Directional assist (0 1 0) plane growth in LiMnPO4 prepared by solvothermal method with polyols to enhance electrochemical performance
[Display omitted] Phosphate material LiMnPO4 is popular for its high energy density (697 W·h·kg−1) and safety. When LiMnPO4 crystal grows, the potential barrier along b and c axis is strong, which makes the crystal grow along b axis to form a one-dimensional chain structure. However, the main migrat...
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| Published in | Chinese journal of chemical engineering Vol. 36; no. 8; pp. 181 - 189 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.08.2021
School of Chemistry and Chemical Engineering,Guangzhou University,Guangzhou 510006,China%Sunwoda Electronics Co.,Ltd.,Shenzhen 518107,China%GAC Automotive Research & Development Center,Guangzhou 511434,China%School of Chemical Engineering and Light Industry,Guangdong University of Technology,Guangzhou 510006,China |
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| Online Access | Get full text |
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| Abstract | [Display omitted]
Phosphate material LiMnPO4 is popular for its high energy density (697 W·h·kg−1) and safety. When LiMnPO4 crystal grows, the potential barrier along b and c axis is strong, which makes the crystal grow along b axis to form a one-dimensional chain structure. However, the main migration channel of lithium ions in olivine structure is plane (0 1 0). By shortening the growth in the direction of b axis and enhancing the diffusion along the directions of a and c, two-dimensional nanosheets that are more conducive to the migration of lithium ions are formed. The dosage of polyols is the key factor guiding the dispersion of the crystals to the (0 1 0) plane. X-ray diffraction (XRD), Scanning electron microscopy (SEM), transmission electron microscopy (TEM) and other means are used to characterize the samples. After experiments, we found that when the ratio of polyol/water was 2:1, the morphology of the synthesized sample was 20–30 nm thick nanosheets, which had the best electrochemical performance. At 0.1C, the discharge specific capacity reaches 148.9 mA·h·g−1, still reaches 144.3 mA·h·g−1 at the 50th cycle. and there is still 112.5 mA·h·g−1 under high rate (5C). This is thanks to the good dispersion of the material in the direction of the crystal plane (0 1 0). This can solve the problem of low conductivity and ionic mobility of phosphate materials. |
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| AbstractList | [Display omitted]
Phosphate material LiMnPO4 is popular for its high energy density (697 W·h·kg−1) and safety. When LiMnPO4 crystal grows, the potential barrier along b and c axis is strong, which makes the crystal grow along b axis to form a one-dimensional chain structure. However, the main migration channel of lithium ions in olivine structure is plane (0 1 0). By shortening the growth in the direction of b axis and enhancing the diffusion along the directions of a and c, two-dimensional nanosheets that are more conducive to the migration of lithium ions are formed. The dosage of polyols is the key factor guiding the dispersion of the crystals to the (0 1 0) plane. X-ray diffraction (XRD), Scanning electron microscopy (SEM), transmission electron microscopy (TEM) and other means are used to characterize the samples. After experiments, we found that when the ratio of polyol/water was 2:1, the morphology of the synthesized sample was 20–30 nm thick nanosheets, which had the best electrochemical performance. At 0.1C, the discharge specific capacity reaches 148.9 mA·h·g−1, still reaches 144.3 mA·h·g−1 at the 50th cycle. and there is still 112.5 mA·h·g−1 under high rate (5C). This is thanks to the good dispersion of the material in the direction of the crystal plane (0 1 0). This can solve the problem of low conductivity and ionic mobility of phosphate materials. Phosphate material LiMnPO4 is popular for its high energy density (697 W·h·kg-1) and safety.When LiMnPO4 crystal grows,the potential barrier along b and c axis is strong,which makes the crystal grow along b axis to form a one-dimensional chain structure.However,the main migration channel of lithium ions in olivine structure is plane (010).By shortening the growth in the