Selective reductive annulation reaction for direct synthesis of functionalized quinolines by a cobalt nanocatalyst
By developing a new N-doped ZrO2@C supported cobalt nanomaterial, it has been successfully applied as an efficient catalyst for the reductive annulation of 2-nitroaryl carbonyls with alkynoates and alkynones. The catalytic transformation allows synthesizing a wide array of funcitonalized quinolines...
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| Published in | Journal of catalysis Vol. 383; pp. 239 - 243 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Inc
01.03.2020
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0021-9517 1090-2694 |
| DOI | 10.1016/j.jcat.2020.01.034 |
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| Abstract | By developing a new N-doped ZrO2@C supported cobalt nanomaterial, it has been successfully applied as an efficient catalyst for the reductive annulation of 2-nitroaryl carbonyls with alkynoates and alkynones. The catalytic transformation allows synthesizing a wide array of funcitonalized quinolines with the merits of broad substrate scope, good functional group tolerance, excellent hydrogen transfer selectivity, reusable earth-abundant metal catalyst, and operational simplicity.
[Display omitted]
•New reductive annulation reaction.•New cobalt catalyst.•Direct access to functionalized quinolines.•Selective transfer hydrogenation.
Due to the extensive applications of quinolines, the search for selective construction of such products has long been an attractive subject in scientific community. Herein, by developing a new N-doped ZrO2@C supported cobalt nanomaterial, it has been successfully applied as an efficient catalyst for the reductive annulation of 2-nitroaryl carbonyls with alkynoates and alkynones. The catalytic transformation allows synthesizing a wide array of funcitonalized quinolines with the merits of broad substrate scope, good functional group tolerance, excellent hydrogen transfer selectivity, reusable earth-abundant metal catalyst, and operational simplicity. The developed chemistry paves the ways for further design of hydrogen transfer-mediated coupling reactions by developing heterogeneous catalysts with suitable supports. |
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| AbstractList | By developing a new N-doped ZrO2@C supported cobalt nanomaterial, it has been successfully applied as an efficient catalyst for the reductive annulation of 2-nitroaryl carbonyls with alkynoates and alkynones. The catalytic transformation allows synthesizing a wide array of funcitonalized quinolines with the merits of broad substrate scope, good functional group tolerance, excellent hydrogen transfer selectivity, reusable earth-abundant metal catalyst, and operational simplicity.
[Display omitted]
•New reductive annulation reaction.•New cobalt catalyst.•Direct access to functionalized quinolines.•Selective transfer hydrogenation.
Due to the extensive applications of quinolines, the search for selective construction of such products has long been an attractive subject in scientific community. Herein, by developing a new N-doped ZrO2@C supported cobalt nanomaterial, it has been successfully applied as an efficient catalyst for the reductive annulation of 2-nitroaryl carbonyls with alkynoates and alkynones. The catalytic transformation allows synthesizing a wide array of funcitonalized quinolines with the merits of broad substrate scope, good functional group tolerance, excellent hydrogen transfer selectivity, reusable earth-abundant metal catalyst, and operational simplicity. The developed chemistry paves the ways for further design of hydrogen transfer-mediated coupling reactions by developing heterogeneous catalysts with suitable supports. Due to the extensive applications of quinolines, the search for selective construction of such products has long been an attractive subject in scientific community. Herein, by developing a new N-doped ZrO₂@C supported cobalt nanomaterial, it has been successfully applied as an efficient catalyst for the reductive annulation of 2-nitroaryl carbonyls with alkynoates and alkynones. The catalytic transformation allows synthesizing a wide array of funcitonalized quinolines with the merits of broad substrate scope, good functional group tolerance, excellent hydrogen transfer selectivity, reusable earth-abundant metal catalyst, and operational simplicity. The developed chemistry paves the ways for further design of hydrogen transfer-mediated coupling reactions by developing heterogeneous catalysts with suitable supports. |
| Author | Xie, Rong Lu, Guang-Peng Jiang, Huan-Feng Zhang, Min |
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| Keywords | Reductive annulation Heterogeneous catalysis Transfer hydrogenation Functionalized quinolines Cobalt |
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| Snippet | By developing a new N-doped ZrO2@C supported cobalt nanomaterial, it has been successfully applied as an efficient catalyst for the reductive annulation of... Due to the extensive applications of quinolines, the search for selective construction of such products has long been an attractive subject in scientific... |
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| SubjectTerms | catalytic activity Cobalt Functionalized quinolines Heterogeneous catalysis hydrogen moieties nanocatalysts nanomaterials quinolines Reductive annulation Transfer hydrogenation zirconium oxide |
| Title | Selective reductive annulation reaction for direct synthesis of functionalized quinolines by a cobalt nanocatalyst |
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