Copper-ceria sheets catalysts: Effect of copper species on catalytic activity in CO oxidation reaction
Copper-ceria sheets catalysts with different loadings of copper(2 wt.%, 5 wt.% and 10 wt.%) supported on ceria nanosheets were synthesized via a depositioneprecipitation(DP) method. The prepared catalysts were systematically characterized with various structural and textural detections including X-r...
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Published in | Journal of rare earths Vol. 35; no. 12; pp. 1186 - 1196 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.12.2017
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Abstract | Copper-ceria sheets catalysts with different loadings of copper(2 wt.%, 5 wt.% and 10 wt.%) supported on ceria nanosheets were synthesized via a depositioneprecipitation(DP) method. The prepared catalysts were systematically characterized with various structural and textural detections including X-ray diffraction(XRD), Raman spectra, transmission electron microscopy(TEM), X-ray absorption fine structure(XAFS), and temperature-programmed reduction by hydrogen(H2-TPR), and tested for the CO oxidation reaction. Notably, the sample containing 5 wt.% of Cu exhibited the best catalytic performance as a result of the highest number of active CuO species on the catalyst surface. Further increase of copper content strongly affects the dispersion of copper and thus leads to the formation of less active bulk CuO phase, which was verified by XRD and H2-TPR analysis. Moreover, on the basis of in-situ diffuse reflectance infrared Fourier transform spectroscopy(in-situ DRIFTS) results, the surface Cu~+ species, which are derived from the reduction of Cu~(2+), are likely to play a crucial role in the catalyzing CO oxidation.Consequently, the superior catalytic performance of the copper-ceria sheets is mainly attributed to the highly dispersed CuOx cluster rather than Cu-[Ox]-Ce structure, while the bulk CuO phase is adverse to the catalytic activity of CO oxidation. |
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AbstractList | Copper-ceria sheets catalysts with different loadings of copper (2 wt.%, 5 wt.% and 10 wt.%) supported on ceria nanosheets were synthesized via a deposition–precipitation (DP) method. The prepared catalysts were systematically characterized with various structural and textural detections including X-ray diffraction (XRD), Raman spectra, transmission electron microscopy (TEM), X-ray absorption fine structure (XAFS), and temperature-programmed reduction by hydrogen (H2-TPR), and tested for the CO oxidation reaction. Notably, the sample containing 5 wt.% of Cu exhibited the best catalytic performance as a result of the highest number of active CuO species on the catalyst surface. Further increase of copper content strongly affects the dispersion of copper and thus leads to the formation of less active bulk CuO phase, which was verified by XRD and H2-TPR analysis. Moreover, on the basis of in-situ diffuse reflectance infrared Fourier transform spectroscopy (in-situ DRIFTS) results, the surface Cu+ species, which are derived from the reduction of Cu2+, are likely to play a crucial role in the catalyzing CO oxidation. Consequently, the superior catalytic performance of the copper-ceria sheets is mainly attributed to the highly dispersed CuOx cluster rather than Cu-[Ox]-Ce structure, while the bulk CuO phase is adverse to the catalytic activity of CO oxidation.
