Unraveling synergistic mixing of SnO2–TiO2 composite as anode for Li-ion battery and their electrochemical properties
The effect of Sn/Ti ratio on the electrochemical properties of the anode is studied in Sn-doped TiO 2 and SnO 2 –TiO 2 nanofibers synthesized using a pilot-scale electrospinning system. Changes in the lattice structure of TiO 2 due to the presence of Sn are studied through X-ray diffraction and high...
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| Published in | Journal of materials research Vol. 36; no. 20; pp. 4120 - 4130 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cham
Springer International Publishing
28.10.2021
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The effect of Sn/Ti ratio on the electrochemical properties of the anode is studied in Sn-doped TiO
2
and SnO
2
–TiO
2
nanofibers synthesized using a pilot-scale electrospinning system. Changes in the lattice structure of TiO
2
due to the presence of Sn are studied through X-ray diffraction and high-resolution transmission electron microscopy. Lowering of electrochemical potential (vs Li/Li
+
) is observed alongside the enhanced capacity (400–600 mAh g
−1
) with increasing Sn content. Formation of SnO
2
grain in sample with high Sn content (70 wt%) shows detrimental effect on cycling stability due to severe volume changes during lithiation/delithiation. We show that the relative fraction of TiO
2
and SnO
2
framework determines whether the composite is high capacity or high stability. In overall, SnO
2
–TiO
2
composite anode with optimized Sn/Ti ratio can be used for high energy density, cycling stability and working potential lithium-ion battery.
Graphic abstract
The relative fraction of TiO
2
and SnO
2
framework determines whether the composite is high capacity or high stability |
|---|---|
| AbstractList | The effect of Sn/Ti ratio on the electrochemical properties of the anode is studied in Sn-doped TiO
2
and SnO
2
–TiO
2
nanofibers synthesized using a pilot-scale electrospinning system. Changes in the lattice structure of TiO
2
due to the presence of Sn are studied through X-ray diffraction and high-resolution transmission electron microscopy. Lowering of electrochemical potential (vs Li/Li
+
) is observed alongside the enhanced capacity (400–600 mAh g
−1
) with increasing Sn content. Formation of SnO
2
grain in sample with high Sn content (70 wt%) shows detrimental effect on cycling stability due to severe volume changes during lithiation/delithiation. We show that the relative fraction of TiO
2
and SnO
2
framework determines whether the composite is high capacity or high stability. In overall, SnO
2
–TiO
2
composite anode with optimized Sn/Ti ratio can be used for high energy density, cycling stability and working potential lithium-ion battery.
Graphic abstract
The relative fraction of TiO
2
and SnO
2
framework determines whether the composite is high capacity or high stability The effect of Sn/Ti ratio on the electrochemical properties of the anode is studied in Sn-doped TiO2 and SnO2–TiO2 nanofibers synthesized using a pilot-scale electrospinning system. Changes in the lattice structure of TiO2 due to the presence of Sn are studied through X-ray diffraction and high-resolution transmission electron microscopy. Lowering of electrochemical potential (vs Li/Li+) is observed alongside the enhanced capacity (400–600 mAh g−1) with increasing Sn content. Formation of SnO2 grain in sample with high Sn content (70 wt%) shows detrimental effect on cycling stability due to severe volume changes during lithiation/delithiation. We show that the relative fraction of TiO2 and SnO2 framework determines whether the composite is high capacity or high stability. In overall, SnO2–TiO2 composite anode with optimized Sn/Ti ratio can be used for high energy density, cycling stability and working potential lithium-ion battery.Graphic abstractThe relative fraction of TiO2 and SnO2 framework determines whether the composite is high capacity or high stability |
| Author | Yang, Chun-Chen Jose, Rajan Pal, Bhupender Ling, JinKiong Karuppiah, Chelladurai Reddy, M. V. |
| Author_xml | – sequence: 1 givenname: JinKiong surname: Ling fullname: Ling, JinKiong organization: Nanostructured Renewable Energy Material Laboratory, Faculty of Industrial Sciences & Technology, Universiti Malaysia Pahang – sequence: 2 givenname: Chelladurai surname: Karuppiah fullname: Karuppiah, Chelladurai organization: Battery Research Center for Green Energy (BRCGE), Ming Chi University of Technology – sequence: 3 givenname: M. V. surname: Reddy fullname: Reddy, M. V. organization: Centre of Excellent in Transportation Electrification and Energy Storage (CETEES), Institute of Research Hydro-Québec – sequence: 4 givenname: Bhupender surname: Pal fullname: Pal, Bhupender organization: Nanostructured Renewable Energy Material Laboratory, Faculty of Industrial Sciences & Technology, Universiti Malaysia Pahang, Department of Inorganic Chemistry, University of Chemistry and Technology Prague – sequence: 5 givenname: Chun-Chen surname: Yang fullname: Yang, Chun-Chen organization: Battery Research Center for Green Energy (BRCGE), Ming Chi University of Technology – sequence: 6 givenname: Rajan orcidid: 0000-0003-4540-321X surname: Jose fullname: Jose, Rajan email: rjose@ump.edu.my organization: Nanostructured Renewable Energy Material Laboratory, Faculty of Industrial Sciences & Technology, Universiti Malaysia Pahang |
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| Snippet | The effect of Sn/Ti ratio on the electrochemical properties of the anode is studied in Sn-doped TiO
2
and SnO
2
–TiO
2
nanofibers synthesized using a... The effect of Sn/Ti ratio on the electrochemical properties of the anode is studied in Sn-doped TiO2 and SnO2–TiO2 nanofibers synthesized using a pilot-scale... |
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| SubjectTerms | Applied and Technical Physics Biomaterials Chemistry and Materials Science Cycles Electrochemical analysis Electrochemical potential High resolution electron microscopy Inorganic Chemistry Invited Paper Lithium-ion batteries Materials Engineering Materials research Materials Science Nanofibers Nanotechnology Rechargeable batteries Stability Tin Tin dioxide Titanium dioxide |
| Title | Unraveling synergistic mixing of SnO2–TiO2 composite as anode for Li-ion battery and their electrochemical properties |
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