Pressure-induced structural modifications of imogolite nanotubes and of their methylated analogues

Structural modifications of single-walled aluminosilicate clay nanotubes have been studied under hydrostatic pressure by in situ synchrotron X-ray scattering. Imogolite nanotubes (INT) of nominal composition (OH)3Al2O3SiOH, and methyl-modified imogolite nanotubes (m-INT), (OH)3Al2O3SiCH3, have hydro...

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Published inApplied clay science Vol. 254; p. 107372
Main Authors Rouzière, Stéphan, Balédent, Victor, Bodin, Jennifer, Elkaim, Erik, Paineau, Erwan, Launois, Pascale
Format Journal Article
LanguageEnglish
Published Elsevier B.V 15.06.2024
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Abstract Structural modifications of single-walled aluminosilicate clay nanotubes have been studied under hydrostatic pressure by in situ synchrotron X-ray scattering. Imogolite nanotubes (INT) of nominal composition (OH)3Al2O3SiOH, and methyl-modified imogolite nanotubes (m-INT), (OH)3Al2O3SiCH3, have hydrophilic and hydrophobic internal cavities, respectively. Nanotube chiralities also differ, with zigzag (INT) and armchair (m-INT) chirality. In this work, pressure-induced changes in nanotube morphology and atomic structure are studied as a function of chirality, affinity of the inner cavity, and the pressure-transmitting medium used. Radial deformation and collapse of nanotubes are evidenced below 3 GPa, followed by the formation of a lamellar phase at higher pressures. In the case of INT, the collapse pressure value depends on the pressure transmitting medium chosen. Axial compressibility is measured, and a pseudo Young's modulus Y is determined to be equal to ∼265 GPa for INT and below 80 GPa for m-INT, underpinning the role of nanotube chirality in mechanical properties. [Display omitted] •Aluminosilicate imogolite nanotubes collapse radially at Pc≤3 GPa..•Strong structural modification occurs at high pressures which is reminiscent of a lamellar phase.•A pseudo Young's modulus is determined for imogolite nanotube and its methylated analogue.•Axial compressibility strongly depends on nanotube chirality.
AbstractList Structural modifications of single-walled aluminosilicate clay nanotubes have been studied under hydrostatic pressure by in situ synchrotron X-ray scattering. Imogolite nanotubes (INT) of nominal composition (OH)$_3$Al$_2$O$_3$SiOH, and methyl-modified imogolite nanotubes (m-INT), (OH)$_3$Al$_2$O$_3$SiCH$_3$, have hydrophilic and hydrophobic internal cavities, respectively. Nanotube chiralities also differ, with zigzag (INT) and armchair (m-INT) chirality. In this work, pressure-induced changes in nanotube morphology and atomic structure are studied as a function of chirality, affinity of the inner cavity, and the pressure-transmitting medium used. Radial deformation and collapse of nanotubes are evidenced below 3 GPa, followed by the formation of a lamellar phase at higher pressures. In the case of INT, the collapse pressure value depends on the pressure transmitting medium chosen. Axial compressibility is measured, and a pseudo Young's modulus Y is determined to be equal to ∼265 GPa for INT and below 80 GPa for m-INT, underpinning the role of nanotube chirality in mechanical properties.
Structural modifications of single-walled aluminosilicate clay nanotubes have been studied under hydrostatic pressure by in situ synchrotron X-ray scattering. Imogolite nanotubes (INT) of nominal composition (OH)3Al2O3SiOH, and methyl-modified imogolite nanotubes (m-INT), (OH)3Al2O3SiCH3, have hydrophilic and hydrophobic internal cavities, respectively. Nanotube chiralities also differ, with zigzag (INT) and armchair (m-INT) chirality. In this work, pressure-induced changes in nanotube morphology and atomic structure are studied as a function of chirality, affinity of the inner cavity, and the pressure-transmitting medium used. Radial deformation and collapse of nanotubes are evidenced below 3 GPa, followed by the formation of a lamellar phase at higher pressures. In the case of INT, the collapse pressure value depends on the pressure transmitting medium chosen. Axial compressibility is measured, and a pseudo Young's modulus Y is determined to be equal to ∼265 GPa for INT and below 80 GPa for m-INT, underpinning the role of nanotube chirality in mechanical properties. [Display omitted] •Aluminosilicate imogolite nanotubes collapse radially at Pc≤3 GPa..•Strong structural modification occurs at high pressures which is reminiscent of a lamellar phase.•A pseudo Young's modulus is determined for imogolite nanotube and its methylated analogue.•Axial compressibility strongly depends on nanotube chirality.
ArticleNumber 107372
Author Rouzière, Stéphan
Launois, Pascale
Balédent, Victor
Elkaim, Erik
Paineau, Erwan
Bodin, Jennifer
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  givenname: Pascale
  surname: Launois
  fullname: Launois, Pascale
  organization: Université Paris Saclay, CNRS, Laboratoire de Physique des Solides, 1 rue Nicolas Appert, Orsay 91405, France
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Keywords Imogolite
Young's modulus
X-ray scattering
Structure
Pressure
Nanotubes
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Snippet Structural modifications of single-walled aluminosilicate clay nanotubes have been studied under hydrostatic pressure by in situ synchrotron X-ray scattering....
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elsevier
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StartPage 107372
SubjectTerms Condensed Matter
Imogolite
Materials Science
Nanotubes
Physics
Pressure
Structure
X-ray scattering
Young's modulus
Title Pressure-induced structural modifications of imogolite nanotubes and of their methylated analogues
URI https://dx.doi.org/10.1016/j.clay.2024.107372
https://hal.science/hal-04564813
Volume 254
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