Enhanced head-to-head photodimers in the photocyclodimerization of anthracenecarboxylic acid with a cationic pillar[6]arene
The complexation behaviors of anthracenecarboxylic acid and water-soluble cationic pillararenes have been investigated by 1H NMR,UV-vis and ITC methods.The cationic pillar[6]arene was found to stepwise form 1：1 and 1：2 complexes,having a large K1 and a relatively small K2 values.Photocyclodimerizati...
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| Published in | Chinese chemical letters Vol. 27; no. 7; pp. 1017 - 1021 |
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| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.07.2016
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| Abstract | The complexation behaviors of anthracenecarboxylic acid and water-soluble cationic pillararenes have been investigated by 1H NMR,UV-vis and ITC methods.The cationic pillar[6]arene was found to stepwise form 1：1 and 1：2 complexes,having a large K1 and a relatively small K2 values.Photocyclodimerization of AC within the pillar[6]arene improved the yield of the head-to-head photodimers.Up to 4.97 HH/HT ratio has been reached by optimizing the reaction conditions. |
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| AbstractList | The complexation behaviors of anthracenecarboxylic acid and water-soluble cationic pillararenes have been investigated by 1H NMR,UV-vis and ITC methods.The cationic pillar[6]arene was found to stepwise form 1：1 and 1：2 complexes,having a large K1 and a relatively small K2 values.Photocyclodimerization of AC within the pillar[6]arene improved the yield of the head-to-head photodimers.Up to 4.97 HH/HT ratio has been reached by optimizing the reaction conditions. Photocyclodimerization of anthracenecarboxylic acid within a cationic pillar[6]arene improved the yield of the head-to-head photodimers. [Display omitted] The complexation behaviors of anthracenecarboxylic acid and water-soluble cationic pillararenes have been investigated by 1H NMR, UV–vis and ITC methods. The cationic pillar[6]arene was found to stepwise form 1:1 and 1:2 complexes, having a large K1 and a relatively small K2 values. Photocyclodimerization of AC within the pillar[6]arene improved the yield of the head-to-head photodimers. Up to 4.97 HH/HT ratio has been reached by optimizing the reaction conditions. |
| Author | Jian-Chang Gui Zhi-Qiang Yan Yuan Peng Ji-Gao Yi Da-Yang Zhou Dan Su Zhi-Hui Zhong Guo-Wei Gao Wan-Hua Wu Cheng Yang |
| AuthorAffiliation | Key Laboratory of Green Chemistry ＆ Technology, College of Chemistry, State Key Laboratory of Biotherapy, West China Medical Center and State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610064, China Chengdu Environmental Monitoring Center, Chengdu 610042, China Comprehensive Analysis Center, ISIR, Osaka University, 8-I Mihogaoka, lbaraki, Osaka 5670047, Japan |
| Author_xml | – sequence: 1 givenname: Jian-Chang surname: Gui fullname: Gui, Jian-Chang organization: Key Laboratory of Green Chemistry & Technology, College of Chemistry, State Key Laboratory of Biotherapy, West China Medical Center and State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610064, China – sequence: 2 givenname: Zhi-Qiang surname: Yan fullname: Yan, Zhi-Qiang organization: Key Laboratory of Green Chemistry & Technology, College of Chemistry, State Key Laboratory of Biotherapy, West China Medical Center and State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610064, China – sequence: 3 givenname: Yuan surname: Peng fullname: Peng, Yuan organization: Chengdu Environmental Monitoring Center, Chengdu 610042, China – sequence: 4 givenname: Ji-Gao surname: Yi fullname: Yi, Ji-Gao organization: Key Laboratory of Green Chemistry & Technology, College of Chemistry, State Key Laboratory of Biotherapy, West China Medical Center and State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610064, China – sequence: 5 givenname: Da-Yang surname: Zhou fullname: Zhou, Da-Yang organization: Comprehensive Analysis Center, ISIR, Osaka University, 8-1 Mihogaoka, Ibaraki, Osaka 5670047, Japan – sequence: 6 givenname: Dan surname: Su fullname: Su, Dan organization: Key Laboratory of Green Chemistry & Technology, College of Chemistry, State Key Laboratory of Biotherapy, West China Medical Center and State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610064, China – sequence: 7 givenname: Zhi-Hui surname: Zhong fullname: Zhong, Zhi-Hui organization: Key Laboratory of Green Chemistry & Technology, College of Chemistry, State Key Laboratory of Biotherapy, West China Medical Center and State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610064, China – sequence: 8 givenname: Guo-Wei surname: Gao fullname: Gao, Guo-Wei organization: Key Laboratory of Green Chemistry & Technology, College of Chemistry, State Key Laboratory of Biotherapy, West China Medical Center and State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610064, China – sequence: 9 givenname: Wan-Hua surname: Wu fullname: Wu, Wan-Hua organization: Key Laboratory of Green Chemistry & Technology, College of Chemistry, State Key Laboratory of Biotherapy, West China Medical Center and State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610064, China – sequence: 10 givenname: Cheng surname: Yang fullname: Yang, Cheng email: yangchengyc@scu.edu.cn organization: Key Laboratory of Green Chemistry & Technology, College of Chemistry, State Key Laboratory of Biotherapy, West China Medical Center and State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610064, China |
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| Keywords | Anthracenecarboxylic acid Supramolecular complexation Photocyclodimerization Pillararene |
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| Notes | 11-2710/O6 Pillar[6]arene;Photocyclodimerization;Anthracenecarboxylic acid;Supramolecular complexation The complexation behaviors of anthracenecarboxylic acid and water-soluble cationic pillararenes have been investigated by 1H NMR,UV-vis and ITC methods.The cationic pillar[6]arene was found to stepwise form 1：1 and 1：2 complexes,having a large K1 and a relatively small K2 values.Photocyclodimerization of AC within the pillar[6]arene improved the yield of the head-to-head photodimers.Up to 4.97 HH/HT ratio has been reached by optimizing the reaction conditions. |
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| Snippet | The complexation behaviors of anthracenecarboxylic acid and water-soluble cationic pillararenes have been investigated by 1H NMR,UV-vis and ITC methods.The... Photocyclodimerization of anthracenecarboxylic acid within a cationic pillar[6]arene improved the yield of the head-to-head photodimers. [Display omitted] The... |
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| SubjectTerms | Anthracenecarboxylic acid Photocyclodimerization Pillararene Supramolecular complexation 光二聚反应 反应条件 水溶性 甲酸 络合性能 芳烃 蒽 阳离子柱 |
| Title | Enhanced head-to-head photodimers in the photocyclodimerization of anthracenecarboxylic acid with a cationic pillar[6]arene |
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