Polyoxometalate-based organic-inorganic hybrid compounds containing transition metal mixed-organic-ligand complexes of N-containing and pyridinecarboxylate ligands
Five new organic–inorganic hybrid compounds based on the Keggin-type polyoxoanion [SiW12O40]4−, namely [Cu3(2,2′-bpy)3(inic)(μ2-OH)(H2O)][SiW12O40]·2H2O (1), [Cu6(phen)6(μ3-Cl)2(μ2-Cl)2Cl2(inic)2][SiW12O40]·6H2O (2), [Cu2(hnic)(2,2′-bpy)2Cl]2[H2SiW12O40] (3), [Cu2(nic)(phen)2Cl2]2[SiW12O40] (4) and...
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Published in | Dalton transactions : an international journal of inorganic chemistry Vol. 44; no. 19; pp. 8971 - 8983 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
Published |
England
21.05.2015
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Abstract | Five new organic–inorganic hybrid compounds based on the Keggin-type polyoxoanion [SiW12O40]4−, namely [Cu3(2,2′-bpy)3(inic)(μ2-OH)(H2O)][SiW12O40]·2H2O (1), [Cu6(phen)6(μ3-Cl)2(μ2-Cl)2Cl2(inic)2][SiW12O40]·6H2O (2), [Cu2(hnic)(2,2′-bpy)2Cl]2[H2SiW12O40] (3), [Cu2(nic)(phen)2Cl2]2[SiW12O40] (4) and [Cu2(pic)(2,2′-bpy)2Cl]2[SiW12O40] (5) (inic = isonicotinic acid, hnic = 2-hydroxy-nicotinic acid, nic = nicotinic acid, pic = picolinic acid, 2,2′-bpy = 2,2′-bipyridine, phen = 1,10-phenanthroline) have been synthesized and characterized by IR, UV-Vis, XPS, XRD, cyclic voltammetric measurements, photoluminescence analysis and single crystal X-ray diffraction analysis. Crystal analysis reveals that compound 1 exhibits a 2-D double layered framework structure constructed from [SiW12O40]4− and copper-aqua-2,2′-bipy-hydroxyl-isonicotinate complexes. Compound 2 is a 0-D discrete structure formed by [SiW12O40]4− and copper-chloro-isonicotinate-phenanthroline complexes. Compound 3 shows a 1-D single chain structure based on the linkage of copper-2,2-bpy-chloro-2-hydroxy-nicotinate complexes and [SiW12O40]4−. Compounds 4 and 5 both contain polyoxometalate supported transition metal complexes, one is a polyoxometalate supported copper-chloro-nicotinate-phenanthroline complex in 4, and the other is a polyoxometalate supported copper-2,2-bpy-chloro-nicotinate complex in 5. It should be noted that nicotinic, isonicotinic and picolinic acids are structural isomers and 2-hydroxy-nicotinic acid is an in situ hydroxylated product of nicotinic acid. In addition, photocatalytic degradation of Rhodamine B (RhB) by compounds 1–5 has been investigated in aqueous solutions. |
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AbstractList | Five new organic–inorganic hybrid compounds based on the Keggin-type polyoxoanion [SiW12O40]4−, namely [Cu3(2,2′-bpy)3(inic)(μ2-OH)(H2O)][SiW12O40]·2H2O (1), [Cu6(phen)6(μ3-Cl)2(μ2-Cl)2Cl2(inic)2][SiW12O40]·6H2O (2), [Cu2(hnic)(2,2′-bpy)2Cl]2[H2SiW12O40] (3), [Cu2(nic)(phen)2Cl2]2[SiW12O40] (4) and [Cu2(pic)(2,2′-bpy)2Cl]2[SiW12O40] (5) (inic = isonicotinic acid, hnic = 2-hydroxy-nicotinic acid, nic = nicotinic acid, pic = picolinic acid, 2,2′-bpy = 2,2′-bipyridine, phen = 1,10-phenanthroline) have been synthesized and characterized by IR, UV-Vis, XPS, XRD, cyclic voltammetric measurements, photoluminescence analysis and single crystal X-ray diffraction analysis. Crystal analysis reveals that compound 1 exhibits a 2-D double layered framework structure constructed from [SiW12O40]4− and copper-aqua-2,2′-bipy-hydroxyl-isonicotinate complexes. Compound 2 is a 0-D discrete structure formed by [SiW12O40]4− and copper-chloro-isonicotinate-phenanthroline