Dip-coating on TiO2 foams using a suspension of Pt-TiO2 nanopowder synthesized by laser pyrolysis- : preliminary evaluation of the catalytic performances of the resulting composites in deVOC reactions
In an extension of a study to generate ceramic-metal nanosized composites deposited on ceramic foams, a new route to prepare Pt-TiO2 nanopowders of controlled metallic size and their further coating on TiO2 foams is described. Their efficiency as catalysts in volatile organic compound elimination (d...
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| Published in | Journal of the European Ceramic Society Vol. 27; no. 2-3; pp. 931 - 936 |
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| Main Authors | , , , , , , , |
| Format | Conference Proceeding Journal Article |
| Language | English |
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Oxford
Elsevier
2007
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| Abstract | In an extension of a study to generate ceramic-metal nanosized composites deposited on ceramic foams, a new route to prepare Pt-TiO2 nanopowders of controlled metallic size and their further coating on TiO2 foams is described. Their efficiency as catalysts in volatile organic compound elimination (deVOC) reactions was evaluated and compared with corresponding classical unsupported mixed powders. Composite metal/ceramic nanopowders (Pt-TiO2) were synthesised by laser pyrolysis using organo-metallic precursors. Successive dip-coatings on TiO2 foams using aqueous slurries of nanodispersed Pt-TiO2 particles were achieved. Both foam-supported and unsupported Pt-TiO2 grains of about 20 nm were stabilised, confirming no significant particle coalescence after a thermal treatment at 460 C. Both proved equally efficient catalysts for the total oxidation of methanol, selected as a probe deVOC reaction, thereby demonstrating that the dispersion of the nanopowders over the preformed ceramics did not modify their catalytic performance. 26 refs. |
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| AbstractList | In an extension of a study to generate ceramic-metal nanosized composites deposited on ceramic foams, a new route to prepare Pt-TiO2 nanopowders of controlled metallic size and their further coating on TiO2 foams is described. Their efficiency as catalysts in volatile organic compound elimination (deVOC) reactions was evaluated and compared with corresponding classical unsupported mixed powders. Composite metal/ceramic nanopowders (Pt-TiO2) were synthesised by laser pyrolysis using organo-metallic precursors. Successive dip-coatings on TiO2 foams using aqueous slurries of nanodispersed Pt-TiO2 particles were achieved. Both foam-supported and unsupported Pt-TiO2 grains of about 20 nm were stabilised, confirming no significant particle coalescence after a thermal treatment at 460 C. Both proved equally efficient catalysts for the total oxidation of methanol, selected as a probe deVOC reaction, thereby demonstrating that the dispersion of the nanopowders over the preformed ceramics did not modify their catalytic performance. 26 refs. |
| Author | GABELICA, Zelimir GIRAUD, Sophie MASKROT, Hicham LOUPIAS, Guillaume HERLIN-BOIME, Nathalie VALANGE, Sabine BARRAULT, Joël GUELOU, Erwan |
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| CitedBy_id | crossref_primary_10_1007_s12039_012_0290_9 crossref_primary_10_1016_j_apsusc_2013_06_125 crossref_primary_10_1016_j_jssc_2021_122817 crossref_primary_10_1021_cm8014034 crossref_primary_10_4028_www_scientific_net_AMM_670_671_22 crossref_primary_10_1016_j_ijhydene_2012_12_002 crossref_primary_10_1155_2013_452542 crossref_primary_10_1021_jp9003714 |
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| Keywords | Pyrolysis Catalytic reaction Composites Nanoparticle Transition element compounds Suspension Volatile organic compound Laser pyrolysis Composite material Powder Heterogeneous catalysis Platinum Laser Dip coating Titanium oxide |
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| Title | Dip-coating on TiO2 foams using a suspension of Pt-TiO2 nanopowder synthesized by laser pyrolysis- : preliminary evaluation of the catalytic performances of the resulting composites in deVOC reactions |
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