Graphene-wrapped WO3 nanospheres with room-temperature NO2 sensing induced by interface charge transfer
Graphene (GR)-wrapped WO3 nanosphere composite was synthesized by using a facile sol–gel method. The morphology and structural properties of the GR-WO3 nanocomposites were characterized by field-emission scanning electron microscopy (FESEM), X-ray powder diffraction (XRD), transmission electron micr...
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| Published in | Sensors and actuators. B, Chemical Vol. 220; pp. 201 - 209 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.12.2015
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| Abstract | Graphene (GR)-wrapped WO3 nanosphere composite was synthesized by using a facile sol–gel method. The morphology and structural properties of the GR-WO3 nanocomposites were characterized by field-emission scanning electron microscopy (FESEM), X-ray powder diffraction (XRD), transmission electron microscopy (TEM), and Raman spectroscopy. The GR-wrapped WO3 nanospheres composite exhibits p-type gas sensing behavior and the response of GR-WO3 sensor toward NO2 shows a linear increase with an increase in the concentration from 7 to 56ppm at room temperature. Upon exposure to 56ppm NO2, its response value becomes 40.8%, but there is no responsiveness for the sensors based on pure WO3 and graphene sensors. The effective charge transfer through chemically bonded interfacial contact between graphene and WO3 nanospheres is proposed to be responsible for the room temperature sensing performance. This work may provide a new insight into the structural design of GR-base nanocomposites and has a potential prospect in the environment monitoring or disease detection of NO2 at room temperature. |
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| AbstractList | Graphene (GR)-wrapped WO3 nanosphere composite was synthesized by using a facile sol–gel method. The morphology and structural properties of the GR-WO3 nanocomposites were characterized by field-emission scanning electron microscopy (FESEM), X-ray powder diffraction (XRD), transmission electron microscopy (TEM), and Raman spectroscopy. The GR-wrapped WO3 nanospheres composite exhibits p-type gas sensing behavior and the response of GR-WO3 sensor toward NO2 shows a linear increase with an increase in the concentration from 7 to 56ppm at room temperature. Upon exposure to 56ppm NO2, its response value becomes 40.8%, but there is no responsiveness for the sensors based on pure WO3 and graphene sensors. The effective charge transfer through chemically bonded interfacial contact between graphene and WO3 nanospheres is proposed to be responsible for the room temperature sensing performance. This work may provide a new insight into the structural design of GR-base nanocomposites and has a potential prospect in the environment monitoring or disease detection of NO2 at room temperature. |
| Author | Zeng, Dawen Zhang, Jian Zhu, Baokun Jie, Xiaoqin Xu, Keng Wu, Jinjin Xie, Changsheng |
| Author_xml | – sequence: 1 givenname: Xiaoqin surname: Jie fullname: Jie, Xiaoqin organization: State Key Laboratory of Materials Processing and Die & Mould Technology, Huazhong University of Science and Technology, No. 1037, Luoyu Road, Wuhan 430074, PR China – sequence: 2 givenname: Dawen surname: Zeng fullname: Zeng, Dawen email: dwzeng@mail.hust.edu.cn organization: State Key Laboratory of Materials Processing and Die & Mould Technology, Huazhong University of Science and Technology, No. 1037, Luoyu Road, Wuhan 430074, PR China – sequence: 3 givenname: Jian surname: Zhang fullname: Zhang, Jian organization: Nanomaterials and Smart Sensors Research Laboratory (NSSRL), Department of Materials Science and Engineering, Huazhong University of Science and Technology, No. 1037, Luoyu Road, Wuhan 430074, PR China – sequence: 4 givenname: Keng surname: Xu fullname: Xu, Keng organization: Nanomaterials and Smart Sensors Research Laboratory (NSSRL), Department of Materials Science and Engineering, Huazhong University of Science and Technology, No. 1037, Luoyu Road, Wuhan 430074, PR China – sequence: 5 givenname: Jinjin surname: Wu fullname: Wu, Jinjin organization: Nanomaterials and Smart Sensors Research Laboratory (NSSRL), Department of Materials Science and Engineering, Huazhong University of Science and Technology, No. 1037, Luoyu Road, Wuhan 430074, PR China – sequence: 6 givenname: Baokun surname: Zhu fullname: Zhu, Baokun organization: R&D Center of China Tobacco Yunan Industrial CO., Ltd., No. 367, Hongjin Road, Wuhua District, Kunming, Yunnan, PR China – sequence: 7 givenname: Changsheng surname: Xie fullname: Xie, Changsheng organization: Nanomaterials and Smart Sensors Research Laboratory (NSSRL), Department of Materials Science and Engineering, Huazhong University of Science and Technology, No. 1037, Luoyu Road, Wuhan 430074, PR China |
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| Snippet | Graphene (GR)-wrapped WO3 nanosphere composite was synthesized by using a facile sol–gel method. The morphology and structural properties of the GR-WO3... Graphene (GR)-wrapped WO3 nanosphere composite was synthesized by using a facile sol-gel method. The morphology and structural properties of the GR-WO3... |
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| SubjectTerms | Charge transfer Detection Gas sensing GR-WO3 nanocomposites Graphene Nanospheres Nitrogen dioxide NO2 Room temperature Scanning electron microscopy Sensors Tungsten oxides WO3 |
| Title | Graphene-wrapped WO3 nanospheres with room-temperature NO2 sensing induced by interface charge transfer |
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