A new 3D composite of V2O5-based biodegradable ceramic material prepared by an environmentally friendly thermal method for supercapacitor applications
Major obstacles associated with aqueous supercapacitor materials such as slower rate capability and shorter cyclic lives are commonly found in pure V2O5 electrodes, limiting their extensive applications. This study demonstrates the preparation of a novel V2O5 composite grown on a biodegradable ceram...
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| Published in | Environmental technology & innovation Vol. 22; p. 101474 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.05.2021
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Major obstacles associated with aqueous supercapacitor materials such as slower rate capability and shorter cyclic lives are commonly found in pure V2O5 electrodes, limiting their extensive applications. This study demonstrates the preparation of a novel V2O5 composite grown on a biodegradable ceramic material of three-dimensional (3D) vanadium aluminum carbide (V2O5@V2AlC) with a convenient thermal oxidation process to reinforce its structural stability for improved electrochemical performance. The physicochemical properties of the composite were investigated using X-ray diffraction for phase analysis, scanning electron microscopy for surface morphology, energy dispersive X-ray for elemental composition, and Brunauer–Emmet–Teller analysis for specific surface area measurements. When investigated as supercapacitor electrodes in three different aqueous electrolytic media such as acidic (1 M H2SO4), neutral (0.5 M K2SO4), and alkaline (1 M KOH) solution, the composite exhibits enhanced electrochemical performance in the neutral solution. The maximum specific areal capacitance of 680 mF cm−2 at 5 mVs −1 and 740 mF cm−2 at 2 mA cm−2 was obtained and with improved cyclic stability. The enhanced capacitance properties and extended cyclic life along with the lower charge transfer resistance of the 3D-V2O5@V2AlC composite can be attributed to the strong mechanical properties of the material with an excellent capacitive contribution.
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•A novel composite of V2O5@V2AlC was prepared by simple thermal oxidation.•Surface morphology exhibits three-dimensional microflake-like structures.•Energy storage properties were investigated for aqueous supercapacitors.•Excellent performance was observed in a neutral electrolyte of 0.5 M K2SO4.•Superior capacitance was estimated to be 680 mF cm-2 at 5 mVs-1. |
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| AbstractList | Major obstacles associated with aqueous supercapacitor materials such as slower rate capability and shorter cyclic lives are commonly found in pure V₂O₅ electrodes, limiting their extensive applications. This study demonstrates the preparation of a novel V₂O₅ composite grown on a biodegradable ceramic material of three-dimensional (3D) vanadium aluminum carbide (V₂O₅@V₂AlC) with a convenient thermal oxidation process to reinforce its structural stability for improved electrochemical performance. The physicochemical properties of the composite were investigated using X-ray diffraction for phase analysis, scanning electron microscopy for surface morphology, energy dispersive X-ray for elemental composition, and Brunauer–Emmet–Teller analysis for specific surface area measurements. When investigated as supercapacitor electrodes in three different aqueous electrolytic media such as acidic (1 M H₂SO₄), neutral (0.5 M K₂SO₄), and alkaline (1 M KOH) solution, the composite exhibits enhanced electrochemical performance in the neutral solution. The maximum specific areal capacitance of 680 mF cm⁻² at 5 mVs ⁻¹ and 740 mF cm⁻² at 2 mA cm⁻² was obtained and with improved cyclic stability. The enhanced capacitance properties and extended cyclic life along with the lower charge transfer resistance of the 3D-V₂O₅@V₂AlC composite can be attributed to the strong mechanical properties of the material with an excellent capacitive contribution. Major obstacles associated with aqueous supercapacitor materials such as slower rate capability and shorter cyclic lives are commonly found in pure V2O5 electrodes, limiting their extensive applications. This study demonstrates the preparation of a novel V2O5 composite grown on a biodegradable ceramic material of three-dimensional (3D) vanadium aluminum carbide (V2O5@V2AlC) with a convenient thermal oxidation process to reinforce its structural stability for improved electrochemical performance. The physicochemical properties of the composite were investigated using X-ray diffraction for phase analysis, scanning electron microscopy for surface morphology, energy dispersive X-ray for elemental composition, and Brunauer–Emmet–Teller analysis for specific surface area measurements. When investigated as supercapacitor electrodes in three different aqueous electrolytic media such as acidic (1 M H2SO4), neutral (0.5 M K2SO4), and alkaline (1 M KOH) solution, the composite exhibits enhanced electrochemical performance in the neutral solution. The maximum specific areal capacitance of 680 mF cm−2 at 5 mVs −1 and 740 mF cm−2 at 2 mA cm−2 was obtained and with improved cyclic stability. The enhanced capacitance properties and extended cyclic life along with the lower charge transfer resistance of the 3D-V2O5@V2AlC composite can be attributed to the strong mechanical properties of the material with an excellent capacitive contribution. [Display omitted] •A novel composite of V2O5@V2AlC was prepared by simple thermal oxidation.•Surface morphology exhibits three-dimensional microflake-like structures.•Energy storage properties were investigated for aqueous supercapacitors.•Excellent performance was observed in a neutral electrolyte of 0.5 M K2SO4.•Superior capacitance was estimated to be 680 mF cm-2 at 5 mVs-1. |
| ArticleNumber | 101474 |
| Author | Venkatkarthick, Radhakrishnan Qin, Jiaqian |
| Author_xml | – sequence: 1 givenname: Radhakrishnan surname: Venkatkarthick fullname: Venkatkarthick, Radhakrishnan email: radhakrishnan.v@chula.ac.th – sequence: 2 givenname: Jiaqian surname: Qin fullname: Qin, Jiaqian email: jiaqian.q@chula.ac.th |
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Mater. Chem. A doi: 10.1039/C3TA15391F |
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| Snippet | Major obstacles associated with aqueous supercapacitor materials such as slower rate capability and shorter cyclic lives are commonly found in pure V2O5... Major obstacles associated with aqueous supercapacitor materials such as slower rate capability and shorter cyclic lives are commonly found in pure V₂O₅... |
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| SubjectTerms | aluminum biodegradability capacitance ceramics Composite electrochemical capacitors electrochemistry Electrode elemental composition energy-dispersive X-ray analysis environmental technology oxidation Supercapacitor surface area Thermal oxidation V2O5@V2AlC vanadium X-ray diffraction |
| Title | A new 3D composite of V2O5-based biodegradable ceramic material prepared by an environmentally friendly thermal method for supercapacitor applications |
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