Introducing an Electrochemical Sensor Based on Two Layers of Ag Nanoparticles Decorated Graphene for Rapid Determination of Methadone in Human Blood Serum
In the present study, a highly efficient electrochemical sensor for methadone measurement through the use of a glassy carbon electrode modified with two layers of graphene/Ag nanoparticles ((Gr/AgNPs) 2 /GCE) nanocomposite is introduced. The morphological, elemental and electrochemical properties of...
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| Published in | Topics in catalysis Vol. 65; no. 5-6; pp. 623 - 632 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.04.2022
Springer Nature B.V |
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| Online Access | Get full text |
| ISSN | 1022-5528 1572-9028 |
| DOI | 10.1007/s11244-021-01483-4 |
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| Abstract | In the present study, a highly efficient electrochemical sensor for methadone measurement through the use of a glassy carbon electrode modified with two layers of graphene/Ag nanoparticles ((Gr/AgNPs)
2
/GCE) nanocomposite is introduced. The morphological, elemental and electrochemical properties of the as-prepared nanocomposite were evaluated by scanning electron microscopy, energy dispersive spectroscopy. The influence of different experimental parameters such as pH and scan rate on the voltammetric response of methadone was also addressed. Exhibiting a peak potential at + 0.79 V (vs. Ag/AgCl), the as-prepared electrode manifested an improvement in its catalytic activity toward methadone oxidation. Under optimal conditions, the developed sensor exhibited an excellent response toward methadone in the concentration range of 1.0–200.0 µM with a detection limit of 0.12 µM. Moreover, the proposed electrode offered superior selectivity for methadone reflecting its efficiency for the real samples such as human blood serum. |
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| AbstractList | In the present study, a highly efficient electrochemical sensor for methadone measurement through the use of a glassy carbon electrode modified with two layers of graphene/Ag nanoparticles ((Gr/AgNPs)
2
/GCE) nanocomposite is introduced. The morphological, elemental and electrochemical properties of the as-prepared nanocomposite were evaluated by scanning electron microscopy, energy dispersive spectroscopy. The influence of different experimental parameters such as pH and scan rate on the voltammetric response of methadone was also addressed. Exhibiting a peak potential at + 0.79 V (vs. Ag/AgCl), the as-prepared electrode manifested an improvement in its catalytic activity toward methadone oxidation. Under optimal conditions, the developed sensor exhibited an excellent response toward methadone in the concentration range of 1.0–200.0 µM with a detection limit of 0.12 µM. Moreover, the proposed electrode offered superior selectivity for methadone reflecting its efficiency for the real samples such as human blood serum. In the present study, a highly efficient electrochemical sensor for methadone measurement through the use of a glassy carbon electrode modified with two layers of graphene/Ag nanoparticles ((Gr/AgNPs)2/GCE) nanocomposite is introduced. The morphological, elemental and electrochemical properties of the as-prepared nanocomposite were evaluated by scanning electron microscopy, energy dispersive spectroscopy. The influence of different experimental parameters such as pH and scan rate on the voltammetric response of methadone was also addressed. Exhibiting a peak potential at + 0.79 V (vs. Ag/AgCl), the as-prepared electrode manifested an improvement in its catalytic activity toward methadone oxidation. Under optimal conditions, the developed sensor exhibited an excellent response toward methadone in the concentration range of 1.0–200.0 µM with a detection limit of 0.12 µM. Moreover, the proposed electrode offered superior selectivity for methadone reflecting its efficiency for the real samples such as human blood serum. |
| Author | Baghayeri, Mehdi Nabavi, Samaneh Hasheminejad, Ehteram Ebrahimi, Vida |
| Author_xml | – sequence: 1 givenname: Mehdi orcidid: 0000-0003-3004-1324 surname: Baghayeri fullname: Baghayeri, Mehdi email: m.baghayeri@hsu.ac.ir organization: Department of Chemistry, Faculty of Science, Hakim Sabzevari University – sequence: 2 givenname: Samaneh surname: Nabavi fullname: Nabavi, Samaneh email: samanenabavifard@yahoo.com organization: Research Institute of Police Science and Social Studies – sequence: 3 givenname: Ehteram surname: Hasheminejad fullname: Hasheminejad, Ehteram organization: Young Researchers and Elite Club, Sabzevar Branch, Islamic Azad University – sequence: 4 givenname: Vida surname: Ebrahimi fullname: Ebrahimi, Vida organization: Department of Chemistry, Faculty of Science, Hakim Sabzevari University |
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| Snippet | In the present study, a highly efficient electrochemical sensor for methadone measurement through the use of a glassy carbon electrode modified with two layers... |
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| SubjectTerms | Blood Catalysis Catalytic activity Characterization and Evaluation of Materials Chemical sensors Chemistry Chemistry and Materials Science Electrochemical analysis Electrodes Glassy carbon Graphene Industrial Chemistry/Chemical Engineering Methadone Nanocomposites Nanoparticles Original Paper Oxidation Pharmacy Physical Chemistry Selectivity Sensors Silver |
| Title | Introducing an Electrochemical Sensor Based on Two Layers of Ag Nanoparticles Decorated Graphene for Rapid Determination of Methadone in Human Blood Serum |
| URI | https://link.springer.com/article/10.1007/s11244-021-01483-4 https://www.proquest.com/docview/2655135233 |
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