Pressure-induced structural modifications of imogolite nanotubes and of their methylated analogues
Structural modifications of single-walled aluminosilicate clay nanotubes have been studied under hydrostatic pressure by in situ synchrotron X-ray scattering. Imogolite nanotubes (INT) of nominal composition (OH)3Al2O3SiOH, and methyl-modified imogolite nanotubes (m-INT), (OH)3Al2O3SiCH3, have hydro...
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| Published in | Applied clay science Vol. 254; p. 107372 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
15.06.2024
Elsevier |
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| Abstract | Structural modifications of single-walled aluminosilicate clay nanotubes have been studied under hydrostatic pressure by in situ synchrotron X-ray scattering. Imogolite nanotubes (INT) of nominal composition (OH)3Al2O3SiOH, and methyl-modified imogolite nanotubes (m-INT), (OH)3Al2O3SiCH3, have hydrophilic and hydrophobic internal cavities, respectively. Nanotube chiralities also differ, with zigzag (INT) and armchair (m-INT) chirality. In this work, pressure-induced changes in nanotube morphology and atomic structure are studied as a function of chirality, affinity of the inner cavity, and the pressure-transmitting medium used. Radial deformation and collapse of nanotubes are evidenced below 3 GPa, followed by the formation of a lamellar phase at higher pressures. In the case of INT, the collapse pressure value depends on the pressure transmitting medium chosen. Axial compressibility is measured, and a pseudo Young's modulus Y is determined to be equal to ∼265 GPa for INT and below 80 GPa for m-INT, underpinning the role of nanotube chirality in mechanical properties.
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•Aluminosilicate imogolite nanotubes collapse radially at Pc≤3 GPa..•Strong structural modification occurs at high pressures which is reminiscent of a lamellar phase.•A pseudo Young's modulus is determined for imogolite nanotube and its methylated analogue.•Axial compressibility strongly depends on nanotube chirality. |
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| AbstractList | Structural modifications of single-walled aluminosilicate clay nanotubes have been studied under hydrostatic pressure by in situ synchrotron X-ray scattering. Imogolite nanotubes (INT) of nominal composition (OH)$_3$Al$_2$O$_3$SiOH, and methyl-modified imogolite nanotubes (m-INT), (OH)$_3$Al$_2$O$_3$SiCH$_3$, have hydrophilic and hydrophobic internal cavities, respectively. Nanotube chiralities also differ, with zigzag (INT) and armchair (m-INT) chirality. In this work, pressure-induced changes in nanotube morphology and atomic structure are studied as a function of chirality, affinity of the inner cavity, and the pressure-transmitting medium used. Radial deformation and collapse of nanotubes are evidenced below 3 GPa, followed by the formation of a lamellar phase at higher pressures. In the case of INT, the collapse pressure value depends on the pressure transmitting medium chosen. Axial compressibility is measured, and a pseudo Young's modulus Y is determined to be equal to ∼265 GPa for INT and below 80 GPa for m-INT, underpinning the role of nanotube chirality in mechanical properties. Structural modifications of single-walled aluminosilicate clay nanotubes have been studied under hydrostatic pressure by in situ synchrotron X-ray scattering. Imogolite nanotubes (INT) of nominal composition (OH)3Al2O3SiOH, and methyl-modified imogolite nanotubes (m-INT), (OH)3Al2O3SiCH3, have hydrophilic and hydrophobic internal cavities, respectively. Nanotube chiralities also differ, with zigzag (INT) and armchair (m-INT) chirality. In this work, pressure-induced changes in nanotube morphology and atomic structure are studied as a function of chirality, affinity of the inner cavity, and the pressure-transmitting medium used. Radial deformation and collapse of nanotubes are evidenced below 3 GPa, followed by the formation of a lamellar phase at higher pressures. In the case of INT, the collapse pressure value depends on the pressure transmitting medium chosen. Axial compressibility is measured, and a pseudo Young's modulus Y is determined to be equal to ∼265 GPa for INT and below 80 GPa for m-INT, underpinning the role of nanotube chirality in mechanical properties. [Display omitted] •Aluminosilicate imogolite nanotubes collapse radially at Pc≤3 GPa..•Strong structural modification occurs at high pressures which is reminiscent of a lamellar phase.•A pseudo Young's modulus is determined for imogolite nanotube and its methylated analogue.•Axial compressibility strongly depends on nanotube chirality. |
| ArticleNumber | 107372 |
| Author | Rouzière, Stéphan Launois, Pascale Balédent, Victor Elkaim, Erik Paineau, Erwan Bodin, Jennifer |
| Author_xml | – sequence: 1 givenname: Stéphan surname: Rouzière fullname: Rouzière, Stéphan email: stephan.rouziere@universite-paris-saclay.fr organization: Université Paris Saclay, CNRS, Laboratoire de Physique des Solides, 1 rue Nicolas Appert, Orsay 91405, France – sequence: 2 givenname: Victor surname: Balédent fullname: Balédent, Victor email: victor.baledent@universite-paris-saclay.fr organization: Université Paris Saclay, CNRS, Laboratoire de Physique des Solides, 1 rue Nicolas Appert, Orsay 91405, France – sequence: 3 givenname: Jennifer surname: Bodin fullname: Bodin, Jennifer organization: Université Paris Saclay, CNRS, Laboratoire de Physique des Solides, 1 rue Nicolas Appert, Orsay 91405, France – sequence: 4 givenname: Erik surname: Elkaim fullname: Elkaim, Erik organization: Synchrotron SOLEIL, L'Orme des Merisiers, Saint-Aubin 91190, France – sequence: 5 givenname: Erwan surname: Paineau fullname: Paineau, Erwan organization: Université Paris Saclay, CNRS, Laboratoire de Physique des Solides, 1 rue Nicolas Appert, Orsay 91405, France – sequence: 6 givenname: Pascale surname: Launois fullname: Launois, Pascale organization: Université Paris Saclay, CNRS, Laboratoire de Physique des Solides, 1 rue Nicolas Appert, Orsay 91405, France |
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| Keywords | Imogolite Young's modulus X-ray scattering Structure Pressure Nanotubes |
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