Gradient nanostructure evolution and phase transformation of α phase in Ti-6Al-4V alloy induced by ultrasonic surface rolling process

The gradient nanostructure evolution and the mechanism governing this evolution of α phase in Ti-6Al-4V alloy induced by ultrasonic surface rolling process were investigated. A gradient nanostructure consisting of a roughly equiaxed nanograin layer, an elongated nano-lamellar layer, an elongated ult...

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Published inMaterials science & engineering. A, Structural materials : properties, microstructure and processing Vol. 742; pp. 820 - 834
Main Authors Ao, Ni, Liu, Daoxin, Xu, Xingchen, Zhang, Xiaohua, Liu, Dan
Format Journal Article
LanguageEnglish
Published Lausanne Elsevier B.V 10.01.2019
Elsevier BV
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ISSN0921-5093
1873-4936
DOI10.1016/j.msea.2018.10.098

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Abstract The gradient nanostructure evolution and the mechanism governing this evolution of α phase in Ti-6Al-4V alloy induced by ultrasonic surface rolling process were investigated. A gradient nanostructure consisting of a roughly equiaxed nanograin layer, an elongated nano-lamellar layer, an elongated ultrafine lamellar layer, a refined grain layer, and a low-strain coarse-grained layer was formed with a thickness of more than 400 µm. The formation of gradient nanostructure of α phase was dominated by complex dislocation activities in hcp grains without twins occurring, supplemented by hexagonal close-packed (hcp) titanium (Ti) to face-centered cubic (fcc) Ti phase transformation. During the microstructural evolution, the coarse hcp-Ti grains were first elongated into lamellae. Then, these sub-micron lamellae were gradually transformed into roughly equiaxed nanograins via two deformation modes of longitudinal splitting and transverse breakdown, accompanied by dynamic recovery. The fcc-Ti grains were deformed mainly via twin-twin intersections and twin-dislocation interactions, accompanied by longitudinal splitting and transverse breakdown, resulted in refinement of the micron-scale fcc-Ti grains to roughly equiaxed nanograins. The interaction of hcp and fcc phases influenced and synergistically promoted the microstructural evolution process. In addition, the microhardness improvement in the surface layer of Ti-6Al-4V alloy was attributed to the increase of dislocation density, grain refinement and the occurrence of deformation twinning in fcc-Ti grains.
AbstractList The gradient nanostructure evolution and the mechanism governing this evolution of α phase in Ti-6Al-4V alloy induced by ultrasonic surface rolling process were investigated. A gradient nanostructure consisting of a roughly equiaxed nanograin layer, an elongated nano-lamellar layer, an elongated ultrafine lamellar layer, a refined grain layer, and a low-strain coarse-grained layer was formed with a thickness of more than 400 µm. The formation of gradient nanostructure of α phase was dominated by complex dislocation activities in hcp grains without twins occurring, supplemented by hexagonal close-packed (hcp) titanium (Ti) to face-centered cubic (fcc) Ti phase transformation. During the microstructural evolution, the coarse hcp-Ti grains were first elongated into lamellae. Then, these sub-micron lamellae were gradually transformed into roughly equiaxed nanograins via two deformation modes of longitudinal splitting and transverse breakdown, accompanied by dynamic recovery. The fcc-Ti grains were deformed mainly via twin-twin intersections and twin-dislocation interactions, accompanied by longitudinal splitting and transverse breakdown, resulted in refinement of the micron-scale fcc-Ti grains to roughly equiaxed nanograins. The interaction of hcp and fcc phases influenced and synergistically promoted the microstructural evolution process. In addition, the microhardness improvement in the surface layer of Ti-6Al-4V alloy was attributed to the increase of dislocation density, grain refinement and the occurrence of deformation twinning in fcc-Ti grains.
The gradient nanostructure evolution and the mechanism governing this evolution of α phase in Ti-6Al-4V alloy induced by ultrasonic surface rolling process were investigated. A gradient nanostructure consisting of a roughly equiaxed nanograin layer, an elongated nano-lamellar layer, an elongated ultrafine lamellar layer, a refined grain layer, and a low-strain coarse-grained layer was formed with a thickness of more than 400 µm. The formation of gradient nanostructure of α phase was dominated by complex dislocation activities in hcp grains without twins occurring, supplemented by hexagonal close-packed (hcp) titanium (Ti) to face-centered cubic (fcc) Ti phase transformation. During the microstructural evolution, the coarse hcp-Ti grains were first elongated into lamellae. Then, these sub-micron lamellae were gradually transformed into roughly equiaxed nanograins via two deformation modes of longitudinal splitting and transverse breakdown, accompanied by dynamic recovery. The fcc-Ti grains were deformed mainly via twin-twin intersections and twin-dislocation interactions, accompanied by longitudinal splitting and transverse breakdown, resulted in refinement of the micron-scale fcc-Ti grains to roughly equiaxed nanograins. The interaction of hcp and fcc phases influenced and synergistically promoted the microstructural evolution process. In addition, the microhardness improvement in the surface layer of Ti-6Al-4V alloy was attributed to the increase of dislocation density, grain refinement and the occurrence of deformation twinning in fcc-Ti grains.
Author Xu, Xingchen
Liu, Daoxin
Zhang, Xiaohua
Ao, Ni
Liu, Dan
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  givenname: Dan
  surname: Liu
  fullname: Liu, Dan
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Keywords Face-centered cubic titanium
Phase transformation
Ultrasonic surface rolling process
Gradient nanostructure evolution
Ti-6Al-4V alloy
Deformation twins
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Snippet The gradient nanostructure evolution and the mechanism governing this evolution of α phase in Ti-6Al-4V alloy induced by ultrasonic surface rolling process...
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SubjectTerms Breakdown
Deformation mechanisms
Deformation twins
Dislocation density
Elongation
Equiaxed structure
Evolution
Face-centered cubic titanium
Gradient nanostructure evolution
Grain refinement
Intersections
Microhardness
Nanostructure
Phase transformation
Phase transitions
Skin pass rolling
Splitting
Surface layers
Ti-6Al-4V alloy
Titanium base alloys
Twinning
Ultrafines
Ultrasonic surface rolling process
Title Gradient nanostructure evolution and phase transformation of α phase in Ti-6Al-4V alloy induced by ultrasonic surface rolling process
URI https://dx.doi.org/10.1016/j.msea.2018.10.098
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