Structural study and thermal stability of Artemetin extracted from Artemisia absinthium L
The interest given to the bioactive properties of phenolic compounds, extracted from aromatic and medicinal plants, has eclipsed in a sense the physicochemical characterization of these molecules which are from a chemical point of view only chemical reagents. In this work, the molecule C20H20O8 (Art...
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| Published in | Chemical Data Collections Vol. 40; p. 100880 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.08.2022
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| Subjects | |
| Online Access | Get full text |
| ISSN | 2405-8300 2405-8300 |
| DOI | 10.1016/j.cdc.2022.100880 |
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| Abstract | The interest given to the bioactive properties of phenolic compounds, extracted from aromatic and medicinal plants, has eclipsed in a sense the physicochemical characterization of these molecules which are from a chemical point of view only chemical reagents. In this work, the molecule C20H20O8 (Artemetin), extracted from Artemisia absinthium L by hexane and then by diethyl ether was studied. The Artemetin extract was concentrated and characterized by High-performance liquid chromatography-Diode array detector, Single crystals and powder were isolated by solvent evaporation and recrystallization. They were characterized by X-Ray Diffraction, Infrared spectroscopy, Ultraviolet–visible spectroscopy, scanning electron microscope- Energy-dispersive X-ray spectroscopy, Differential Thermal-Thermogravimetric-Calorimetry Analysis. The concentrate of the extract can reach 98% in Artemetin. The structure of the isolated single crystal is identical to that of Artemetin with more precision in the interatomic distances and angles. The thermal stability range of artemetin was studied in an oxidizing (air) or inert (N2) atmosphere. The temperature and enthalpy of fusion were determined (Tfus = 160 °C, ΔHfus = 1.36 kJ/mol). Quantum chemical calculations have made it possible to evaluate the optimized geometry of artemetin, which is described as a soft molecule with a high molecular polarity that can give it a high chemical reactivity. |
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| AbstractList | The interest given to the bioactive properties of phenolic compounds, extracted from aromatic and medicinal plants, has eclipsed in a sense the physicochemical characterization of these molecules which are from a chemical point of view only chemical reagents. In this work, the molecule C20H20O8 (Artemetin), extracted from Artemisia absinthium L by hexane and then by diethyl ether was studied. The Artemetin extract was concentrated and characterized by High-performance liquid chromatography-Diode array detector, Single crystals and powder were isolated by solvent evaporation and recrystallization. They were characterized by X-Ray Diffraction, Infrared spectroscopy, Ultraviolet–visible spectroscopy, scanning electron microscope- Energy-dispersive X-ray spectroscopy, Differential Thermal-Thermogravimetric-Calorimetry Analysis. The concentrate of the extract can reach 98% in Artemetin. The structure of the isolated single crystal is identical to that of Artemetin with more precision in the interatomic distances and angles. The thermal stability range of artemetin was studied in an oxidizing (air) or inert (N2) atmosphere. The temperature and enthalpy of fusion were determined (Tfus = 160 °C, ΔHfus = 1.36 kJ/mol). Quantum chemical calculations have made it possible to evaluate the optimized geometry of artemetin, which is described as a soft molecule with a high molecular polarity that can give it a high chemical reactivity. |
| ArticleNumber | 100880 |
| Author | Ammari, Lahcen El Hbika, Asmae Bouyanzer, Abdelhamid Gharibi, El Khadir Saadi, Mohamed Zarrouk, Abdelkader Benali, Mohammed Majidi, Lhou |
| Author_xml | – sequence: 1 givenname: Asmae surname: Hbika fullname: Hbika, Asmae organization: Laboratory of Applied Chemistry and Environment, team Applied Analytical Chemistry of Materials and Environment Faculty of Sciences, Mohammed First University, Oujda, Morocco – sequence: 2 givenname: Abdelhamid surname: Bouyanzer fullname: Bouyanzer, Abdelhamid email: bouyanzer@yahoo.fr organization: Laboratory of Applied Chemistry and Environment, team Applied Analytical Chemistry of Materials and Environment Faculty of Sciences, Mohammed First University, Oujda, Morocco – sequence: 3 givenname: Mohamed surname: Saadi fullname: Saadi, Mohamed organization: Laboratoire de Chimie Appliquée des Matériaux Centre des Sciences des Matériaux, Faculty of Science, Mohammed V University in Rabat, Avenue Ibn Batouta, B.P. 1014, Rabat, Morocco – sequence: 4 givenname: Lahcen El surname: Ammari fullname: Ammari, Lahcen El organization: Laboratoire de Chimie Appliquée des Matériaux Centre des Sciences des Matériaux, Faculty of Science, Mohammed V University in Rabat, Avenue Ibn Batouta, B.P. 1014, Rabat, Morocco – sequence: 5 givenname: Mohammed surname: Benali fullname: Benali, Mohammed organization: Université de Technologie de Compiègne, ESCOM, TIMR (Integrated Transformations of Renewable Matter), Centre de recherche Royallieu, CS 60319 – 60203, Compiègne Cedex, France – sequence: 6 givenname: Lhou surname: Majidi fullname: Majidi, Lhou organization: Laboratory of Natural Substances Synthesis and Molecular Dynamics, Faculty of Sciences and Techniques, Moulay Ismail University, Errachidia, Morocco – sequence: 7 givenname: El Khadir surname: Gharibi fullname: Gharibi, El Khadir organization: Laboratory of Applied Chemistry and Environment, Team Solid Mineral Chemistry, Faculty of Sciences, Mohammed First University, Oujda, Morocco – sequence: 8 givenname: Abdelkader orcidid: 0000-0002-5495-2125 surname: Zarrouk fullname: Zarrouk, Abdelkader email: azarrouk@gmail.com organization: Laboratory of Materials, Nanotechnology and Environment, Faculty of Sciences, Mohammed V University in Rabat, P.O. Box. 1014, Rabat, Morocco |
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| Keywords | Artemisia absinthium L Aromatic and medicinal plants Artemetin X-Ray Diffraction/Infrared spectroscopy/Ultraviolet–visible spectroscopy Recrystallization, Crystal structure |
| Language | English |
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| SubjectTerms | Aromatic and medicinal plants Artemetin Artemisia absinthium L Chemical Sciences Recrystallization, Crystal structure X-Ray Diffraction/Infrared spectroscopy/Ultraviolet–visible spectroscopy |
| Title | Structural study and thermal stability of Artemetin extracted from Artemisia absinthium L |
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