Densification of alumina by SPS and HP: A comparative study

In this study, the densification of alumina by spark plasma sintering (SPS) was investigated and compared to conventional hot pressing. It was shown that SPS is very effective in the sintering of alumina leading to higher densities and allows to work at lower temperatures and with shorter sintering...

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Published inJournal of the European Ceramic Society Vol. 32; no. 9; pp. 1957 - 1964
Main Authors Demuynck, Maryse, Erauw, Jean-Pierre, Van der Biest, Omer, Delannay, Francis, Cambier, Francis
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.07.2012
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Abstract In this study, the densification of alumina by spark plasma sintering (SPS) was investigated and compared to conventional hot pressing. It was shown that SPS is very effective in the sintering of alumina leading to higher densities and allows to work at lower temperatures and with shorter sintering cycles. The effect of the heating rate is dependent on the heating mode (SPS or HP). The identification of active sintering mechanisms was attempted by an isothermal and an anisothermal methods, showing that other mechanisms probably related to electrical effects enhance the densification. We suggest the higher contribution of surface diffusion mainly during the initial stage of sintering and an influence of the presence of impurities segregated at the grain boundaries. They could create conductive layers and also introduce ions with a lower valence than Al3+; defects are created in the surface layers and the diffusion of the species is increased.
AbstractList In this study, the densification of alumina by spark plasma sintering (SPS) was investigated and compared to conventional hot pressing. It was shown that SPS is very effective in the sintering of alumina leading to higher densities and allows to work at lower temperatures and with shorter sintering cycles. The effect of the heating rate is dependent on the heating mode (SPS or HP). The identification of active sintering mechanisms was attempted by an isothermal and an anisothermal methods, showing that other mechanisms probably related to electrical effects enhance the densification. We suggest the higher contribution of surface diffusion mainly during the initial stage of sintering and an influence of the presence of impurities segregated at the grain boundaries. They could create conductive layers and also introduce ions with a lower valence than Al3+; defects are created in the surface layers and the diffusion of the species is increased.
Author Erauw, Jean-Pierre
Demuynck, Maryse
Cambier, Francis
Delannay, Francis
Van der Biest, Omer
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  organization: Belgian Ceramic Research Centre (EMRA), Avenue Gouverneur Cornez 4, B-7000 Mons, Belgium
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Keywords Grain size
Spark plasma sintering (SPS)
Hot pressing (HP)
Sintering
Al2O3
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Snippet In this study, the densification of alumina by spark plasma sintering (SPS) was investigated and compared to conventional hot pressing. It was shown that SPS...
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SubjectTerms Al2O3
Grain size
Hot pressing (HP)
Sintering
Spark plasma sintering (SPS)
Title Densification of alumina by SPS and HP: A comparative study
URI https://dx.doi.org/10.1016/j.jeurceramsoc.2011.10.031
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