Combined hot extrusion and spark plasma sintering method for producing highly textured thermoelectric Bi2Te3 alloys
Hot extrusion is a promising method for producing high-performance thermoelectric bismuth telluride alloys because of its ability to create textured microstructures. However, hot extrusion is less favourable for scaling-up because of temperature and strain gradients along the radial direction, and o...
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| Published in | Journal of the European Ceramic Society Vol. 40; no. 8; pp. 3042 - 3048 |
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| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.07.2020
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| Abstract | Hot extrusion is a promising method for producing high-performance thermoelectric bismuth telluride alloys because of its ability to create textured microstructures. However, hot extrusion is less favourable for scaling-up because of temperature and strain gradients along the radial direction, and only -textured thermoelectric legs can be obtained because of the fibre-like texture. We suggest a way to overcome these disadvantages by implementing an additional spark plasma sintering process on a stack of extrudates. Using this combined process, we demonstrate the fabrication of 12 × 15 × 13 mm3 p-type (Bi0.2Sb0.8)2Te3 samples from extrudates that had originally been 3 mm in diameter. The evolution of sheet-like texture revealed by SEM, XRD, and EBSD allows us to obtain both - and -textured thermoelectric legs from a single specimen that are desirable for low- and high-temperature applications, respectively. Our results demonstrate the combined method as an industry-friendly process for fabricating high-performance thermoelectric materials. |
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| AbstractList | Hot extrusion is a promising method for producing high-performance thermoelectric bismuth telluride alloys because of its ability to create textured microstructures. However, hot extrusion is less favourable for scaling-up because of temperature and strain gradients along the radial direction, and only -textured thermoelectric legs can be obtained because of the fibre-like texture. We suggest a way to overcome these disadvantages by implementing an additional spark plasma sintering process on a stack of extrudates. Using this combined process, we demonstrate the fabrication of 12 × 15 × 13 mm3 p-type (Bi0.2Sb0.8)2Te3 samples from extrudates that had originally been 3 mm in diameter. The evolution of sheet-like texture revealed by SEM, XRD, and EBSD allows us to obtain both - and -textured thermoelectric legs from a single specimen that are desirable for low- and high-temperature applications, respectively. Our results demonstrate the combined method as an industry-friendly process for fabricating high-performance thermoelectric materials. |
| Author | Jung, Sung-Jin Kim, Jin-Sang Kim, Seong Keun Lee, Byeong-Hyeon Lim, Sang-Soon Park, Hyung-Ho Kim, Dong-Ik Shin, Joonchul Won, Sung Ok Kim, Byung Kyu Baek, Seung-Hyub |
| Author_xml | – sequence: 1 givenname: Sang-Soon surname: Lim fullname: Lim, Sang-Soon organization: Center for Electronic Materials, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea – sequence: 2 givenname: Sung-Jin surname: Jung fullname: Jung, Sung-Jin organization: Center for Electronic Materials, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea – sequence: 3 givenname: Byung Kyu surname: Kim fullname: Kim, Byung Kyu organization: High Temp. Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea – sequence: 4 givenname: Dong-Ik surname: Kim fullname: Kim, Dong-Ik organization: High Temp. Energy Materials Research Center, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea – sequence: 5 givenname: Byeong-Hyeon surname: Lee fullname: Lee, Byeong-Hyeon organization: Advanced Analysis Center, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea – sequence: 6 givenname: Sung Ok surname: Won fullname: Won, Sung Ok organization: Advanced Analysis Center, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea – sequence: 7 givenname: Joonchul surname: Shin fullname: Shin, Joonchul organization: Center for Electronic Materials, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea – sequence: 8 givenname: Hyung-Ho surname: Park fullname: Park, Hyung-Ho organization: Department of Materials Science and Engineering, Yonsei University, Seoul 03722, Republic of Korea – sequence: 9 givenname: Seong Keun surname: Kim fullname: Kim, Seong Keun organization: Center for Electronic Materials, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea – sequence: 10 givenname: Jin-Sang surname: Kim fullname: Kim, Jin-Sang email: jskim@kist.re.kr organization: Center for Electronic Materials, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea – sequence: 11 givenname: Seung-Hyub surname: Baek fullname: Baek, Seung-Hyub email: shbaek77@kist.re.kr organization: Center for Electronic Materials, Korea Institute of Science and Technology, Seoul 02792, Republic of Korea |
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| Keywords | Hot extrusion (HE) Thermoelectrics Spark plasma sintering (SPS) Bi2Te3 alloys |
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