complexes. Compound 3 shows a 1-D single chain structure based on the linkage of copper-2,2-bpy-chloro-2-hydroxy-nicotinate complexes and [SiW12O40]4−. Compounds 4 and 5 both contain polyoxometalate supported transition metal complexes, one is a polyoxometalate supported copper-chloro-nicotinate-phenanthroline complex in 4, and the other is a polyoxometalate supported copper-2,2-bpy-chloro-nicotinate complex in 5. It should be noted that nicotinic, isonicotinic and picolinic acids are structural isomers and 2-hydroxy-nicotinic acid is an in situ hydroxylated product of nicotinic acid. In addition, photocatalytic degradation of Rhodamine B (RhB) by compounds 1–5 has been investigated in aqueous solutions. Five new organic-inorganic hybrid compounds based on the Keggin-type polyoxoanion [SiW sub(12)O sub(40)] super(4-), namely [Cu sub(3)(2,2'-bpy) sub(3)(inic)( mu sub(2)-OH)(H sub(2)O)][SiW sub(12)O sub(40)]. 2H sub(2)O (1), [Cu sub(6)(phen) sub(6)( mu sub(3)-Cl) sub(2)( mu sub(2)-Cl) sub(2)Cl sub(2)(inic) sub(2)][SiW sub(12)O sub(40)].6H sub(2)O (2), [Cu sub(2)(hnic)(2,2'-bpy) sub(2)Cl] sub(2)[H sub(2)SiW sub(12)O sub(40)] (3), [Cu sub(2)(nic)(phen) sub(2)Cl sub(2)] sub(2)[SiW sub(12)O sub(40)] (4) and [Cu sub(2)(pic)(2,2'-bpy) sub(2)Cl] sub(2)[SiW sub(12)O sub(40)] (5) (inic = isonicotinic acid, hnic = 2-hydroxy-nicotinic acid, nic = nicotinic acid, pic = picolinic acid, 2,2'-bpy = 2,2'-bipyridine, phen = 1,10-phenanthroline) have been synthesized and characterized by IR, UV-Vis, XPS, XRD, cyclic voltammetric measurements, photoluminescence analysis and single crystal X-ray diffraction analysis. Crystal analysis reveals that compound 1 exhibits a 2-D double layered framework structure constructed from [SiW sub(12)O sub(40)] super(4-) and copper-aqua-2,2'-bipy-hydroxyl-isonicotinate complexes. Compound 2 is a 0-D discrete structure formed by [SiW sub(12)O sub(40)] super(4-) and copper-chloro-isonicotinate-phenanthroline complexes. Compound 3 shows a 1-D single chain structure based on the linkage of copper-2,2-bpy-chloro-2-hydroxy-nicotinate complexes and [SiW sub(12)O sub(40)] super(4-). Compounds 4 and 5 both contain polyoxometalate supported transition metal complexes, one is a polyoxometalate supported copper-chloro-nicotinate-phenanthroline complex in 4, and the other is a polyoxometalate supported copper-2,2-bpy-chloro-nicotinate complex in 5. It should be noted that nicotinic, isonicotinic and picolinic acids are structural isomers and 2-hydroxy-nicotinic acid is an in situ hydroxylated product of nicotinic acid. In addition, photocatalytic degradation of Rhodamine B (RhB) by compounds 1-5 has been investigated in aqueous solutions. Five new organic–inorganic hybrid compounds based on the Keggin-type polyoxoanion [SiW 12 O 40 ] 4− , namely [Cu 3 (2,2′-bpy) 3 (inic)(μ 2 -OH)(H 2 O)][SiW 12 O 40 ]·2H 2 O ( 1 ), [Cu 6 (phen) 6 (μ 3 -Cl) 2 (μ 2 -Cl) 2 Cl 2 (inic) 2 ][SiW 12 O 40 ]·6H 2 O ( 2 ), [Cu 2 (hnic)(2,2′-bpy) 2 Cl] 2 [H 2 SiW 12 O 40 ] ( 3 ), [Cu 2 (nic)(phen) 2 Cl 2 ] 2 [SiW 12 O 40 ] ( 4 ) and [Cu 2 (pic)(2,2′-bpy) 2 Cl] 2 [SiW 12 O 40 ] ( 5 ) (inic = isonicotinic acid, hnic = 2-hydroxy-nicotinic acid, nic = nicotinic acid, pic = picolinic acid, 2,2′-bpy = 2,2′-bipyridine, phen = 1,10-phenanthroline) have been synthesized and characterized by IR, UV-Vis, XPS, XRD, cyclic voltammetric measurements, photoluminescence analysis and single crystal X-ray diffraction analysis. Crystal