Effect of the surface condition of silicas with grafted monofunctional polyfluoroalkylsilanes on the adsorption of polar molecules
Lyophobized silicas containing relatively small numbers of grafted perfluorohexyl (1.1 nm −2 ) and perfluorobutyl (1.7 nm −2 ) groups are studied by means of gas chromatography, adsorption under static conditions, and IR spectroscopy. The results are compared to those obtained by us previously for a...
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Published in | Russian Journal of Physical Chemistry A Vol. 87; no. 8; pp. 1367 - 1373 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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01.08.2013
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Abstract | Lyophobized silicas containing relatively small numbers of grafted perfluorohexyl (1.1 nm
−2
) and perfluorobutyl (1.7 nm
−2
) groups are studied by means of gas chromatography, adsorption under static conditions, and IR spectroscopy. The results are compared to those obtained by us previously for a series of samples with dense polyfluoroalkyl monolayers (≥2.0 nm
−2
). Effects related to the influence of the grafting density and the size of fluorine-containing groups on the adsorption of polar compounds and the hydrophobicity of the surface are discussed. |
---|---|
AbstractList | Lyophobized silicas containing relatively small numbers of grafted perfluorohexyl (1.1 nm
−2
) and perfluorobutyl (1.7 nm
−2
) groups are studied by means of gas chromatography, adsorption under static conditions, and IR spectroscopy. The results are compared to those obtained by us previously for a series of samples with dense polyfluoroalkyl monolayers (≥2.0 nm
−2
). Effects related to the influence of the grafting density and the size of fluorine-containing groups on the adsorption of polar compounds and the hydrophobicity of the surface are discussed. Lyophobized silicas containing relatively small numbers of grafted perfluorohexyl (1.1 nm/2) and perfluorobutyl (1.7 nm/2) groups are studied by means of gas chromatography, adsorption under static conditions, and IR spectroscopy. The results are compared to those obtained by us previously for a series of samples with dense polyfluoroalkyl monolayers (-2.0 nm/2). Effects related to the influence of the grafting density and the size of fluorine-containing groups on the adsorption of polar compounds and the hydrophobicity of the surface are discussed. |
Author | Roshchina, T. M. Tkachenko, O. P. Shoniya, N. K. Kustov, L. M. Tayakina, O. Ya |
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Snippet | Lyophobized silicas containing relatively small numbers of grafted perfluorohexyl (1.1 nm
−2
) and perfluorobutyl (1.7 nm
−2
) groups are studied by means of... Lyophobized silicas containing relatively small numbers of grafted perfluorohexyl (1.1 nm/2) and perfluorobutyl (1.7 nm/2) groups are studied by means of gas... |
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SubjectTerms | Chemistry Chemistry and Materials Science Physical Chemistry Physical Chemistry of Surface Phenomena |
Title | Effect of the surface condition of silicas with grafted monofunctional polyfluoroalkylsilanes on the adsorption of polar molecules |
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