Effect of hydrolysis on the colloidal stability of fine alumina suspensions

This paper investigates the effect of hydrolysis and the formation of hydrated polycations on the colloidal stability and rheological properties of fine alumina suspensions. This is an important phenomenon in colloidal processing of advanced ceramic materials and nanocomposite materials from fine pa...

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Published inMaterials science & engineering. A, Structural materials : properties, microstructure and processing Vol. 204; no. 1; pp. 169 - 175
Main Authors Liu, J., Wang, L.Q., Bunker, B.C., Graff, G.L., Virden, J.W., Jones, R.H.
Format Journal Article Conference Proceeding
LanguageEnglish
Published Amsterdam Elsevier B.V 01.12.1995
Elsevier
Subjects
Chemistry
Colloidal stability
Colloidal state and disperse state
Emulsions and suspensions
Emulsions. Microemulsions. Foams
Exact sciences and technology
Fine alumina suspensions
General and physical chemistry
Hydrolysis
Hydrolysis
Colloidal stability
Fine alumina suspensions
Viscosity
Particle size
Stability
Colloids
Binary compounds
Ceramics
Particle suspension
Experimental study
NMR
Polycation
Fine particle
Alumina
TEM
Aluminium oxides
Rheological properties
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Abstract This paper investigates the effect of hydrolysis and the formation of hydrated polycations on the colloidal stability and rheological properties of fine alumina suspensions. This is an important phenomenon in colloidal processing of advanced ceramic materials and nanocomposite materials from fine particles. The aging process and the formation of large polycations in the solution are monitored by nuclear magnetic resonance, and the aggregation rate and viscosity of the suspension are measured under similar conditions. It is observed that aging under acidic conditions increases colloidal stability against aggregation in dispersed suspensions, and reduces the viscosity in flocculated suspensions. This behavior corresponds well to the formation of large polynuclear species through hydrolysis. It is suggested that the hydrated polycations significantly modify the total interaction energy between two particles at short separation distances.
AbstractList This paper investigates the effect of hydrolysis and the formation of hydrated polycations on the colloidal stability and rheological properties of fine alumina suspensions. This is an important phenomenon in colloidal processing of advanced ceramic materials and nanocomposite materials from fine particles. The aging process and the formation of large polycations in the solution are monitored by nuclear magnetic resonance, and the aggregation rate and viscosity of the suspension are measured under similar conditions. It is observed that aging under acidic conditions increases colloidal stability against aggregation in dispersed suspensions, and reduces the viscosity in flocculated suspensions. This behavior corresponds well to the formation of large polynuclear species through hydrolysis. It is suggested that the hydrated polycations significantly modify the total interaction energy between two particles at short separation distances.
Author Jones, R.H.
Liu, J.
Wang, L.Q.
Virden, J.W.
Bunker, B.C.
Graff, G.L.
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CitedBy_id crossref_primary_10_15826_chimtech_2022_9_2_07
crossref_primary_10_1021_jp971609y
crossref_primary_10_1006_jcis_1997_5013
crossref_primary_10_1016_j_jallcom_2013_10_019
Cites_doi 10.1111/j.1151-2916.1990.tb05168.x
10.1016/0021-9797(77)90151-5
10.1111/j.1151-2916.1994.tb06980.x
10.1016/0021-9797(84)90316-3
10.1021/la00097a023
10.1007/BF00551313
10.1016/0927-7757(93)80329-D
10.1016/0021-9797(81)90348-9
10.1111/j.1151-2916.1989.tb05961.x
10.1111/j.1151-2916.1989.tb05945.x
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10.1111/j.1151-2916.1992.tb04426.x
10.1016/0166-6622(90)80101-9
10.1016/0021-9797(91)90047-C
10.1039/FT9928803201
10.1111/j.1151-2916.1994.tb07012.x
10.1111/j.1151-2916.1994.tb07266.x
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Issue 1
Keywords Hydrolysis
Colloidal stability
Fine alumina suspensions
Viscosity
Particle size
Stability
Colloids
Binary compounds
Ceramics
Particle suspension
Experimental study
NMR
Polycation
Fine particle
Alumina
TEM
Aluminium oxides
Rheological properties
Language English
License CC BY 4.0
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PublicationTitle Materials science & engineering. A, Structural materials : properties, microstructure and processing
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Elsevier
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  year: 1990
  ident: 10.1016/0921-5093(95)09955-7_BIB23
  article-title: Sol-Gel Science
  contributor:
    fullname: Brinker
SSID ssj0001405
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Snippet This paper investigates the effect of hydrolysis and the formation of hydrated polycations on the colloidal stability and rheological properties of fine...
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elsevier
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StartPage 169
SubjectTerms Chemistry
Colloidal stability
Colloidal state and disperse state
Emulsions and suspensions
Emulsions. Microemulsions. Foams
Exact sciences and technology
Fine alumina suspensions
General and physical chemistry
Hydrolysis
Title Effect of hydrolysis on the colloidal stability of fine alumina suspensions
URI https://dx.doi.org/10.1016/0921-5093(95)09955-7
Volume 204
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