Enhanced removal of I− on hierarchically structured layered double hydroxides by in suit growth of Cu/Cu2O
To further improve the removal ability of layered double hydroxide (LDH) for iodide (I−) anions from wastewater, we prepared hierarchically porous Cu5Mg10Al5-LDH and used as a matrix for in suit growth of Cu/Cu2O on its surface, forming Cu/Cu2O-LDH, which was characterized and applied as an adsorben...
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Published in | Journal of environmental sciences (China) Vol. 88; pp. 338 - 348 |
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Main Authors | , , , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.02.2020
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Abstract | To further improve the removal ability of layered double hydroxide (LDH) for iodide (I−) anions from wastewater, we prepared hierarchically porous Cu5Mg10Al5-LDH and used as a matrix for in suit growth of Cu/Cu2O on its surface, forming Cu/Cu2O-LDH, which was characterized and applied as an adsorbent. Results displayed high I− saturation uptake capability (137.8 mg/g) of Cu/Cu2O-LDH compared with Cu5Mg10Al5-LDH (26.4 mg/g) even thermal activated LDH (76.1 mg/g). Thermodynamic analysis showed that the reaction between I− anions and Cu/Cu2O-LDH is a spontaneous and exothermic. Uptake kinetics analysis exhibited that adsorption equilibrium can be reached after 265 min. Additionally, the adsorbent showed satisfactory selectivity in the presence of competitive anions (e.g., SO42−), and could achieve good adsorption performance in a wide pH range of 3–8. A cooperative adsorption mechanism was proposed on the basis of the following two aspects: (1) ion exchange between iodide and interlayer anions; (2) the adsorption performance of Cu, Cu(II) and Cu2O for I−. Meanwhile, the difference between the adsorption mechanism of Cu/Cu2O-LDH, Cu5Mg10Al5-LDH and Cu5Mg10Al5-CLDH adsorbents was also elaborated and verified.
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AbstractList | To further improve the removal ability of layered double hydroxide (LDH) for iodide (I−) anions from wastewater, we prepared hierarchically porous Cu5Mg10Al5-LDH and used as a matrix for in suit growth of Cu/Cu2O on its surface, forming Cu/Cu2O-LDH, which was characterized and applied as an adsorbent. Results displayed high I− saturation uptake capability (137.8 mg/g) of Cu/Cu2O-LDH compared with Cu5Mg10Al5-LDH (26.4 mg/g) even thermal activated LDH (76.1 mg/g). Thermodynamic analysis showed that the reaction between I− anions and Cu/Cu2O-LDH is a spontaneous and exothermic. Uptake kinetics analysis exhibited that adsorption equilibrium can be reached after 265 min. Additionally, the adsorbent showed satisfactory selectivity in the presence of competitive anions (e.g., SO42−), and could achieve good adsorption performance in a wide pH range of 3–8. A cooperative adsorption mechanism was proposed on the basis of the following two aspects: (1) ion exchange between iodide and interlayer anions; (2) the adsorption performance of Cu, Cu(II) and Cu2O for I−. Meanwhile, the difference between the adsorption mechanism of Cu/Cu2O-LDH, Cu5Mg10Al5-LDH and Cu5Mg10Al5-CLDH adsorbents was also elaborated and verified.
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Author | Jiao, Yan Gao, Qianhong Wang, Peng Liu, Ying Chen, Jiuyu Wang, Junyi Zhang, Xiaomei Zhang, Zongxiang Yang, Yi |
Author_xml | – sequence: 1 givenname: Jiuyu surname: Chen fullname: Chen, Jiuyu organization: Jiangsu Key Laboratory of Chemical Pollution Control and Resources Reuse, School of Environmental and Biological Engineering, Nanjing University of Science and Technology, Nanjing 210094, China – sequence: 2 givenname: Junyi surname: Wang fullname: Wang, Junyi organization: Jiangsu Key Laboratory of Chemical Pollution Control and Resources Reuse, School of Environmental and Biological Engineering, Nanjing University of Science and Technology, Nanjing 210094, China – sequence: 3 givenname: Qianhong surname: Gao fullname: Gao, Qianhong organization: Jiangsu Key Laboratory of Chemical Pollution Control and Resources Reuse, School of Environmental and Biological Engineering, Nanjing University of Science and Technology, Nanjing 210094, China – sequence: 4 givenname: Xiaomei surname: Zhang fullname: Zhang, Xiaomei organization: Jiangsu Key Laboratory of Chemical Pollution Control and Resources Reuse, School of Environmental and Biological Engineering, Nanjing University of Science and Technology, Nanjing 210094, China – sequence: 5 givenname: Ying surname: Liu fullname: Liu, Ying organization: Jiangsu Key Laboratory of Chemical Pollution Control and Resources Reuse, School of Environmental and Biological Engineering, Nanjing University of Science and Technology, Nanjing 210094, China – sequence: 6 givenname: Peng surname: Wang fullname: Wang, Peng email: wp739130046@njust.edu.cn organization: Jiangsu Key Laboratory of Chemical Pollution Control and Resources Reuse, School of Environmental and Biological Engineering, Nanjing University of Science and Technology, Nanjing 210094, China – sequence: 7 givenname: Yan surname: Jiao fullname: Jiao, Yan organization: Collaborative Innovation Center of Atmospheric Environment and Equipment Technology, Jiangsu Key Laboratory of Atmospheric Environment Monitoring and Pollution Control (AEMPC), Nanjing University of Information Science & Technology, Nanjing 210044, China – sequence: 8 givenname: Zongxiang surname: Zhang fullname: Zhang, Zongxiang organization: Jiangsu Environmental Protection Key Laboratory of Monitoring for Organic Pollutants in Soil, Taizhou Environmental Monitoring Center, Taizhou 225300, China – sequence: 9 givenname: Yi surname: Yang fullname: Yang, Yi email: yangyi@njust.edu.cn organization: Jiangsu Key Laboratory of Chemical Pollution Control and Resources Reuse, School of Environmental and Biological Engineering, Nanjing University of Science and Technology, Nanjing 210094, China |
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Snippet | To further improve the removal ability of layered double hydroxide (LDH) for iodide (I−) anions from wastewater, we prepared hierarchically porous... |
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SubjectTerms | Cu/Cu2O Hierarchical structure In suit growth Iodide adsorption Layered double hydroxide |
Title | Enhanced removal of I− on hierarchically structured layered double hydroxides by in suit growth of Cu/Cu2O |
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