Fluorescent Properties of three Zinc(II) Coordination Polymers derived from Flexible N-(4/3-Carboxyphenyl)iminodiacetic Acids
Three polymers [Zn2(p‐CPIDA)(OH)]n (1), [Zn2(p‐HCPIDA)2(bipy)(H2O)4]·2H2O (2), and [Zn(m‐HCPIDA)(bipy)]n (3) [p/m‐H3CPIDA = N‐(4/3‐carboxyphenyl) iminodiacetic acid, bipy = 4, 4′‐bipyridine] were hydrothermally synthesized and characterized by single‐crystal X‐ray diffraction, X‐ray powder diffracti...
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| Published in | Zeitschrift für anorganische und allgemeine Chemie (1950) Vol. 638; no. 3-4; pp. 641 - 647 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Weinheim
WILEY-VCH Verlag
01.03.2012
WILEY‐VCH Verlag |
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| Abstract | Three polymers [Zn2(p‐CPIDA)(OH)]n (1), [Zn2(p‐HCPIDA)2(bipy)(H2O)4]·2H2O (2), and [Zn(m‐HCPIDA)(bipy)]n (3) [p/m‐H3CPIDA = N‐(4/3‐carboxyphenyl) iminodiacetic acid, bipy = 4, 4′‐bipyridine] were hydrothermally synthesized and characterized by single‐crystal X‐ray diffraction, X‐ray powder diffraction patterns (XPRD), FTIR spectroscopy, and fluorescence analyses. Compound 1 displays an interesting three‐dimensional framework consisting of novel paddle wheel Zn8O10C2 units, which are further linked by p‐CPIDA3– ligands with versatile coordination modes. In 2, the structural motifs formed by terminal p‐HCPIDA2– ligands and ZnII ions are bridged by ancillary bipy to give a zero‐dimensional Z‐shaped dimer. Compound 3 has an infinite zigzag chain linked by bipy, in which terminal m‐HCPIDA2– ligands alternately run along the chain like flags. Compounds 2 and 3 are further connected by hydrogen bonding and π···π stacking interactions to result in 3D supramolecular frameworks. Moreover, compounds 1–3 exhibit intense solid state fluorescent emissions at room temperature. |
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| AbstractList | Three polymers [Zn2(p‐CPIDA)(OH)]n (1), [Zn2(p‐HCPIDA)2(bipy)(H2O)4]·2H2O (2), and [Zn(m‐HCPIDA)(bipy)]n (3) [p/m‐H3CPIDA = N‐(4/3‐carboxyphenyl) iminodiacetic acid, bipy = 4, 4′‐bipyridine] were hydrothermally synthesized and characterized by single‐crystal X‐ray diffraction, X‐ray powder diffraction patterns (XPRD), FTIR spectroscopy, and fluorescence analyses. Compound 1 displays an interesting three‐dimensional framework consisting of novel paddle wheel Zn8O10C2 units, which are further linked by p‐CPIDA3– ligands with versatile coordination modes. In 2, the structural motifs formed by terminal p‐HCPIDA2– ligands and ZnII ions are bridged by ancillary bipy to give a zero‐dimensional Z‐shaped dimer. Compound 3 has an infinite zigzag chain linked by bipy, in which terminal m‐HCPIDA2– ligands alternately run along the chain like flags. Compounds 2 and 3 are further connected by hydrogen bonding and π···π stacking interactions to result in 3D supramolecular frameworks. Moreover, compounds 1–3 exhibit intense solid state fluorescent emissions at room temperature. Abstract Three polymers [Zn 2 ( p ‐CPIDA)(OH)] n ( 1 ), [Zn 2 ( p ‐HCPIDA) 2 (bipy)(H 2 O) 4 ] · 2H 2 O ( 2 ), and [Zn( m ‐HCPIDA)(bipy)] n ( 3 ) [ p / m ‐H 3 CPIDA = N ‐(4/3‐carboxyphenyl) iminodiacetic acid, bipy = 4, 4′‐bipyridine] were hydrothermally synthesized and characterized by single‐crystal X‐ray diffraction, X‐ray powder diffraction patterns (XPRD), FTIR spectroscopy, and fluorescence analyses. Compound 1 displays an interesting three‐dimensional framework consisting of novel paddle wheel Zn 8 O 10 C 2 units, which are further linked by p ‐CPIDA 3– ligands with versatile coordination modes. In 2 , the structural motifs formed by terminal p ‐HCPIDA 2– ligands and Zn II ions are bridged by ancillary bipy to give a zero‐dimensional Z‐shaped dimer. Compound 3 has an infinite zigzag chain linked by bipy, in which terminal m ‐HCPIDA 2– ligands alternately run along the chain like flags. Compounds 2 and 3 are further connected by hydrogen bonding and π ··· π stacking interactions to result in 3D supramolecular frameworks. Moreover, compounds 1 – 3 exhibit intense solid state fluorescent emissions at room temperature. |
| Author | Liang, Yong-Ping Chen, Yi-Ping Zhang, Han-Hui Zhao, Yan-Fei Gong, Qiao-Juan Chai, Xiao-Chuan |
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| CitedBy_id | crossref_primary_10_1021_acsanm_9b01047 crossref_primary_10_1515_znb_2021_0014 crossref_primary_10_1016_j_polymer_2012_11_021 crossref_primary_10_1002_ejic_201402419 crossref_primary_10_1002_zaac_201200341 crossref_primary_10_1016_j_ica_2017_06_048 |
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| Snippet | Three polymers [Zn2(p‐CPIDA)(OH)]n (1), [Zn2(p‐HCPIDA)2(bipy)(H2O)4]·2H2O (2), and [Zn(m‐HCPIDA)(bipy)]n (3) [p/m‐H3CPIDA = N‐(4/3‐carboxyphenyl) iminodiacetic... Abstract Three polymers [Zn 2 ( p ‐CPIDA)(OH)] n ( 1 ), [Zn 2 ( p ‐HCPIDA) 2 (bipy)(H 2 O) 4 ] · 2H 2 O ( 2 ), and [Zn( m ‐HCPIDA)(bipy)] n ( 3 ) [ p / m ‐H 3... |
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| SubjectTerms | Coordination modes Fluorescence Multicarboxylate Topological analysis Zinc |
| Title | Fluorescent Properties of three Zinc(II) Coordination Polymers derived from Flexible N-(4/3-Carboxyphenyl)iminodiacetic Acids |
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