[Display omitted] Copper-ceria sheets catalysts with different loadings of copper(2 wt.%, 5 wt.% and 10 wt.%) supported on ceria nanosheets were synthesized via a depositioneprecipitation(DP) method. The prepared catalysts were systematically characterized with various structural and textural detections including X-ray diffraction(XRD), Raman spectra, transmission electron microscopy(TEM), X-ray absorption fine structure(XAFS), and temperature-programmed reduction by hydrogen(H2-TPR), and tested for the CO oxidation reaction. Notably, the sample containing 5 wt.% of Cu exhibited the best catalytic performance as a result of the highest number of active CuO species on the catalyst surface. Further increase of copper content strongly affects the dispersion of copper and thus leads to the formation of less active bulk CuO phase, which was verified by XRD and H2-TPR analysis. Moreover, on the basis of in-situ diffuse reflectance infrared Fourier transform spectroscopy(in-situ DRIFTS) results, the surface Cu~+ species, which are derived from the reduction of Cu~(2+), are likely to play a crucial role in the catalyzing CO oxidation.Consequently, the superior catalytic performance of the copper-ceria sheets is mainly attributed to the highly dispersed CuOx cluster rather than Cu-[Ox]-Ce structure, while the bulk CuO phase is adverse to the catalytic activity of CO oxidation. |
Author | Linying Du;Weiwei Wang;Han Yan;Xu Wang;Zhao Jin;Qisheng Song;Rui Si;Chunjiang Jia |
AuthorAffiliation | Key Laboratory for Colloid and Interface Chemistry, Key Laboratory of Special Aggregated Materials, School of Chemistry and Chemical Engineering,Shandong University;Shanghai Synchrotron Radiation Facility, Shanghai Institute of Applied Physics, Chinese Academy of Sciences |
Author_xml | – sequence: 1 givenname: Linying surname: Du fullname: Du, Linying organization: Key Laboratory for Colloid and Interface Chemistry, Key Laboratory of Special Aggregated Materials, School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100, China – sequence: 2 givenname: Weiwei surname: Wang fullname: Wang, Weiwei organization: Key Laboratory for Colloid and Interface Chemistry, Key Laboratory of Special Aggregated Materials, School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100, China – sequence: 3 givenname: Han surname: Yan fullname: Yan, Han organization: Key Laboratory for Colloid and Interface Chemistry, Key Laboratory of Special Aggregated Materials, School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100, China – sequence: 4 givenname: Xu surname: Wang fullname: Wang, Xu organization: Shanghai Synchrotron Radiation Facility, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201204, China – sequence: 5 givenname: Zhao surname: Jin fullname: Jin, Zhao email: jinzhao@sdu.edu.cn organization: Key Laboratory for Colloid and Interface Chemistry, Key Laboratory of Special Aggregated Materials, School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100, China – sequence: 6 givenname: Qisheng surname: Song fullname: Song, Qisheng organization: Key Laboratory for Colloid and Interface Chemistry, Key Laboratory of Special Aggregated Materials, School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100, China – sequence: 7 givenname: Rui surname: Si fullname: Si, Rui organization: Shanghai Synchrotron Radiation Facility, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201204, China – sequence: 8 givenname: Chunjiang orcidid: 0000-0002-4254-5100 surname: Jia fullname: Jia, Chunjiang email: jiacj@sdu.edu.cn organization: Key Laboratory for Colloid and Interface Chemistry, Key Laboratory of Special Aggregated Materials, School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100, China |
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Keywords | Copper-ceria catalysts Copper oxide species Structure–properties relationship CO oxidation Ceria nanosheets |
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Notes | 11-2788/TF Ceria nanosheets Copper-ceria catalysts CO oxidation Copper oxide species Structure-properties relationship Copper-ceria sheets catalysts with different loadings of copper(2 wt.%, 5 wt.% and 10 wt.%) supported on ceria nanosheets were synthesized via a depositioneprecipitation(DP) method. The prepared catalysts were systematically characterized with various structural and textural detections including X-ray diffraction(XRD), Raman spectra, transmission electron microscopy(TEM), X-ray absorption fine structure(XAFS), and temperature-programmed reduction by hydrogen(H2-TPR), and tested for the CO oxidation reaction. Notably, the sample containing 5 wt.% of Cu exhibited the best catalytic performance as a result of the highest number of active CuO species on the catalyst surface. Further increase of copper content strongly affects the dispersion of copper and thus leads to the formation of less active bulk CuO phase, which was verified by XRD and H2-TPR analysis. Moreover, on the basis of in-situ diffuse reflectance infrared Fourier transform spectroscopy(in-situ DRIFTS) results, the surface Cu~+ species, which are derived from the reduction of Cu~(2+), are likely to play a crucial role in the catalyzing CO oxidation.Consequently, the superior catalytic performance of the copper-ceria sheets is mainly attributed to the highly dispersed CuOx cluster rather than Cu-[Ox]-Ce structure, while the bulk CuO phase is adverse to the catalytic activity of CO oxidation. |
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Snippet | Copper-ceria sheets catalysts with different loadings of copper(2 wt.%, 5 wt.% and 10 wt.%) supported on ceria nanosheets were synthesized via a... Copper-ceria sheets catalysts with different loadings of copper (2 wt.%, 5 wt.% and 10 wt.%) supported on ceria nanosheets were synthesized via a... |
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SubjectTerms | Ceria nanosheets CO oxidation Copper oxide species Copper-ceria catalysts Structure–properties relationship |
Title | Copper-ceria sheets catalysts: Effect of copper species on catalytic activity in CO oxidation reaction |
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