic conditions increases colloidal stability against aggregation in dispersed suspensions, and reduces the viscosity in flocculated suspensions. This behavior corresponds well to the formation of large polynuclear species through hydrolysis. It is suggested that the hydrated polycations significantly modify the total interaction energy between two particles at short separation distances. |
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AbstractList | This paper investigates the effect of hydrolysis and the formation of hydrated polycations on the colloidal stability and rheological properties of fine alumina suspensions. This is an important phenomenon in colloidal processing of advanced ceramic materials and nanocomposite materials from fine particles. The aging process and the formation of large polycations in the solution are monitored by nuclear magnetic resonance, and the aggregation rate and viscosity of the suspension are measured under similar conditions. It is observed that aging under acidic conditions increases colloidal stability against aggregation in dispersed suspensions, and reduces the viscosity in flocculated suspensions. This behavior corresponds well to the formation of large polynuclear species through hydrolysis. It is suggested that the hydrated polycations significantly modify the total interaction energy between two particles at short separation distances. |
Author | Jones, R.H. Liu, J. Wang, L.Q. Virden, J.W. Bunker, B.C. Graff, G.L. |
Author_xml | – sequence: 1 givenname: J. surname: Liu fullname: Liu, J. – sequence: 2 givenname: L.Q. surname: Wang fullname: Wang, L.Q. – sequence: 3 givenname: B.C. surname: Bunker fullname: Bunker, B.C. – sequence: 4 givenname: G.L. surname: Graff fullname: Graff, G.L. – sequence: 5 givenname: J.W. surname: Virden fullname: Virden, J.W. – sequence: 6 givenname: R.H. surname: Jones fullname: Jones, R.H. |
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CitedBy_id | crossref_primary_10_15826_chimtech_2022_9_2_07 crossref_primary_10_1021_jp971609y crossref_primary_10_1006_jcis_1997_5013 crossref_primary_10_1016_j_jallcom_2013_10_019 |
Cites_doi | 10.1111/j.1151-2916.1990.tb05168.x 10.1016/0021-9797(77)90151-5 10.1111/j.1151-2916.1994.tb06980.x 10.1016/0021-9797(84)90316-3 10.1021/la00097a023 10.1007/BF00551313 10.1016/0927-7757(93)80329-D 10.1016/0021-9797(81)90348-9 10.1111/j.1151-2916.1989.tb05961.x 10.1111/j.1151-2916.1989.tb05945.x 10.1006/jcis.1993.1016 10.1111/j.1151-2916.1992.tb04426.x 10.1016/0166-6622(90)80101-9 10.1016/0021-9797(91)90047-C 10.1039/FT9928803201 10.1111/j.1151-2916.1994.tb07012.x 10.1111/j.1151-2916.1994.tb07266.x |
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Keywords | Hydrolysis Colloidal stability Fine alumina suspensions Viscosity Particle size Stability Colloids Binary compounds Ceramics Particle suspension Experimental study NMR Polycation Fine particle Alumina TEM Aluminium oxides Rheological properties |
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Soc. doi: 10.1111/j.1151-2916.1994.tb07266.x contributor: fullname: Luther – start-page: 60 year: 1990 ident: 10.1016/0921-5093(95)09955-7_BIB23 article-title: Sol-Gel Science contributor: fullname: Brinker |
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SubjectTerms | Chemistry Colloidal stability Colloidal state and disperse state Emulsions and suspensions Emulsions. Microemulsions. Foams Exact sciences and technology Fine alumina suspensions General and physical chemistry Hydrolysis |
Title | Effect of hydrolysis on the colloidal stability of fine alumina suspensions |
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