Synthesis and characterization of phosphorus-containing polysulfone

Chemical modification of a chloromethylated polysulfone (CMPS) was performed by reacting the chlorometyl group with PH bond of 9,10‐dihydro‐oxa‐10‐phosphophenanthrene‐10‐oxide (DOPO). A kinetic study of phosphorylation of CMPS with different chlorine content was reported. The obtained polymers bear...

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Published in	Polymer engineering and science Vol. 50; no. 1; pp. 48 - 56
Main Authors	Petreus, Oana, Avram, Ecaterina, Serbezeanu, Diana
Format	Journal Article
Language	English
Published	Hoboken Wiley Subscription Services, Inc., A Wiley Company 01.01.2010 Wiley Blackwell Publishing Ltd
Subjects	Applied sciences Chemical modifications Chemical reactions and properties Chemical-mechanical polishing Dynamic tests Dynamics Exact sciences and technology Mechanical analysis Morphology NMR Nuclear magnetic resonance Organic polymers Phosphorylation Physicochemistry of polymers Polymers Polysulfone resins Spectroscopy Spectrum analysis Ethersulfone copolymer Phosphorus copolymer Molecular structure Aromatic polymer Organic phosphinate Ethersulfone polymer Experimental study Thermal stability Thermal properties Chemical modification Dynamic mechanical properties Morphology Preparation Aromatic copolymer Kinetics Chlorine containing polymer Nucleophilic substitution
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ISSN	0032-3888 1548-2634
DOI	10.1002/pen.21508