analysis reveals that compound 1 exhibits a 2-D double layered framework structure constructed from [SiW 12 O 40 ] 4− and copper-aqua-2,2′-bipy-hydroxyl-isonicotinate complexes. Compound 2 is a 0-D discrete structure formed by [SiW 12 O 40 ] 4− and copper-chloro-isonicotinate-phenanthroline complexes. Compound 3 shows a 1-D single chain structure based on the linkage of copper-2,2-bpy-chloro-2-hydroxy-nicotinate complexes and [SiW 12 O 40 ] 4− . Compounds 4 and 5 both contain polyoxometalate supported transition metal complexes, one is a polyoxometalate supported copper-chloro-nicotinate-phenanthroline complex in 4 , and the other is a polyoxometalate supported copper-2,2-bpy-chloro-nicotinate complex in 5 . It should be noted that nicotinic, isonicotinic and picolinic acids are structural isomers and 2-hydroxy-nicotinic acid is an in situ hydroxylated product of nicotinic acid. In addition, photocatalytic degradation of Rhodamine B (RhB) by compounds 1–5 has been investigated in aqueous solutions. |
Author | Zhang, Xiao Huo, Qi-Sheng Ding, Hong Guo, Hai-Yang Hu, Yang-Yang Cui, Xiao-Bing Zhao, De-Chuan Xu, Ji-Qing |
Author_xml | – sequence: 1 givenname: De-Chuan surname: Zhao fullname: Zhao, De-Chuan email: cuixb@mail.jlu.edu.cn organization: College of Chemistry and State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun, Jilin 130023, China. cuixb@mail.jlu.edu.cn – sequence: 2 givenname: Yang-Yang surname: Hu fullname: Hu, Yang-Yang – sequence: 3 givenname: Hong surname: Ding fullname: Ding, Hong – sequence: 4 givenname: Hai-Yang surname: Guo fullname: Guo, Hai-Yang – sequence: 5 givenname: Xiao-Bing surname: Cui fullname: Cui, Xiao-Bing – sequence: 6 givenname: Xiao surname: Zhang fullname: Zhang, Xiao – sequence: 7 givenname: Qi-Sheng surname: Huo fullname: Huo, Qi-Sheng – sequence: 8 givenname: Ji-Qing surname: Xu fullname: Xu, Ji-Qing |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/25882351$$D View this record in MEDLINE/PubMed |
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PublicationTitleAlternate | Dalton Trans |
PublicationYear | 2015 |
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Snippet | Five new organic–inorganic hybrid compounds based on the Keggin-type polyoxoanion [SiW12O40]4−, namely [Cu3(2,2′-bpy)3(inic)(μ2-OH)(H2O)][SiW12O40]·2H2O (1),... Five new organic–inorganic hybrid compounds based on the Keggin-type polyoxoanion [SiW 12 O 40 ] 4− , namely [Cu 3 (2,2′-bpy) 3 (inic)(μ 2 -OH)(H 2 O)][SiW 12... Five new organic-inorganic hybrid compounds based on the Keggin-type polyoxoanion [SiW sub(12)O sub(40)] super(4-), namely [Cu sub(3)(2,2'-bpy) sub(3)(inic)(... |
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SubjectTerms | Carboxylic Acids - chemistry Chains Crystallography, X-Ray Degradation Diffraction Isomers Ligands Models, Molecular Molecular Structure Nicotinic acid Organometallic Compounds - chemical synthesis Organometallic Compounds - chemistry Pyridines - chemistry Rhodamine Transition Elements - chemistry Transition metals Tungsten Compounds - chemistry X-ray photoelectron spectroscopy |
Title | Polyoxometalate-based organic-inorganic hybrid compounds containing transition metal mixed-organic-ligand complexes of N-containing and pyridinecarboxylate ligands |
URI | https://www.ncbi.nlm.nih.gov/pubmed/25882351 https://search.proquest.com/docview/1680193283 https://search.proquest.com/docview/1692331007 |
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