Experimental evidence for segregation of interstitial impurities to defects in a near α titanium alloy during dynamic strain aging using energy filtered transmission electron microscopy

Dynamic strain aging was observed in the temperature range between 300°C and 500°C in a near α titanium alloy 834 without Silicon (10.38%Al–0.16%Sn–1.86%Zr–0.37%Nb–0.25%Mo–0.27%C–0.30%O–0.006%N, all in at%) tested in the temperature range from room temperature to 500°C. Electron microscopic investig...

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Published inMaterials science & engineering. A, Structural materials : properties, microstructure and processing Vol. 638; pp. 90 - 96
Main Authors Prasad, Kartik, Amrithapandian, S., Panigrahi, B.K., Kumar, Vikas, Bhanu Sankara Rao, K., Sundararaman, M.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 25.06.2015
Subjects
Carbon
Defects
Diffusion
Dislocations
Dynamic strain aging
Electron microscopy
Energy filtered transmission electron microscopy (EFTEM)
Energy transmission
High temperature alloys
Interstitials
Mechanical properties
Segregations
Titanium base alloys
Mechanical properties
High temperature alloys
Energy filtered transmission electron microscopy (EFTEM)
Diffusion
Dislocations
Dynamic strain aging
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Abstract Dynamic strain aging was observed in the temperature range between 300°C and 500°C in a near α titanium alloy 834 without Silicon (10.38%Al–0.16%Sn–1.86%Zr–0.37%Nb–0.25%Mo–0.27%C–0.30%O–0.006%N, all in at%) tested in the temperature range from room temperature to 500°C. Electron microscopic investigation of tensile tested samples in an energy filtered transmission electron microscopy provided direct experimental evidence for segregation of interstitial elements like carbon (C) and nitrogen (N) to lath boundaries and dislocation pile ups. On the basis of these results and the comparison of lattice strain generated by different interstitials in α-Ti, it was concluded that segregation of carbon and nitrogen and not oxygen to defects is responsible for DSA in this alloy.
AbstractList Dynamic strain aging was observed in the temperature range between 300°C and 500°C in a near α titanium alloy 834 without Silicon (10.38%Al–0.16%Sn–1.86%Zr–0.37%Nb–0.25%Mo–0.27%C–0.30%O–0.006%N, all in at%) tested in the temperature range from room temperature to 500°C. Electron microscopic investigation of tensile tested samples in an energy filtered transmission electron microscopy provided direct experimental evidence for segregation of interstitial elements like carbon (C) and nitrogen (N) to lath boundaries and dislocation pile ups. On the basis of these results and the comparison of lattice strain generated by different interstitials in α-Ti, it was concluded that segregation of carbon and nitrogen and not oxygen to defects is responsible for DSA in this alloy.
Dynamic strain aging was observed in the temperature range between 300 degree C and 500 degree C in a near alpha titanium alloy 834 without Silicon (10.38%Al-0.16%Sn-1.86%Zr-0.37%Nb-0.25% Mo-0.27%C-0.30%O-0.006%N, all in at%) tested in the temperature range from room temperature to 500 degree C. Electron microscopic investigation of tensile tested samples in an energy filtered transmission electron microscopy provided direct experimental evidence for segregation of interstitial elements like carbon (C) and nitrogen (N) to lath boundaries and dislocation pile ups. On the basis of these results and the comparison of lattice strain generated by different interstitials in alpha -Ti, it was concluded that segregation of carbon and nitrogen and not oxygen to defects is responsible for DSA in this alloy.
Author Prasad, Kartik
Bhanu Sankara Rao, K.
Sundararaman, M.
Amrithapandian, S.
Kumar, Vikas
Panigrahi, B.K.
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Keywords Mechanical properties
High temperature alloys
Energy filtered transmission electron microscopy (EFTEM)
Diffusion
Dislocations
Dynamic strain aging
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Snippet Dynamic strain aging was observed in the temperature range between 300°C and 500°C in a near α titanium alloy 834 without Silicon...
Dynamic strain aging was observed in the temperature range between 300 degree C and 500 degree C in a near alpha titanium alloy 834 without Silicon...
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StartPage 90
SubjectTerms Carbon
Defects
Diffusion
Dislocations
Dynamic strain aging
Electron microscopy
Energy filtered transmission electron microscopy (EFTEM)
Energy transmission
High temperature alloys
Interstitials
Mechanical properties
Segregations
Titanium base alloys
Title Experimental evidence for segregation of interstitial impurities to defects in a near α titanium alloy during dynamic strain aging using energy filtered transmission electron microscopy
URI https://dx.doi.org/10.1016/j.msea.2015.04.060
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