Template-directed synthesis of sulphur doped NiCoFe layered double hydroxide porous nanosheets with enhanced electrocatalytic activity for the oxygen evolution reaction
The development of readily available, highly efficient and stable electrocatalysts for the oxygen evolution reaction (OER) is extremely significant to facilitate water splitting for the generation of clean hydrogen energy. Layered double hydroxides (LDHs) exhibit promising electrocatalytic performan...
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| Published in | Journal of materials chemistry. A, Materials for energy and sustainability Vol. 6; no. 7; pp. 3224 - 3230 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cambridge
Royal Society of Chemistry
2018
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The development of readily available, highly efficient and stable electrocatalysts for the oxygen evolution reaction (OER) is extremely significant to facilitate water splitting for the generation of clean hydrogen energy. Layered double hydroxides (LDHs) exhibit promising electrocatalytic performance for the OER. However, their electrical conductivity and active sites should be increased for the preparation of more effective OER electrocatalysts based on LDHs for large-scale applications. Herein, we demonstrate a facile and practical pathway for the hierarchical fabrication of three-dimensional (3D) porous sulphur incorporated NiCoFe LDH nanosheets (S-NiCoFe LDH) on carbon cloth (CC). The as-obtained hierarchically structured S-NiCoFe LDH electrode shows superb electrocatalytic activity and stability for the OER, requiring overpotentials as low as 206 mV and 258 mV to achieve current densities of 10 mA cm
−2
and 100 mA cm
−2
in 1.0 M KOH solution, respectively, making S-NiCoFe LDH one of the most efficient low-cost electrocatalysts for the OER. The enhanced electrocatalytic performance is attributed to the unique 3D hierarchical nanostructure and sulphur doping, which endow the self-supported S-NiCoFe LDH electrode with abundant active sites and superb electrical conductivity. The strategy expands the possibilities for boosting the catalytic activity of LDH-based OER electrocatalysts. |
|---|---|
| AbstractList | The development of readily available, highly efficient and stable electrocatalysts for the oxygen evolution reaction (OER) is extremely significant to facilitate water splitting for the generation of clean hydrogen energy. Layered double hydroxides (LDHs) exhibit promising electrocatalytic performance for the OER. However, their electrical conductivity and active sites should be increased for the preparation of more effective OER electrocatalysts based on LDHs for large-scale applications. Herein, we demonstrate a facile and practical pathway for the hierarchical fabrication of three-dimensional (3D) porous sulphur incorporated NiCoFe LDH nanosheets (S-NiCoFe LDH) on carbon cloth (CC). The as-obtained hierarchically structured S-NiCoFe LDH electrode shows superb electrocatalytic activity and stability for the OER, requiring overpotentials as low as 206 mV and 258 mV to achieve current densities of 10 mA cm⁻² and 100 mA cm⁻² in 1.0 M KOH solution, respectively, making S-NiCoFe LDH one of the most efficient low-cost electrocatalysts for the OER. The enhanced electrocatalytic performance is attributed to the unique 3D hierarchical nanostructure and sulphur doping, which endow the self-supported S-NiCoFe LDH electrode with abundant active sites and superb electrical conductivity. The strategy expands the possibilities for boosting the catalytic activity of LDH-based OER electrocatalysts. The development of readily available, highly efficient and stable electrocatalysts for the oxygen evolution reaction (OER) is extremely significant to facilitate water splitting for the generation of clean hydrogen energy. Layered double hydroxides (LDHs) exhibit promising electrocatalytic performance for the OER. However, their electrical conductivity and active sites should be increased for the preparation of more effective OER electrocatalysts based on LDHs for large-scale applications. Herein, we demonstrate a facile and practical pathway for the hierarchical fabrication of three-dimensional (3D) porous sulphur incorporated NiCoFe LDH nanosheets (S-NiCoFe LDH) on carbon cloth (CC). The as-obtained hierarchically structured S-NiCoFe LDH electrode shows superb electrocatalytic activity and stability for the OER, requiring overpotentials as low as 206 mV and 258 mV to achieve current densities of 10 mA cm −2 and 100 mA cm −2 in 1.0 M KOH solution, respectively, making S-NiCoFe LDH one of the most efficient low-cost electrocatalysts for the OER. The enhanced electrocatalytic performance is attributed to the unique 3D hierarchical nanostructure and sulphur doping, which endow the self-supported S-NiCoFe LDH electrode with abundant active sites and superb electrical conductivity. The strategy expands the possibilities for boosting the catalytic activity of LDH-based OER electrocatalysts. The development of readily available, highly efficient and stable electrocatalysts for the oxygen evolution reaction (OER) is extremely significant to facilitate water splitting for the generation of clean hydrogen energy. Layered double hydroxides (LDHs) exhibit promising electrocatalytic performance for the OER. However, their electrical conductivity and active sites should be increased for the preparation of more effective OER electrocatalysts based on LDHs for large-scale applications. Herein, we demonstrate a facile and practical pathway for the hierarchical fabrication of three-dimensional (3D) porous sulphur incorporated NiCoFe LDH nanosheets (S-NiCoFe LDH) on carbon cloth (CC). The as-obtained hierarchically structured S-NiCoFe LDH electrode shows superb electrocatalytic activity and stability for the OER, requiring overpotentials as low as 206 mV and 258 mV to achieve current densities of 10 mA cm−2 and 100 mA cm−2 in 1.0 M KOH solution, respectively, making S-NiCoFe LDH one of the most efficient low-cost electrocatalysts for the OER. The enhanced electrocatalytic performance is attributed to the unique 3D hierarchical nanostructure and sulphur doping, which endow the self-supported S-NiCoFe LDH electrode with abundant active sites and superb electrical conductivity. The strategy expands the possibilities for boosting the catalytic activity of LDH-based OER electrocatalysts. |
| Author | Cao, Li-Ming Wang, Jia-Wei Lu, Tong-Bu Zhong, Di-Chang |
| Author_xml | – sequence: 1 givenname: Li-Ming surname: Cao fullname: Cao, Li-Ming organization: MOE Key Laboratory of Bioinorganic and Synthetic Chemistry, School of Chemistry, Sun Yat-Sen University, Guangzhou 510275, China – sequence: 2 givenname: Jia-Wei orcidid: 0000-0003-1966-7131 surname: Wang fullname: Wang, Jia-Wei organization: MOE Key Laboratory of Bioinorganic and Synthetic Chemistry, School of Chemistry, Sun Yat-Sen University, Guangzhou 510275, China – sequence: 3 givenname: Di-Chang orcidid: 0000-0002-5504-249X surname: Zhong fullname: Zhong, Di-Chang organization: Institute for New Energy Materials & Low Carbon Technologies, School of Materials Science & Engineering, Tianjin University of Technology, Tianjin 300384, China – sequence: 4 givenname: Tong-Bu orcidid: 0000-0002-6087-4880 surname: Lu fullname: Lu, Tong-Bu organization: MOE Key Laboratory of Bioinorganic and Synthetic Chemistry, School of Chemistry, Sun Yat-Sen University, Guangzhou 510275, China |
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| SubjectTerms | active sites carbon Catalysis Catalytic activity Clean energy Cloth Electrical conductivity Electrical resistivity Electrocatalysts Electrodes energy Fabrication hydrogen Hydrogen-based energy Hydroxides Nanosheets Nanostructure Oxygen Oxygen evolution reactions oxygen production potassium hydroxide Sulfur Water splitting |
| Title | Template-directed synthesis of sulphur doped NiCoFe layered double hydroxide porous nanosheets with enhanced electrocatalytic activity for the oxygen evolution reaction |
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