Optimization Extraction of Scandium from Scandium Concentrate with Titanium Dioxide Wastewater by Response Surface Methodology
Scandium concentrate and titanium dioxide wastewater (TDWW) all belong to waste, especially TDWW belongs to hazardous waste, it is urgent to find a more efficient and safer treatment method to deal with them, and both waste acid and waste ore contain scandium. The use of waste acid as a leaching age...
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| Published in | Journal of sustainable metallurgy Vol. 10; no. 1; pp. 278 - 295 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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Cham
Springer International Publishing
01.03.2024
Springer Nature B.V |
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| Abstract | Scandium concentrate and titanium dioxide wastewater (TDWW) all belong to waste, especially TDWW belongs to hazardous waste, it is urgent to find a more efficient and safer treatment method to deal with them, and both waste acid and waste ore contain scandium. The use of waste acid as a leaching agent can achieve the synergistic recovery effect of scandium. First, the leaching temperature, time, and liquid–solid ratio are found to be significant factors through single-factor tests. Then, the test program is designed by using the Box Behnken unit of Design Expert software to explore the relationship between each factor including leaching temperature (℃), leaching time (h), and liquid-to-solid ratio (mL/g). The results show that the interaction between leaching time and liquid–solid ratio was the strongest. The second-order regression model equation generated by the software can well predict the leaching effect of scandium. The scandium leaching efficiency reaches 85.30%, and the scandium content in the leaching residue decreases to 10.24 g/t under the optimal conditions: leaching temperature of 70 ℃, leaching time of 2.0 h, and liquid–solid ratio 8.7 mL/g. The finite element analysis is to simulate the mineral roasting process and the temperature field changes are always present.
Graphical Abstract |
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| AbstractList | Scandium concentrate and titanium dioxide wastewater (TDWW) all belong to waste, especially TDWW belongs to hazardous waste, it is urgent to find a more efficient and safer treatment method to deal with them, and both waste acid and waste ore contain scandium. The use of waste acid as a leaching agent can achieve the synergistic recovery effect of scandium. First, the leaching temperature, time, and liquid–solid ratio are found to be significant factors through single-factor tests. Then, the test program is designed by using the Box Behnken unit of Design Expert software to explore the relationship between each factor including leaching temperature (℃), leaching time (h), and liquid-to-solid ratio (mL/g). The results show that the interaction between leaching time and liquid–solid ratio was the strongest. The second-order regression model equation generated by the software can well predict the leaching effect of scandium. The scandium leaching efficiency reaches 85.30%, and the scandium content in the leaching residue decreases to 10.24 g/t under the optimal conditions: leaching temperature of 70 ℃, leaching time of 2.0 h, and liquid–solid ratio 8.7 mL/g. The finite element analysis is to simulate the mineral roasting process and the temperature field changes are always present.
Graphical Abstract Scandium concentrate and titanium dioxide wastewater (TDWW) all belong to waste, especially TDWW belongs to hazardous waste, it is urgent to find a more efficient and safer treatment method to deal with them, and both waste acid and waste ore contain scandium. The use of waste acid as a leaching agent can achieve the synergistic recovery effect of scandium. First, the leaching temperature, time, and liquid–solid ratio are found to be significant factors through single-factor tests. Then, the test program is designed by using the Box Behnken unit of Design Expert software to explore the relationship between each factor including leaching temperature (℃), leaching time (h), and liquid-to-solid ratio (mL/g). The results show that the interaction between leaching time and liquid–solid ratio was the strongest. The second-order regression model equation generated by the software can well predict the leaching effect of scandium. The scandium leaching efficiency reaches 85.30%, and the scandium content in the leaching residue decreases to 10.24 g/t under the optimal conditions: leaching temperature of 70 ℃, leaching time of 2.0 h, and liquid–solid ratio 8.7 mL/g. The finite element analysis is to simulate the mineral roasting process and the temperature field changes are always present. |
| Author | Xiao, Junhui Cheng, Renju Zhang, Junhui Zhong, Nanlan |
| Author_xml | – sequence: 1 givenname: Junhui orcidid: 0000-0002-1256-2196 surname: Xiao fullname: Xiao, Junhui email: xiaojunhui33@163.com organization: School of Environment and Resource, Southwest University of Science and Technology, Technology Innovation Center for Comprehensive Utilization of Strategic Mineral Resources, Ministry of Natural Resources, Chinese Academy of Geological Sciences, Applied Technology Innovation Center of Rare Earth Resources, China Geological Survey, Institute of Multipurpose Utilization of Mineral Resources, Chinese Academy of Geological Sciences, Dongfang Boiler Group Co., Ltd., Sichuan Provincial Engineering Lab of Nonmetallic Mineral Powder Modification and High-Value Utilization, Southwest University of Science and Technology, Key Laboratory of Ministry of Education for Solid Waste Treatment and Resource Recycle, Southwest University of Science and Technology – sequence: 2 givenname: Nanlan surname: Zhong fullname: Zhong, Nanlan organization: School of Environment and Resource, Southwest University of Science and Technology – sequence: 3 givenname: Renju surname: Cheng fullname: Cheng, Renju organization: Technology Innovation Center for Comprehensive Utilization of Strategic Mineral Resources, Ministry of Natural Resources, Chinese Academy of Geological Sciences, Applied Technology Innovation Center of Rare Earth Resources, China Geological Survey, Institute of Multipurpose Utilization of Mineral Resources, Chinese Academy of Geological Sciences – sequence: 4 givenname: Junhui surname: Zhang fullname: Zhang, Junhui organization: Technology Innovation Center for Comprehensive Utilization of Strategic Mineral Resources, Ministry of Natural Resources, Chinese Academy of Geological Sciences, Applied Technology Innovation Center of Rare Earth Resources, China Geological Survey, Institute of Multipurpose Utilization of Mineral Resources, Chinese Academy of Geological Sciences |
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| Snippet | Scandium concentrate and titanium dioxide wastewater (TDWW) all belong to waste, especially TDWW belongs to hazardous waste, it is urgent to find a more... |
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| SubjectTerms | Earth and Environmental Science Environment Finite element method Hazardous wastes Leaching Metallic Materials Regression models Research Article Response surface methodology Scandium Software Sustainable Development Temperature distribution Titanium Titanium dioxide Wastewater |
| Title | Optimization Extraction of Scandium from Scandium Concentrate with Titanium Dioxide Wastewater by Response Surface Methodology |
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