direction ofb axis and enhancing the diffusion along the directions of a and c,two-dimensional nanosheets that are more conducive to the migration of lithium ions are formed.The dosage of polyols is the key factor guiding the dispersion of the crystals to the (010) plane.X-ray diffraction (XRD),Scanning electron microscopy (SEM),transmission electron microscopy (TEM) and other means are used to characterize the samples.After experiments,we found that when the ratio of polyol/water was 2∶1,the morphology of the synthesized sample was 20-30 nm thick nanosheets,which had the best electrochemical performance.At 0.1C,the discharge specific capacity reaches 148.9 mA·h·g-1,still reaches 144.3 mA·h·g-1 at the 50th cycle,and there is still 112.5 mA·h·g-1 under high rate (5C).This is thanks to the good dispersion of the material in the direction of the crystal plane (010).This can solve the problem of low conductivity and ionic mobility of phosphate materials. |
| Author | Zhu, Jihua Wang, Yali Xie, Qian Chen, Shengzhou Wang, Chengyun Fang, Kaibin Liu, Quanbing Yang, Wei |
| AuthorAffiliation | School of Chemistry and Chemical Engineering,Guangzhou University,Guangzhou 510006,China%Sunwoda Electronics Co.,Ltd.,Shenzhen 518107,China%GAC Automotive Research & Development Center,Guangzhou 511434,China%School of Chemical Engineering and Light Industry,Guangdong University of Technology,Guangzhou 510006,China |
| AuthorAffiliation_xml | – name: School of Chemistry and Chemical Engineering,Guangzhou University,Guangzhou 510006,China%Sunwoda Electronics Co.,Ltd.,Shenzhen 518107,China%GAC Automotive Research & Development Center,Guangzhou 511434,China%School of Chemical Engineering and Light Industry,Guangdong University of Technology,Guangzhou 510006,China |
| Author_xml | – sequence: 1 givenname: Qian surname: Xie fullname: Xie, Qian organization: School of Chemistry and Chemical Engineering, Guangzhou University, Guangzhou 510006, China – sequence: 2 givenname: Jihua surname: Zhu fullname: Zhu, Jihua organization: Sunwoda Electronics Co., Ltd., Shenzhen 518107, China – sequence: 3 givenname: Chengyun surname: Wang fullname: Wang, Chengyun organization: GAC Automotive Research & Development Center, Guangzhou 511434, China – sequence: 4 givenname: Kaibin surname: Fang fullname: Fang, Kaibin organization: School of Chemistry and Chemical Engineering, Guangzhou University, Guangzhou 510006, China – sequence: 5 givenname: Wei surname: Yang fullname: Yang, Wei email: wyang@gzhu.edu.cn organization: School of Chemistry and Chemical Engineering, Guangzhou University, Guangzhou 510006, China – sequence: 6 givenname: Quanbing surname: Liu fullname: Liu, Quanbing email: liuqb@gdut.edu.cn organization: School of Chemical Engineering and Light Industry, Guangdong University of Technology, Guangzhou 510006, China – sequence: 7 givenname: Yali surname: Wang fullname: Wang, Yali organization: School of Chemistry and Chemical Engineering, Guangzhou University, Guangzhou 510006, China – sequence: 8 givenname: Shengzhou surname: Chen fullname: Chen, Shengzhou organization: School of Chemistry and Chemical Engineering, Guangzhou University, Guangzhou 510006, China |
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| CitedBy_id | crossref_primary_10_1016_j_mtener_2022_101162 crossref_primary_10_1021_acs_iecr_1c04639 crossref_primary_10_1016_j_est_2024_112378 crossref_primary_10_1016_j_jpowsour_2024_236082 crossref_primary_10_1002_tcr_202200128 crossref_primary_10_1016_j_jallcom_2024_175853 crossref_primary_10_1016_j_ensm_2024_103722 crossref_primary_10_1016_j_ssi_2023_116274 crossref_primary_10_1016_j_mseb_2023_117032 crossref_primary_10_1016_j_ensm_2023_103125 crossref_primary_10_1002_aenm_202302893 crossref_primary_10_1016_j_jpowsour_2025_236747 |
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| Keywords | LMnPO4 Lithium-ion battery Polyols Phosphate material Crystal |
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Phosphate material LiMnPO4 is popular for its high energy density (697 W·h·kg−1) and safety. When LiMnPO4 crystal grows, the potential... Phosphate material LiMnPO4 is popular for its high energy density (697 W·h·kg-1) and safety.When LiMnPO4 crystal grows,the potential barrier along b and c axis... |
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