Metal-organic framework derived magnetic nanoporous carbon as an adsorbent for the magnetic solid-phase extraction of chlorophenols from mushroom sample
In this work, a metal-organic framework derived nanoporous carbon （MOF-5-C） was fabricated and modified with Fe3O4 magnetic nanoparticles. The resulting magnetic MOF-5-derived porous carbon （Fe304@MOF-5-C） was then used for the magnetic solid-phase extraction of chlorophenols （CPs） from mushroom sam...
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| Published in | Chinese chemical letters Vol. 27; no. 5; pp. 783 - 788 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.05.2016
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| Abstract | In this work, a metal-organic framework derived nanoporous carbon （MOF-5-C） was fabricated and modified with Fe3O4 magnetic nanoparticles. The resulting magnetic MOF-5-derived porous carbon （Fe304@MOF-5-C） was then used for the magnetic solid-phase extraction of chlorophenols （CPs） from mushroom samples prior to high performance liquid chromatography-ultraviolet detection. Scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and N2 adsorption were used to characterize the adsorbent. After experimental optimization, the amount of the adsorbent was chosen as 8.0 mg, extraction time as 10 min, sample volume as 50 mL, desorption solvent as 0.4 mL （0.2 mL × 2） of alkaline methanol, and sample pH as 6. Under the above optimized conditions, good linearity for the analytes was obtained in the range of 0.8-100.0 ng g 1 with the correlation coefficients between 0.9923 and 0.9963. The limits of detection （SIN= 3） were in the range of 0.25-0.30 ng g-1, and the relative standard deviations were below 6.8%. The result showed that the Fe304@MOF-5-C has an excellent adsorption capacity for the analytes. |
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| AbstractList | A magnetic nanoporous carbon Fe3O4@MOF-5-C was prepared as the MSPE adsorbent for the extraction of some chlorophenols from mushroom samples.
In this work, a metal-organic framework derived nanoporous carbon (MOF-5-C) was fabricated and modified with Fe3O4 magnetic nanoparticles. The resulting magnetic MOF-5-derived porous carbon (Fe3O4@MOF-5-C) was then used for the magnetic solid-phase extraction of chlorophenols (CPs) from mushroom samples prior to high performance liquid chromatography–ultraviolet detection. Scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and N2 adsorption were used to characterize the adsorbent. After experimental optimization, the amount of the adsorbent was chosen as 8.0mg, extraction time as 10min, sample volume as 50mL, desorption solvent as 0.4mL (0.2mL×2) of alkaline methanol, and sample pH as 6. Under the above optimized conditions, good linearity for the analytes was obtained in the range of 0.8–100.0ngg−1 with the correlation coefficients between 0.9923 and 0.9963. The limits of detection (S/N=3) were in the range of 0.25–0.30ngg−1, and the relative standard deviations were below 6.8%. The result showed that the Fe3O4@MOF-5-C has an excellent adsorption capacity for the analytes. In this work, a metal-organic framework derived nanoporous carbon （MOF-5-C） was fabricated and modified with Fe3O4 magnetic nanoparticles. The resulting magnetic MOF-5-derived porous carbon （Fe304@MOF-5-C） was then used for the magnetic solid-phase extraction of chlorophenols （CPs） from mushroom samples prior to high performance liquid chromatography-ultraviolet detection. Scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and N2 adsorption were used to characterize the adsorbent. After experimental optimization, the amount of the adsorbent was chosen as 8.0 mg, extraction time as 10 min, sample volume as 50 mL, desorption solvent as 0.4 mL （0.2 mL × 2） of alkaline methanol, and sample pH as 6. Under the above optimized conditions, good linearity for the analytes was obtained in the range of 0.8-100.0 ng g 1 with the correlation coefficients between 0.9923 and 0.9963. The limits of detection （SIN= 3） were in the range of 0.25-0.30 ng g-1, and the relative standard deviations were below 6.8%. The result showed that the Fe304@MOF-5-C has an excellent adsorption capacity for the analytes. |
| Author | Lin Hao Xing-Li Liu Jun-Tao Wang Chun Wang Qiu-Hua Wu Zhi Wang |
| AuthorAffiliation | Department of Chemistry, College of Science, Agricultural University of Hebei, Baoding 071001, China |
| Author_xml | – sequence: 1 givenname: Lin surname: Hao fullname: Hao, Lin – sequence: 2 givenname: Xing-Li surname: Liu fullname: Liu, Xing-Li – sequence: 3 givenname: Jun-Tao surname: Wang fullname: Wang, Jun-Tao – sequence: 4 givenname: Chun surname: Wang fullname: Wang, Chun – sequence: 5 givenname: Qiu-Hua surname: Wu fullname: Wu, Qiu-Hua – sequence: 6 givenname: Zhi surname: Wang fullname: Wang, Zhi email: zhiwang2013@aliyun.com, wangzhi@hebau.edu.cn |
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| Keywords | Chlorophenols Magnetic solid-phase extraction Metal-organic frameworks Magnetic nanoporous carbon High performance liquid chromatography Mushroom |
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| Notes | Metal-organic frameworks Magnetic nanoporous carbon Magnetic solid-phase extraction Chlorophenols High performance liquid chromatography Mushroom 11-2710 In this work, a metal-organic framework derived nanoporous carbon （MOF-5-C） was fabricated and modified with Fe3O4 magnetic nanoparticles. The resulting magnetic MOF-5-derived porous carbon （Fe304@MOF-5-C） was then used for the magnetic solid-phase extraction of chlorophenols （CPs） from mushroom samples prior to high performance liquid chromatography-ultraviolet detection. Scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and N2 adsorption were used to characterize the adsorbent. After experimental optimization, the amount of the adsorbent was chosen as 8.0 mg, extraction time as 10 min, sample volume as 50 mL, desorption solvent as 0.4 mL （0.2 mL × 2） of alkaline methanol, and sample pH as 6. Under the above optimized conditions, good linearity for the analytes was obtained in the range of 0.8-100.0 ng g 1 with the correlation coefficients between 0.9923 and 0.9963. The limits of detection （SIN= 3） were in the range of 0.25-0.30 ng g-1, and the relative standard deviations were below 6.8%. The result showed that the Fe304@MOF-5-C has an excellent adsorption capacity for the analytes. |
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| Snippet | In this work, a metal-organic framework derived nanoporous carbon （MOF-5-C） was fabricated and modified with Fe3O4 magnetic nanoparticles. The resulting... A magnetic nanoporous carbon Fe3O4@MOF-5-C was prepared as the MSPE adsorbent for the extraction of some chlorophenols from mushroom samples. In this work, a... |
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| SubjectTerms | Chlorophenols High performance liquid chromatography Magnetic nanoporous carbon Magnetic solid-phase extraction Metal-organic frameworks Mushroom 吸附剂 固相萃取 多孔碳 样品 氯酚 磁性纳米粒子 蘑菇 金属有机 |
| Title | Metal-organic framework derived magnetic nanoporous carbon as an adsorbent for the magnetic solid-phase extraction of chlorophenols from mushroom sample |
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