Improvement in the properties of low carbon MgO-C refractories through the addition of graphite-SiC micro-composite
[Display omitted] •Graphite–SiC microcomposites were synthesized via carbothermal reduction route.•SiC reinforced refractories exhibited much improved properties over the standard.•A low oxidation rate of 1.58 × 10−5 cm2 s-1 was observed in SiC based refractories.•Hot strength was enhanced from 42.3...
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| Published in | Journal of the European Ceramic Society Vol. 42; no. 4; pp. 1804 - 1814 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.04.2022
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Graphite–SiC microcomposites were synthesized via carbothermal reduction route.•SiC reinforced refractories exhibited much improved properties over the standard.•A low oxidation rate of 1.58 × 10−5 cm2 s-1 was observed in SiC based refractories.•Hot strength was enhanced from 42.3 to 57.4 kg cm−2 in SiC fortified refractories.•Designing strength factor above 0.13 with SiC forms a flaw tolerant microstructure.
Graphite–SiC micro-composites have been prepared in–house by carbothermal reduction process. Controlling the process parameters including the weight ratio of SiO2 to graphite as well as carbothermal reduction temperature during the micro-composite preparation favors the homogeneous formation of SiC with preferred morphologies like ribbons and whiskers/fibers. The micro-composite modified low carbon MgO-C refractories have exhibited significantly improved bulk properties over the standard composition. To understand the beneficial role of SiC reinforcement on hot strength performance under air oxidizing conditions, we propose a scaling parameter known as strength factor (fs) based on the ratio of hot strength (HMOR) to cold strength (CCS). Correlating the strength factor data (fs) with oxidative damage provides new insights into the reinforcing effects of distinct SiC morphologies in this new class of micro-composite fortified refractory systems over the standard compositions. |
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| AbstractList | [Display omitted]
•Graphite–SiC microcomposites were synthesized via carbothermal reduction route.•SiC reinforced refractories exhibited much improved properties over the standard.•A low oxidation rate of 1.58 × 10−5 cm2 s-1 was observed in SiC based refractories.•Hot strength was enhanced from 42.3 to 57.4 kg cm−2 in SiC fortified refractories.•Designing strength factor above 0.13 with SiC forms a flaw tolerant microstructure.
Graphite–SiC micro-composites have been prepared in–house by carbothermal reduction process. Controlling the process parameters including the weight ratio of SiO2 to graphite as well as carbothermal reduction temperature during the micro-composite preparation favors the homogeneous formation of SiC with preferred morphologies like ribbons and whiskers/fibers. The micro-composite modified low carbon MgO-C refractories have exhibited significantly improved bulk properties over the standard composition. To understand the beneficial role of SiC reinforcement on hot strength performance under air oxidizing conditions, we propose a scaling parameter known as strength factor (fs) based on the ratio of hot strength (HMOR) to cold strength (CCS). Correlating the strength factor data (fs) with oxidative damage provides new insights into the reinforcing effects of distinct SiC morphologies in this new class of micro-composite fortified refractory systems over the standard compositions. |
| Author | Sarkar, Debasish K., Sarath Chandra Mahata, Tapas Raju, Mula Maiti, Himadri Sekhar |
| Author_xml | – sequence: 1 givenname: Mula surname: Raju fullname: Raju, Mula organization: Materials Science Centre, Indian Institute of Technology, Kharagpur, West Bengal, 721302, India – sequence: 2 givenname: Sarath Chandra surname: K. fullname: K., Sarath Chandra organization: Research and Development Centre, RHI Magnesita, Bhiwadi, Rajasthan, 301019, India – sequence: 3 givenname: Tapas surname: Mahata fullname: Mahata, Tapas organization: TRL Krosaki Refractories Limited, Belpahar, Odisha, 768218, India – sequence: 4 givenname: Debasish orcidid: 0000-0002-6712-0520 surname: Sarkar fullname: Sarkar, Debasish email: dsarkar@nitrkl.ac.in organization: Department of Ceramic Engineering, National Institute of Technology, Rourkela, Odisha, 769008, India – sequence: 5 givenname: Himadri Sekhar surname: Maiti fullname: Maiti, Himadri Sekhar organization: Department of Ceramic Technology, Government College of Engineering and Ceramic Technology, Kolkata, West Bengal, 700010, India |
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| Keywords | Fibrous structure of the SiC Oxidation resistance Strength factor Hot strength Graphite-SiC micro-composite MgO-C refractory |
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•Graphite–SiC microcomposites were synthesized via carbothermal reduction route.•SiC reinforced refractories exhibited much improved... |
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| SubjectTerms | Fibrous structure of the SiC Graphite-SiC micro-composite Hot strength MgO-C refractory Oxidation resistance Strength factor |
| Title | Improvement in the properties of low carbon MgO-C refractories through the addition of graphite-SiC micro-composite |
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