Effect of Crosslinking Agents on the Morphology of Polymer Particles Produced by One-Step Seeded Polymerization
One-step seeded polymerization was used to prepare 7∼10 μm of crosslinked monodisperse spheres with four crosslinking agents using 4.68 μm poly(methyl methacrylate) (PMMA) seed particles in aqueous-alcoholic media in the absence of the swelling process. The crosslinking agents used were ethylene gly...
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Published in | Macromolecular research Vol. 17; no. 4; pp. 250 - 258 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
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Berlin/Heidelberg
한국고분자학회
01.04.2009
Springer-Verlag |
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Abstract | One-step seeded polymerization was used to prepare 7∼10 μm of crosslinked monodisperse spheres with four crosslinking agents using 4.68 μm poly(methyl methacrylate) (PMMA) seed particles in aqueous-alcoholic media in the absence of the swelling process. The crosslinking agents used were ethylene glycol dimethacrylate (EGDMA), allyl methacrylate (AMA), 1,6-hexanediol diacrylate (HDDA) and trimethylolpropane trimethacrylate (TMPTMA). The effects of the type and concentration of the crosslinking agents on the swelling, pore size, thermal property of the networks and morphology of the particles were studied. The chemical structures and concentrations of the crosslinking agents affected both the swelling ratio and the porosity of the networks. In addition, the chemistry of the reactive vinyl group and chain length of the crosslinking agents affected the stability of the monodisperse particles of the ultimate morphology. |
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AbstractList | One-step seeded polymerization was used to prepare 7~10 μm of crosslinked monodisperse spheres with four crosslinking agents using 4.68 μm poly(methyl methacrylate) (PMMA) seed particles in aqueous-alcoholic media in the absence of the swelling process. The crosslinking agents used were ethylene glycol dimethacrylate (EGDMA), allyl methacrylate (AMA), 1,6-hexanediol diacrylate (HDDA) and trimethylolpropane trimethacrylate
(TMPTMA). The effects of the type and concentration of the crosslinking agents on the swelling, pore size, thermal property of the networks and morphology of the particles were studied. The chemical structures and concentrations of the crosslinking agents affected both the swelling ratio and the porosity of the networks. In addition, the chemistry of the reactive vinyl group and chain length of the crosslinking agents affected the stability of the monodisperse particles of the ultimate morphology. KCI Citation Count: 30 One-step seeded polymerization was used to prepare 7∼10 μm of crosslinked monodisperse spheres with four crosslinking agents using 4.68 μm poly(methyl methacrylate) (PMMA) seed particles in aqueous-alcoholic media in the absence of the swelling process. The crosslinking agents used were ethylene glycol dimethacrylate (EGDMA), allyl methacrylate (AMA), 1,6-hexanediol diacrylate (HDDA) and trimethylolpropane trimethacrylate (TMPTMA). The effects of the type and concentration of the crosslinking agents on the swelling, pore size, thermal property of the networks and morphology of the particles were studied. The chemical structures and concentrations of the crosslinking agents affected both the swelling ratio and the porosity of the networks. In addition, the chemistry of the reactive vinyl group and chain length of the crosslinking agents affected the stability of the monodisperse particles of the ultimate morphology. |
Author | Do Yang Lee Soon Ja Choe Dong Hee Kim Kang Seok Lee |
Author_xml | – sequence: 1 givenname: Donghee surname: Kim fullname: Kim, Donghee organization: Department of Chemical Engineering, Inha University – sequence: 2 givenname: Do Yang surname: Lee fullname: Lee, Do Yang organization: Department of Chemical Engineering, Inha University – sequence: 3 givenname: Kangseok surname: Lee fullname: Lee, Kangseok organization: Department of Chemical Engineering, Inha University – sequence: 4 givenname: Soonja surname: Choe fullname: Choe, Soonja email: sjchoe@inha.ac.kr organization: Department of Chemical Engineering, Inha University |
BackLink | https://www.kci.go.kr/kciportal/ci/sereArticleSearch/ciSereArtiView.kci?sereArticleSearchBean.artiId=ART001337002$$DAccess content in National Research Foundation of Korea (NRF) |
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Snippet | One-step seeded polymerization was used to prepare 7∼10 μm of crosslinked monodisperse spheres with four crosslinking agents using 4.68 μm poly(methyl... One-step seeded polymerization was used to prepare 7~10 μm of crosslinked monodisperse spheres with four crosslinking agents using 4.68 μm poly(methyl... |
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SubjectTerms | Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Complex Fluids and Microfluidics Nanochemistry Nanotechnology Physical Chemistry Polymer Sciences Soft and Granular Matter 고분자공학 |
Title | Effect of Crosslinking Agents on the Morphology of Polymer Particles Produced by One-Step Seeded Polymerization |
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