Fe/MCM-41 as a promising heterogeneous catalyst for ozonation of p-chlorobenzoic acid in aqueous solution

Mesoporous MCM-41 and Fe loaded MCM-41（Fe/MCM-41）,which were successfully prepared by a hydrothermal method and a dipping method respectively,were applied as heterogeneous catalysts for ozonation of p-chlorobenzoic acid（p-CBA） in aqueous solution.MCM-41 and Fe/MCM-41 were characterized by XRD,FT-IR...

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Published inChinese chemical letters Vol. 22; no. 6; pp. 683 - 686
Main Authors Huang, Rui Huan, Liu, Jie, Li, Lai Sheng, Zhang, Qiu Yun, Zeng, Li Xuan, Lu, Ping
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.06.2011
Subjects
Catalytic ozonation
CBA
Fe/MCM-41
MCM
p-Chlorobenzoic acid
TOC
TOC去除率
总有机碳
氯苯甲酸
水溶液
臭氧
非均相催化剂
Fe/MCM-41
TOC
Catalytic ozonation
p-Chlorobenzoic acid
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Abstract Mesoporous MCM-41 and Fe loaded MCM-41（Fe/MCM-41）,which were successfully prepared by a hydrothermal method and a dipping method respectively,were applied as heterogeneous catalysts for ozonation of p-chlorobenzoic acid（p-CBA） in aqueous solution.MCM-41 and Fe/MCM-41 were characterized by XRD,FT-IR and diffuse reflectance UV-vis（DR-UV-vis） techniques. The presence of either MCM-41 or Fe/MCM-41 improves p-CBA and total organic carbon（TOC） removal efficiency compared to ozonation alone.Under the experimental condition,TOC removal rate of Fe/MCM-41/O_3 process is over 63.5%at 60 min oxidation time,44.5%using MCM-41 as catalyst,only 37.7%with ozonation alone.The presence of tert-butanol（TBA） in the Fe/MCM-41/ O_3 process indicated that the oxidation mechanism of p-CBA occurs via OH in the liquid bulk.And Fe/MCM-41 is a promising catalyst.
AbstractList Mesoporous MCM-41 and Fe loaded MCM-41（Fe/MCM-41）,which were successfully prepared by a hydrothermal method and a dipping method respectively,were applied as heterogeneous catalysts for ozonation of p-chlorobenzoic acid（p-CBA） in aqueous solution.MCM-41 and Fe/MCM-41 were characterized by XRD,FT-IR and diffuse reflectance UV-vis（DR-UV-vis） techniques. The presence of either MCM-41 or Fe/MCM-41 improves p-CBA and total organic carbon（TOC） removal efficiency compared to ozonation alone.Under the experimental condition,TOC removal rate of Fe/MCM-41/O_3 process is over 63.5%at 60 min oxidation time,44.5%using MCM-41 as catalyst,only 37.7%with ozonation alone.The presence of tert-butanol（TBA） in the Fe/MCM-41/ O_3 process indicated that the oxidation mechanism of p-CBA occurs via OH in the liquid bulk.And Fe/MCM-41 is a promising catalyst.
Mesoporous MCM-41 and Fe loaded MCM-41 (Fe/MCM-41), which were successfully prepared by a hydrothermal method and a dipping method respectively, were applied as heterogeneous catalysts for ozonation of p-chlorobenzoic acid ( p-CBA) in aqueous solution. MCM-41 and Fe/MCM-41 were characterized by XRD, FT-IR and diffuse reflectance UV–vis (DR-UV–vis) techniques. The presence of either MCM-41 or Fe/MCM-41 improves p-CBA and total organic carbon (TOC) removal efficiency compared to ozonation alone. Under the experimental condition, TOC removal rate of Fe/MCM-41/O 3 process is over 63.5% at 60 min oxidation time, 44.5% using MCM-41 as catalyst, only 37.7% with ozonation alone. The presence of turt-butanol (TBA) in the Fe/MCM-41/O 3 process indicated that the oxidation mechanism of p-CBA occurs via OH in the liquid bulk. And Fe/MCM-41 is a promising catalyst.
Author Rui Huan Huang Jie Liu Lai Sheng Li Qiu Yun Zhang Li Xuan Zeng Ping Lu
AuthorAffiliation School of Chemistry ＆ Environment, South China Normal University, Guangzhou 510006, China
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Keywords Fe/MCM-41
TOC
Catalytic ozonation
p-Chlorobenzoic acid
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Notes Fe/MCM-41; Catalytic ozonation; p-Chlorobenzoic acid; TOC
Mesoporous MCM-41 and Fe loaded MCM-41（Fe/MCM-41）,which were successfully prepared by a hydrothermal method and a dipping method respectively,were applied as heterogeneous catalysts for ozonation of p-chlorobenzoic acid（p-CBA） in aqueous solution.MCM-41 and Fe/MCM-41 were characterized by XRD,FT-IR and diffuse reflectance UV-vis（DR-UV-vis） techniques. The presence of either MCM-41 or Fe/MCM-41 improves p-CBA and total organic carbon（TOC） removal efficiency compared to ozonation alone.Under the experimental condition,TOC removal rate of Fe/MCM-41/O_3 process is over 63.5%at 60 min oxidation time,44.5%using MCM-41 as catalyst,only 37.7%with ozonation alone.The presence of tert-butanol（TBA） in the Fe/MCM-41/ O_3 process indicated that the oxidation mechanism of p-CBA occurs via OH in the liquid bulk.And Fe/MCM-41 is a promising catalyst.
11-2710/O6
Rui Huan Huang,Jie Liu,Lai Sheng Li,Qiu Yun Zhang,Li Xuan Zeng,Ping Lu （School of Chemistry ＆ Environment,South China Normal University,Guangzhou 510006,China ）
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Snippet Mesoporous MCM-41 and Fe loaded MCM-41（Fe/MCM-41）,which were successfully prepared by a hydrothermal method and a dipping method respectively,were applied as...
Mesoporous MCM-41 and Fe loaded MCM-41 (Fe/MCM-41), which were successfully prepared by a hydrothermal method and a dipping method respectively, were applied...
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SubjectTerms Catalytic ozonation
CBA
Fe/MCM-41
MCM
p-Chlorobenzoic acid
TOC
TOC去除率
总有机碳
氯苯甲酸
水溶液
臭氧
非均相催化剂
Title Fe/MCM-41 as a promising heterogeneous catalyst for ozonation of p-chlorobenzoic acid in aqueous solution
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