Enhanced removal of I− on hierarchically structured layered double hydroxides by in suit growth of Cu/Cu2O

To further improve the removal ability of layered double hydroxide (LDH) for iodide (I−) anions from wastewater, we prepared hierarchically porous Cu5Mg10Al5-LDH and used as a matrix for in suit growth of Cu/Cu2O on its surface, forming Cu/Cu2O-LDH, which was characterized and applied as an adsorben...

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Published inJournal of environmental sciences (China) Vol. 88; pp. 338 - 348
Main Authors Chen, Jiuyu, Wang, Junyi, Gao, Qianhong, Zhang, Xiaomei, Liu, Ying, Wang, Peng, Jiao, Yan, Zhang, Zongxiang, Yang, Yi
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.02.2020
Subjects
Cu/Cu2O
Hierarchical structure
In suit growth
Iodide adsorption
Layered double hydroxide
Cu/Cu2O
In suit growth
Layered double hydroxide
Iodide adsorption
Hierarchical structure
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Abstract To further improve the removal ability of layered double hydroxide (LDH) for iodide (I−) anions from wastewater, we prepared hierarchically porous Cu5Mg10Al5-LDH and used as a matrix for in suit growth of Cu/Cu2O on its surface, forming Cu/Cu2O-LDH, which was characterized and applied as an adsorbent. Results displayed high I− saturation uptake capability (137.8 mg/g) of Cu/Cu2O-LDH compared with Cu5Mg10Al5-LDH (26.4 mg/g) even thermal activated LDH (76.1 mg/g). Thermodynamic analysis showed that the reaction between I− anions and Cu/Cu2O-LDH is a spontaneous and exothermic. Uptake kinetics analysis exhibited that adsorption equilibrium can be reached after 265 min. Additionally, the adsorbent showed satisfactory selectivity in the presence of competitive anions (e.g., SO42−), and could achieve good adsorption performance in a wide pH range of 3–8. A cooperative adsorption mechanism was proposed on the basis of the following two aspects: (1) ion exchange between iodide and interlayer anions; (2) the adsorption performance of Cu, Cu(II) and Cu2O for I−. Meanwhile, the difference between the adsorption mechanism of Cu/Cu2O-LDH, Cu5Mg10Al5-LDH and Cu5Mg10Al5-CLDH adsorbents was also elaborated and verified. [Display omitted]
AbstractList To further improve the removal ability of layered double hydroxide (LDH) for iodide (I−) anions from wastewater, we prepared hierarchically porous Cu5Mg10Al5-LDH and used as a matrix for in suit growth of Cu/Cu2O on its surface, forming Cu/Cu2O-LDH, which was characterized and applied as an adsorbent. Results displayed high I− saturation uptake capability (137.8 mg/g) of Cu/Cu2O-LDH compared with Cu5Mg10Al5-LDH (26.4 mg/g) even thermal activated LDH (76.1 mg/g). Thermodynamic analysis showed that the reaction between I− anions and Cu/Cu2O-LDH is a spontaneous and exothermic. Uptake kinetics analysis exhibited that adsorption equilibrium can be reached after 265 min. Additionally, the adsorbent showed satisfactory selectivity in the presence of competitive anions (e.g., SO42−), and could achieve good adsorption performance in a wide pH range of 3–8. A cooperative adsorption mechanism was proposed on the basis of the following two aspects: (1) ion exchange between iodide and interlayer anions; (2) the adsorption performance of Cu, Cu(II) and Cu2O for I−. Meanwhile, the difference between the adsorption mechanism of Cu/Cu2O-LDH, Cu5Mg10Al5-LDH and Cu5Mg10Al5-CLDH adsorbents was also elaborated and verified. [Display omitted]
Author Jiao, Yan
Gao, Qianhong
Wang, Peng
Liu, Ying
Chen, Jiuyu
Wang, Junyi
Zhang, Xiaomei
Zhang, Zongxiang
Yang, Yi
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Keywords Cu/Cu2O
In suit growth
Layered double hydroxide
Iodide adsorption
Hierarchical structure
Language English
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Snippet To further improve the removal ability of layered double hydroxide (LDH) for iodide (I−) anions from wastewater, we prepared hierarchically porous...
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StartPage 338
SubjectTerms Cu/Cu2O
Hierarchical structure
In suit growth
Iodide adsorption
Layered double hydroxide
Title Enhanced removal of I− on hierarchically structured layered double hydroxides by in suit growth of Cu/Cu2O
URI https://dx.doi.org/10.1016/j.jes.2019.09.024
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