Electrodeposited Cobalt Hydroxide Thin Films: A Comprehensive Investigation from Synthesis to Advanced Electrochemical Behavior for High-Performance Energy Storage
The synthesis and characterization of cobalt hydroxides generated from cobalt chloride precursors at various concentrations (0.1 to 0.5 M) by using cathodic electrochemical deposition technique for prospective energy storage application. The Co(OH) 2 thin films were discovered to have a crystalline...
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| Published in | Transactions on electrical and electronic materials Vol. 25; no. 5; pp. 589 - 599 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Seoul
The Korean Institute of Electrical and Electronic Material Engineers (KIEEME)
01.10.2024
한국전기전자재료학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1229-7607 2092-7592 |
| DOI | 10.1007/s42341-024-00542-3 |
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| Abstract | The synthesis and characterization of cobalt hydroxides generated from cobalt chloride precursors at various concentrations (0.1 to 0.5 M) by using cathodic electrochemical deposition technique for prospective energy storage application. The Co(OH)
2
thin films were discovered to have a crystalline structure with a crystallite size of ~ 40 nanometers, particle size of 180 nm, and a leaf-like morphology via XRD (X-ray Diffraction) and SEM (Scanning Electron Microscopy) respectively. Further properties were investigated by EDS (Energy-Dispersive X-ray Spectroscopy), FTIR (Fourier Transform Infrared Spectroscopy), and UV Vis Spectra (Ultraviolet-Visible Spectroscopy) analysis. The presence of cobalt hydroxide was confirmed by EDS, verifying the purity of the substance. Electrochemical characteristics, such as CV (Cyclic Voltammetry), GCD (Galvanostatic Charge-Discharge), and EIS (Electrochemical Impedance Spectroscopy) analysis, indicated capacitive behavior, confirming their feasibility for energy storage. The specific capacitances from 450 to 1250 F/g were measured from the GCD curve. The MATLAB study gave quantitative data on critical electrode characteristics which improved the understanding of the performance and a framework for further investigation in the development of sustainable energy solutions.
Graphical Abstract |
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| AbstractList | The synthesis and characterization of cobalt hydroxides generated from cobalt chloride precursors at various concentrations (0.1 to 0.5 M) by using cathodic electrochemical deposition technique for prospective energy storage application. The Co(OH)
2
thin films were discovered to have a crystalline structure with a crystallite size of ~ 40 nanometers, particle size of 180 nm, and a leaf-like morphology via XRD (X-ray Diffraction) and SEM (Scanning Electron Microscopy) respectively. Further properties were investigated by EDS (Energy-Dispersive X-ray Spectroscopy), FTIR (Fourier Transform Infrared Spectroscopy), and UV Vis Spectra (Ultraviolet-Visible Spectroscopy) analysis. The presence of cobalt hydroxide was confirmed by EDS, verifying the purity of the substance. Electrochemical characteristics, such as CV (Cyclic Voltammetry), GCD (Galvanostatic Charge-Discharge), and EIS (Electrochemical Impedance Spectroscopy) analysis, indicated capacitive behavior, confirming their feasibility for energy storage. The specific capacitances from 450 to 1250 F/g were measured from the GCD curve. The MATLAB study gave quantitative data on critical electrode characteristics which improved the understanding of the performance and a framework for further investigation in the development of sustainable energy solutions.
Graphical Abstract The synthesis and characterization of cobalt hydroxides generated from cobalt chloride precursors at various concentrations (0.1 to 0.5 M) by using cathodic electrochemical deposition technique for prospective energy storage application. The Co(OH) 2 thin fi lms were discovered to have a crystalline structure with a crystallite size of ~ 40 nanometers, particle size of 180 nm, and a leaf-like morphology via XRD (X-ray Diff raction) and SEM (Scanning Electron Microscopy) respectively. Further properties were investigated by EDS (Energy-Dispersive X-ray Spectroscopy), FTIR (Fourier TransformInfrared Spectroscopy), and UV Vis Spectra (Ultraviolet-Visible Spectroscopy) analysis. The presence of cobalt hydroxide was confi rmed by EDS, verifying the purity of the substance. Electrochemical characteristics, such as CV (Cyclic Voltammetry), GCD (Galvanostatic Charge-Discharge), and EIS (Electrochemical Impedance Spectroscopy) analysis, indicated capacitive behavior, confi rming their feasibility for energy storage. The specifi c capacitances from 450 to 1250 F/g were measured from the GCD curve. The MATLAB study gave quantitative data on critical electrode characteristics which improved the understanding of the performance and a framework for further investigation in the development of sustainable energy solutions. KCI Citation Count: 0 |
| Author | Naeem, Sajid |
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| Cites_doi | 10.1007/978-3-031-40299-9 10.1021/jp908548f 10.1016/j.jpowsour.2010.06.042 10.1016/j.jpowsour.2008.02.017 10.1039/a807000h 10.1021/cr020731c 10.1016/j.est.2023.106713 10.1149/1.1865852 10.1038/nmat2297 10.1002/chem.201100727 10.1038/ncomms15194 10.1149/1.2140677 10.1039/B609621B 10.20964/2016.12.50 10.1021/jp9005718 10.1063/1.118568 10.1007/s12274-011-0129-6 10.1016/j.cej.2022.138613 10.1002/jccs.201200419 10.1016/j.elecom.2009.07.002 10.1002/cjoc.200690212 10.1016/j.jallcom.2023.169078 10.1016/j.nanoen.2018.08.013 10.1016/j.micromeso.2008.06.004 10.1039/D2TA07626H 10.1039/b418955h 10.1016/j.jpowsour.2006.02.065 10.1149/1.2059264 10.1021/acssuschemeng.2c05636 |
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| Keywords | Electrochemical deposition Supercapacitor MATLAB simulation Material science Cobalt hydroxides Energy storage |
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| Snippet | The synthesis and characterization of cobalt hydroxides generated from cobalt chloride precursors at various concentrations (0.1 to 0.5 M) by using cathodic... The synthesis and characterization of cobalt hydroxides generated from cobalt chloride precursors at various concentrations (0.1 to 0.5 M) by using cathodic... |
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| Title | Electrodeposited Cobalt Hydroxide Thin Films: A Comprehensive Investigation from Synthesis to Advanced Electrochemical Behavior for High-Performance Energy Storage |
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