Preparation and non-linear optical properties of CdS quantum dots in Na2O-B2O3-SiO2 glasses by the sol-gel technique
Nonlinear optical properties of CdS quantum dots embedded in the sol gel derived Na2O-B2O3-SiO2 glass matrix have been studied using nanosecond degenerate four-wave mixing (DFWM), pump-probe experiments, and time-resolved subpicosecond DFWM measurements. The concentration of CdS microcrystallites wa...
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Published in | Journal of materials science Vol. 31; no. 2; pp. 423 - 430 |
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Format | Journal Article |
Language | English |
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1996
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Abstract | Nonlinear optical properties of CdS quantum dots embedded in the sol gel derived Na2O-B2O3-SiO2 glass matrix have been studied using nanosecond degenerate four-wave mixing (DFWM), pump-probe experiments, and time-resolved subpicosecond DFWM measurements. The concentration of CdS microcrystallites was varied from 1.4 to 10.2 wt pct while the particle size was controlled to be in the range of 3 - 6 nm in diameter so that the confinement effects could be realized. The third-order susceptibility was determined to be of the order of 10 exp -7 - 10 exp -6 e.s.u. near the resonant wavelength between 450 and 470 nm by the nanosecond DFWM and pump-probe experiments, and of the order of 10 exp -11 - 10 exp -10 e.s.u. at the off-resonant wavelength, 580 nm, by a time-resolved DFWM measurement with 400 fs laser pulse. The decay time changed from 0.5 to 50 picoseconds as a function of the size, size distribution, and number density of CdS microcrystallites in the glasses. Photodarkening reduced the optical nonlinearity of the melt-quenched samples by a factor of about 20, while it had no appreciable effect on that of the sol gel derived samples. (Author) |
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AbstractList | Non-linear optical properties of CdS quantum dots embedded in the sol-gel derived Na2O-B2O3-SiO2 glass matrix were studied using nanosecond degenerate four-wave mixing (DFWM), pump-probe experiments, and time-resolved subpicosecond DFWM measurements. The concentration of CdS microcrystallites was varied from 1.4 to 10.2 wt% while the particle size was controlled to be in the range of 3-6 nm in diameter so that the confinement effects could be realised. The third-order susceptibility, chi(3), was determined to be of the order of 10 exp(-7)-10 exp(-6) esu near the resonant wavelength between 450 and 470 nm by the nanosecond DFWM and pump-probe experiments, and of the order of 10 exp(-11)-10 exp(-10) esu at the off-resonant wavelength, 580 nm, by a time-resolved DFWM measurement with 400 fs laser pulse. The decay time changed from 0.5 to 50 picoseconds as a function of the size, size distribution and number density of CdS microcrystallites in the glasses. Photodarkening reduced the optical non-linearity of the melt-quenched samples by a factor of approximately equal to 20, while it had no appreciable effect on that of the sol-gel derived samples. 30 refs. Nonlinear optical properties of CdS quantum dots embedded in the sol gel derived Na2O-B2O3-SiO2 glass matrix have been studied using nanosecond degenerate four-wave mixing (DFWM), pump-probe experiments, and time-resolved subpicosecond DFWM measurements. The concentration of CdS microcrystallites was varied from 1.4 to 10.2 wt pct while the particle size was controlled to be in the range of 3 - 6 nm in diameter so that the confinement effects could be realized. The third-order susceptibility was determined to be of the order of 10 exp -7 - 10 exp -6 e.s.u. near the resonant wavelength between 450 and 470 nm by the nanosecond DFWM and pump-probe experiments, and of the order of 10 exp -11 - 10 exp -10 e.s.u. at the off-resonant wavelength, 580 nm, by a time-resolved DFWM measurement with 400 fs laser pulse. The decay time changed from 0.5 to 50 picoseconds as a function of the size, size distribution, and number density of CdS microcrystallites in the glasses. Photodarkening reduced the optical nonlinearity of the melt-quenched samples by a factor of about 20, while it had no appreciable effect on that of the sol gel derived samples. (Author) |
Author | KANG, K REEVES, R. J PEYGHAMBARIAN, N KNOBBE, E. T MACKENZIE, J. D YAMANE, M TAKADA, T POWELL, R. C |
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Keywords | Inorganic compounds Semiconductor materials Quantum dots Transition element compounds Cadmium sulfides Non linear optical susceptibility Glass Experimental study Preparation Size effect Absorption spectra Nonlinear optics Sol-gel process |
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References | T. Tokizaki (CR17) 1992; 117 CR18 A. I. (CR21) 1985; 56 CR14 N. Peyghambarian (CR1) 1990 CR12 CR11 T. Yanagawa (CR6) 1992; 88 Y. Z. Hu (CR15) 1990; 64 K. Kang (CR26) 1994; 64 K. W. Delong (CR8) 1989; 6 P. Roussignol (CR5) 1987; 4 R. K. Jain (CR3) 1983; 73 J. Yumoto (CR4) 1987; 12 B. G. Potter Jr. (CR23) 1988; 37 M. G. Bawendi (CR20) 1990; 65 L-C. Liu (CR25) 1990; 68 B. Wonterghem van (CR7) 1989; 66 S. H. Park (CR16) 1990; 7 E. M. Wright (CR9) 1988; 52 F. Hache (CR28) 1988; 47 T. Takada (CR30) 1994; 1 N. F. Borrelli (CR13) 1987; 61 L. Brus (CR22) 1986; 90 R. W. Bryant (CR2) 1989 F. Hache (CR24) 1986; 3 D. Regard (CR19) 1990; 159 D. W. Hall (CR27) 1988; 5 M. J. Bloemer (CR29) 1990; 7 T. Takada (CR10) 1992; 147 & 148 |
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Snippet | Nonlinear optical properties of CdS quantum dots embedded in the sol gel derived Na2O-B2O3-SiO2 glass matrix have been studied using nanosecond degenerate... Non-linear optical properties of CdS quantum dots embedded in the sol-gel derived Na2O-B2O3-SiO2 glass matrix were studied using nanosecond degenerate... |
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SubjectTerms | Condensed matter: electronic structure, electrical, magnetic, and optical properties Exact sciences and technology Fundamental areas of phenomenology (including applications) Ii-vi semiconductors Nonlinear optics Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation Optical properties of specific thin films Optical susceptibility, hyperpolarizability Optics Physics |
Title | Preparation and non-linear optical properties of CdS quantum dots in Na2O-B2O3-SiO2 glasses by the sol-gel technique |
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