Densification of alumina by SPS and HP: A comparative study
In this study, the densification of alumina by spark plasma sintering (SPS) was investigated and compared to conventional hot pressing. It was shown that SPS is very effective in the sintering of alumina leading to higher densities and allows to work at lower temperatures and with shorter sintering...
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Published in | Journal of the European Ceramic Society Vol. 32; no. 9; pp. 1957 - 1964 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Elsevier Ltd
01.07.2012
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Abstract | In this study, the densification of alumina by spark plasma sintering (SPS) was investigated and compared to conventional hot pressing. It was shown that SPS is very effective in the sintering of alumina leading to higher densities and allows to work at lower temperatures and with shorter sintering cycles. The effect of the heating rate is dependent on the heating mode (SPS or HP). The identification of active sintering mechanisms was attempted by an isothermal and an anisothermal methods, showing that other mechanisms probably related to electrical effects enhance the densification. We suggest the higher contribution of surface diffusion mainly during the initial stage of sintering and an influence of the presence of impurities segregated at the grain boundaries. They could create conductive layers and also introduce ions with a lower valence than Al3+; defects are created in the surface layers and the diffusion of the species is increased. |
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AbstractList | In this study, the densification of alumina by spark plasma sintering (SPS) was investigated and compared to conventional hot pressing. It was shown that SPS is very effective in the sintering of alumina leading to higher densities and allows to work at lower temperatures and with shorter sintering cycles. The effect of the heating rate is dependent on the heating mode (SPS or HP). The identification of active sintering mechanisms was attempted by an isothermal and an anisothermal methods, showing that other mechanisms probably related to electrical effects enhance the densification. We suggest the higher contribution of surface diffusion mainly during the initial stage of sintering and an influence of the presence of impurities segregated at the grain boundaries. They could create conductive layers and also introduce ions with a lower valence than Al3+; defects are created in the surface layers and the diffusion of the species is increased. |
Author | Erauw, Jean-Pierre Demuynck, Maryse Cambier, Francis Delannay, Francis Van der Biest, Omer |
Author_xml | – sequence: 1 givenname: Maryse surname: Demuynck fullname: Demuynck, Maryse email: m.demuynck@bcrc.be organization: Belgian Ceramic Research Centre (EMRA), Avenue Gouverneur Cornez 4, B-7000 Mons, Belgium – sequence: 2 givenname: Jean-Pierre surname: Erauw fullname: Erauw, Jean-Pierre organization: Belgian Ceramic Research Centre (EMRA), Avenue Gouverneur Cornez 4, B-7000 Mons, Belgium – sequence: 3 givenname: Omer surname: Van der Biest fullname: Van der Biest, Omer organization: MTM KULeuven, Kasteelpark Arenberg 44, B-3001 Leuven, Belgium – sequence: 4 givenname: Francis surname: Delannay fullname: Delannay, Francis organization: EMPA UCLouvain, Place Sainte Barbe 2, B-1348 Louvain-la-Neuve, Belgium – sequence: 5 givenname: Francis surname: Cambier fullname: Cambier, Francis organization: Belgian Ceramic Research Centre (EMRA), Avenue Gouverneur Cornez 4, B-7000 Mons, Belgium |
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Cites_doi | 10.1007/s10853-006-6555-2 10.1111/j.1744-7402.2010.02604.x 10.1111/j.1151-2916.1991.tb07815.x 10.1111/j.1551-2916.2009.03102.x 10.1111/j.1551-2916.2007.01778.x 10.1016/S1359-6462(99)00126-8 10.1111/j.1151-2916.1996.tb08097.x 10.1016/j.actamat.2007.01.048 10.1016/j.actamat.2009.07.043 10.1111/j.1551-2916.2008.02630.x 10.1111/j.1551-2916.2010.04210.x 10.1111/j.1551-2916.2010.04089.x 10.1016/S0921-5093(00)00772-3 10.1111/j.1151-2916.2002.tb00381.x |
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Keywords | Grain size Spark plasma sintering (SPS) Hot pressing (HP) Sintering Al2O3 |
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