The Synthesis and Properties of Asymmetrically Substituted 4,4'-Bis(1,3,5-triazine-6-yl)diaminostilbene-2,2'-disulfonic Acid Derivatives as Fluorescent Brighteners [II]
In this work, the key intermediate, 4-amino-4'-(2-amino-4-anilino-1,3,5-triazine-6-yl)-aminostilbene-2,2'-disulfonic acid, was prepared from 4-(2-amino-4-anilino-1,3,5-triazine-6-yl)amino-4'-nitrostilbene-2,2'-disulfonate by using Tin(II) chloride as the reducing agent. Using thi...
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| Published in | Bulletin of the Korean Chemical Society Vol. 34; no. 7; pp. 2131 - 2137 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
대한화학회
20.07.2013
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0253-2964 1229-5949 |
| DOI | 10.5012/bkcs.2013.34.7.2131 |
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| Abstract | In this work, the key intermediate, 4-amino-4'-(2-amino-4-anilino-1,3,5-triazine-6-yl)-aminostilbene-2,2'-disulfonic acid, was prepared from 4-(2-amino-4-anilino-1,3,5-triazine-6-yl)amino-4'-nitrostilbene-2,2'-disulfonate by using Tin(II) chloride as the reducing agent. Using this intermediate, nineteen new asymmetrically substituted bistriazinylstilbene fluorescent brightening agents were synthesized. Chemical structures of the obtained compounds 5a-s were analyzed by proton NMR spectrum. The physical properties of the new compounds 5a-s were characterized by fastness test and whiteness measurement test and the obtained data were compared to measurements obtained from CI 86. KCI Citation Count: 2 |
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| AbstractList | In this work, the key intermediate, 4-amino-4'-(2-amino-4-anilino-1,3,5-triazine-6-yl)-aminostilbene-2,2'-disulfonic acid, was prepared from 4-(2-amino-4-anilino-1,3,5-triazine-6-yl)amino-4'-nitrostilbene-2,2'-disulfonate by using Tin(II) chloride as the reducing agent. Using this intermediate, nineteen new asymmetrically substituted bistriazinylstilbene fluorescent brightening agents were synthesized. Chemical structures of the obtained compounds 5a-s were analyzed by proton NMR spectrum. The physical properties of the new compounds 5a-s were characterized by fastness test and whiteness measurement test and the obtained data were compared to measurements obtained from CI 86. KCI Citation Count: 2 |
| Author | Jung, Jongkeun Kang, Yonghan |
| Author_xml | – sequence: 1 givenname: Jongkeun surname: Jung fullname: Jung, Jongkeun – sequence: 2 givenname: Yonghan surname: Kang fullname: Kang, Yonghan |
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| References_xml | – volume: 106 start-page: 49 year: 1990 ident: JCGMCS_2013_v34n7_2131_002 publication-title: Journal of the Society of Dyes and Colourists doi: 10.1111/j.1478-4408.1990.tb01241.x – volume: 43 start-page: 197 year: 1999 ident: JCGMCS_2013_v34n7_2131_006 publication-title: Dyes and Pigments doi: 10.1016/S0143-7208(99)00061-3 – volume: 64 start-page: 25 year: 2005 ident: JCGMCS_2013_v34n7_2131_008 publication-title: J. Dyes and Pigments doi: 10.1016/j.dyepig.2004.03.016 – volume: 44 start-page: 175 year: 2000 ident: JCGMCS_2013_v34n7_2131_001 publication-title: Dyes and Pigments doi: 10.1016/S0143-7208(99)00088-1 – volume: 29 start-page: 155 year: 1995 ident: JCGMCS_2013_v34n7_2131_005 publication-title: Dyes and Pigments doi: 10.1016/0143-7208(95)00040-M – volume: 27 start-page: 195 year: 1974 ident: JCGMCS_2013_v34n7_2131_003 publication-title: Australian Journal of Chemistry doi: 10.1071/CH9740195 – volume: 65 start-page: 679 year: 1968 ident: JCGMCS_2013_v34n7_2131_007 publication-title: Journal of the American Oil Chemists Society |
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| Title | The Synthesis and Properties of Asymmetrically Substituted 4,4'-Bis(1,3,5-triazine-6-yl)diaminostilbene-2,2'-disulfonic Acid Derivatives as Fluorescent Brighteners [II] |
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