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Abstract	Chemical modification of a chloromethylated polysulfone (CMPS) was performed by reacting the chlorometyl group with PH bond of 9,10‐dihydro‐oxa‐10‐phosphophenanthrene‐10‐oxide (DOPO). A kinetic study of phosphorylation of CMPS with different chlorine content was reported. The obtained polymers bearing cyclic bulky groups containing phosphorus were characterized by analytical methods; Fourier transforms spectroscopy (FTIR), and nuclear magnetic resonance spectroscopy (NMR). The thermal stability of phosphorus‐modified polysulfone was evaluated by dynamic thermogravimetric analysis in nitrogen gas. The polymers were readily soluble in polar organic solvent, such as N‐methylpyr‐rolidone (NMP), N,N‐dimethylacetamide (DMAc), and N,N‐dimethylformamide (DMF). Differential scanning calorimeter (DSC) and dynamic mechanical analysis (DMA) proved an amorphous morphology of these polymers. POLYM. ENG. SCI., 2010. © 2009 Society of Plastics Engineers
AbstractList	Chemical modification of a chloromethylated polysulfone (CMPS) was performed by reacting the chlorometyl group with PH bond of 9,10‐dihydro‐oxa‐10‐phosphophenanthrene‐10‐oxide (DOPO). A kinetic study of phosphorylation of CMPS with different chlorine content was reported. The obtained polymers bearing cyclic bulky groups containing phosphorus were characterized by analytical methods; Fourier transforms spectroscopy (FTIR), and nuclear magnetic resonance spectroscopy (NMR). The thermal stability of phosphorus‐modified polysulfone was evaluated by dynamic thermogravimetric analysis in nitrogen gas. The polymers were readily soluble in polar organic solvent, such as N‐methylpyr‐rolidone (NMP), N,N‐dimethylacetamide (DMAc), and N,N‐dimethylformamide (DMF). Differential scanning calorimeter (DSC) and dynamic mechanical analysis (DMA) proved an amorphous morphology of these polymers. POLYM. ENG. SCI., 2010. © 2009 Society of Plastics Engineers Chemical modification of a chloromethylated polysulfone (CMPS) was performed by reacting the chlorometyl group with P-H bond of 9,10-dihydro-oxa-10-phosphophenanthrene-10-oxide (DOPO). A kinetic study of phosphorylation of CMPS with different chlorine content was reported. The obtained polymers bearing cyclic bulky groups containing phosphorus were characterized by analytical methods; Fourier transforms spectroscopy (FTIR), and nuclear magnetic resonance spectroscopy (NMR). The thermal stability of phosphorus-modified polysulfone was evaluated by dynamic thermogravimetric analysis in nitrogen gas. The polymers were readily soluble in polar organic solvent, such as N-methylpyrrolidone (NMP), N,N-dimethylacetamide (DMAc), and N,N-dimethylformamide (DMF). Differential scanning calorimeter (DSC) and dynamic mechanical analysis (DMA) proved an amorphous morphology of these polymers. [PUBLICATION ABSTRACT] Chemical modification of a chloromethylated polysulfone (CMPS) was performed by reacting the chlorometyl group with PH bond of 9,10‐dihydro‐oxa‐10‐phosphophenanthrene‐10‐oxide (DOPO). A kinetic study of phosphorylation of CMPS with different chlorine content was reported. The obtained polymers bearing cyclic bulky groups containing phosphorus were characterized by analytical methods; Fourier transforms spectroscopy (FTIR), and nuclear magnetic resonance spectroscopy (NMR). The thermal stability of phosphorus‐modified polysulfone was evaluated by dynamic thermogravimetric analysis in nitrogen gas. The polymers were readily soluble in polar organic solvent, such as N ‐methylpyr‐rolidone (NMP), N , N ‐dimethylacetamide (DMAc), and N , N ‐dimethylformamide (DMF). Differential scanning calorimeter (DSC) and dynamic mechanical analysis (DMA) proved an amorphous morphology of these polymers. POLYM. ENG. SCI., 2010. © 2009 Society of Plastics Engineers
Author	Petreus, Oana Avram, Ecaterina Serbezeanu, Diana
Author_xml	– sequence: 1 givenname: Oana surname: Petreus fullname: Petreus, Oana email: opetreus@yahoo.com organization: "Petru Poni" Institute of Macromolecular Chemistry, Aleea Grigore Ghica Voda 41A, Iasi 700487, Romania – sequence: 2 givenname: Ecaterina surname: Avram fullname: Avram, Ecaterina organization: "Petru Poni" Institute of Macromolecular Chemistry, Aleea Grigore Ghica Voda 41A, Iasi 700487, Romania – sequence: 3 givenname: Diana surname: Serbezeanu fullname: Serbezeanu, Diana organization: "Petru Poni" Institute of Macromolecular Chemistry, Aleea Grigore Ghica Voda 41A, Iasi 700487, Romania
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Cites_doi	10.1039/an9608500556 10.1016/S0014-3057(02)00181-7 10.1002/app.1994.070540113 10.1016/S0376-7388(02)00352-6 10.1016/j.biomaterials.2005.07.010 10.1016/j.eurpolymj.2006.12.018 10.1016/S0032-3861(00)00202-0 10.1016/j.polymer.2006.12.011 10.1002/app.10765 10.1080/10601329708010036 10.1002/app.1993.070480912 10.1002/pola.10543 10.1002/1097-4628(20001031)78:5<979::AID-APP60>3.0.CO;2-U 10.1002/app.21126
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Keywords	Ethersulfone copolymer Phosphorus copolymer Molecular structure Aromatic polymer Organic phosphinate Ethersulfone polymer Experimental study Thermal stability Thermal properties Chemical modification Dynamic mechanical properties Morphology Preparation Aromatic copolymer Kinetics Chlorine containing polymer Nucleophilic substitution
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Snippet	Chemical modification of a chloromethylated polysulfone (CMPS) was performed by reacting the chlorometyl group with PH bond of... Chemical modification of a chloromethylated polysulfone (CMPS) was performed by reacting the chlorometyl group with P-H bond of...
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SubjectTerms	Applied sciences Chemical modifications Chemical reactions and properties Chemical-mechanical polishing Dynamic tests Dynamics Exact sciences and technology Mechanical analysis Morphology NMR Nuclear magnetic resonance Organic polymers Phosphorylation Physicochemistry of polymers Polymers Polysulfone resins Spectroscopy Spectrum analysis
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Title	Synthesis and characterization of phosphorus-containing polysulfone
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