One-pot synthesis of MoS2–CNx–metal oxide hetero structures and their synergistic role towards efficient oxygen reduction reaction
Two-dimensional transition metal dichalcogenides are at the forefront of materials research due to their exceptional catalytic, electronic and chemical properties. Herein, we developed a unique heterointerface comprising MoS 2 /CN x /metal oxide (Fe, Co, Ni) to scrutinize the effects of metal oxide...
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| Published in | Journal of materials research Vol. 38; no. 7; pp. 1824 - 1831 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cham
Springer International Publishing
14.04.2023
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Two-dimensional transition metal dichalcogenides are at the forefront of materials research due to their exceptional catalytic, electronic and chemical properties. Herein, we developed a unique heterointerface comprising MoS
2
/CN
x
/metal oxide (Fe, Co, Ni) to scrutinize the effects of metal oxide anchored within MoS
2
layers towards oxygen reduction reaction and catalyst durability. MoS
2
/CN
x
/metal oxide (Fe,Co,Ni) is prepared by a solution combustion method (one-step process). Surface properties and morphology are investigated by various surface probing techniques viz. FT-IR, Raman, XRD, EDAX and TEM. Results revealed that upon MoS
2
integration onto the metal oxides, the ORR activity was found to be significantly enhanced. Further, MoS
2
–CN
x
–FeO
x
matrix retains more than 50% of initial ORR activity at − 0.2 V and is more durable than pristine MoS
2
. The mass activity of metal oxide appreciably improved when combined with MoS
2
. The mass-specific current density towards ORR at − 0.4 V of the catalysts MoS
2
, MoS
2
/CN
x
/FeO
x
, MoS
2
/CN
x
/CoO
x
and MoS
2
/CN
x
/NiO
x
are − 0.5 mA cm
−2
, − 0.7 mA cm
−2
, − 0.42 mA cm
−2
and 0.23 mA cm
−2
respectively.
Graphical abstract |
|---|---|
| AbstractList | Two-dimensional transition metal dichalcogenides are at the forefront of materials research due to their exceptional catalytic, electronic and chemical properties. Herein, we developed a unique heterointerface comprising MoS2/CNx/metal oxide (Fe, Co, Ni) to scrutinize the effects of metal oxide anchored within MoS2 layers towards oxygen reduction reaction and catalyst durability. MoS2/CNx/metal oxide (Fe,Co,Ni) is prepared by a solution combustion method (one-step process). Surface properties and morphology are investigated by various surface probing techniques viz. FT-IR, Raman, XRD, EDAX and TEM. Results revealed that upon MoS2 integration onto the metal oxides, the ORR activity was found to be significantly enhanced. Further, MoS2–CNx–FeOx matrix retains more than 50% of initial ORR activity at − 0.2 V and is more durable than pristine MoS2. The mass activity of metal oxide appreciably improved when combined with MoS2. The mass-specific current density towards ORR at − 0.4 V of the catalysts MoS2, MoS2/CNx/FeOx, MoS2/CNx/CoOx and MoS2/CNx/NiOx are − 0.5 mA cm−2, − 0.7 mA cm−2, − 0.42 mA cm−2 and 0.23 mA cm−2 respectively. Two-dimensional transition metal dichalcogenides are at the forefront of materials research due to their exceptional catalytic, electronic and chemical properties. Herein, we developed a unique heterointerface comprising MoS 2 /CN x /metal oxide (Fe, Co, Ni) to scrutinize the effects of metal oxide anchored within MoS 2 layers towards oxygen reduction reaction and catalyst durability. MoS 2 /CN x /metal oxide (Fe,Co,Ni) is prepared by a solution combustion method (one-step process). Surface properties and morphology are investigated by various surface probing techniques viz. FT-IR, Raman, XRD, EDAX and TEM. Results revealed that upon MoS 2 integration onto the metal oxides, the ORR activity was found to be significantly enhanced. Further, MoS 2 –CN x –FeO x matrix retains more than 50% of initial ORR activity at − 0.2 V and is more durable than pristine MoS 2 . The mass activity of metal oxide appreciably improved when combined with MoS 2 . The mass-specific current density towards ORR at − 0.4 V of the catalysts MoS 2 , MoS 2 /CN x /FeO x , MoS 2 /CN x /CoO x and MoS 2 /CN x /NiO x are − 0.5 mA cm −2 , − 0.7 mA cm −2 , − 0.42 mA cm −2 and 0.23 mA cm −2 respectively. Graphical abstract |
| Author | Prabhakaran, Dhanasekaran Alwarappan, Subbiah Bhat, Santoshkumar Dattatray Subramanian, Mohana Priya Sakthivel, Arunkumar |
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| Cites_doi | 10.1039/C9TA01321K 10.1021/acs.chemmater.7b00745 10.1021/acsami.7b05104 10.1016/j.jcis.2020.01.109 10.1016/j.jcis.2020.03.078 10.1021/acsami.5b08420 10.1021/acsami.0c14464 10.1016/j.ijhydene.2018.01.104 10.1002/adfm.201910302 10.1038/s41598-019-50780-2 10.1016/j.bios.2019.03.005 10.1039/b909451b 10.1016/j.jelechem.2019.03.036 10.1016/j.apsusc.2018.01.030 10.1021/acscatal.7b02739 10.17344/acsi.2016.2305 10.1021/acs.chemmater.5b02902 10.1007/s11356-020-12231-8 10.1021/acsami.9b05086 10.1039/C4RA11852A 10.1039/C7TA02077E 10.1039/c0ee00033g 10.1039/C6RA04120E 10.1039/C6RA16058A 10.1016/j.electacta.2015.06.119 10.1039/D2SC01398C 10.1039/D1RA03552E 10.1002/smll.201804545 10.1557/jmr.2006.0118 10.1016/j.jmmm.2011.11.065 10.1155/2014/723057 10.1016/j.electacta.2016.12.144 10.1039/C7RA12897E 10.1149/2.0021915jes 10.1557/jmr.2017.282 10.1016/j.enchem.2021.100061 10.1016/j.rinp.2019.01.005 10.1038/s41598-018-31354-0 10.1016/j.electacta.2014.11.053 |
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| SubjectTerms | Applied and Technical Physics Biomaterials Catalysts Chemical properties Chemical reduction Chemistry and Materials Science Cobalt oxides Durability Inorganic Chemistry Invited Paper Iron Materials Engineering Materials research Materials Science Metal oxides Molybdenum disulfide Nanotechnology Nickel Oxygen reduction reactions Surface properties Transition metal compounds |
| Title | One-pot synthesis of MoS2–CNx–metal oxide hetero structures and their synergistic role towards efficient oxygen reduction reaction |
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