Optimal current density for cathodic CeCC deposition on anodized AA2024-T3 aircraft alloy

The reliable and durable corrosion protection of structural materials, such as the AA2024-T3 aircraft alloy, is the subject of intensive research worldwide. This alloy, highly doped in its composition, inherently exhibits increased susceptibility to electrochemical corrosion compared to pure aluminu...

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Published inJournal of applied electrochemistry Vol. 54; no. 12; pp. 2887 - 2918
Main Authors Kozhukharov, Stephan, Girginov, Christian, Portolesi, Stefania, Tsanev, Aleksandar, Lilova, Vanya, Petkov, Plamen
Format Journal Article
LanguageEnglish
Published Dordrecht Springer Netherlands 01.12.2024
Springer Nature B.V
Subjects
Aircraft
Aluminum
Aluminum base alloys
Aluminum oxide
Anodic protection
Cathodic protection
Cerium
Chemistry
Chemistry and Materials Science
Contact angle
Conversion coatings
Corrosion prevention
Corrosion tests
Current density
Deposition
Electrochemical corrosion
Electrochemical impedance spectroscopy
Electrochemistry
Energy distribution
Industrial Chemistry/Chemical Engineering
Photoelectrons
Physical Chemistry
Primers (coatings)
Research Article
Spectrum analysis
Surface properties
X ray photoelectron spectroscopy
AA2024-T3 aircraft alloy
Cerium conversion coatings (CeCC) electrodeposition currents
Anodic aluminum oxide (AAO)
Surface characteristics
EIS
PDS
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Abstract The reliable and durable corrosion protection of structural materials, such as the AA2024-T3 aircraft alloy, is the subject of intensive research worldwide. This alloy, highly doped in its composition, inherently exhibits increased susceptibility to electrochemical corrosion compared to pure aluminum. Among the most promising and environmentally friendly primers are Anodic Aluminum Oxide (AAO) and Cerium Conversion Coatings (CeCC). Consequently, the combined AAO/CeCC coating primers are anticipated to offer superior protective properties. However, the optimal approach and conditions for CeCC formation on the AAO layer remain uncertain. This study presents a comparative characterization of cathodically deposited CeCC on pre-formed AAO on the AA2024-T3 alloy, revealing the opportunity for electrochemical CeCC formation and potential detrimental effects. The CeCC depositions were conducted at current densities ranging from 0 to 25 mA cm −2 . The analysis included the following: (1) color characterization and contact angle measurements, (2) surface observations using optical metallographic, atomic force, and scanning electron microscopy, (3) element distribution using energy dispersion X-ray and X-ray photoelectron spectroscopy, and (4) corrosion tests. These involved electrochemical impedance spectroscopy (EIS) and potentiodynamic scanning after 24, 168, 336, 504, and 672 h of exposure to a 3.5% NaCl model corrosive medium. The result analysis has revealed that the most favorable current densities for CeCC deposition on the surface of anodized AA2024-T3 alloy fall within the range of 0 to 5 mA cm −2 . Higher values adversely affect the surface properties of the specimens. These findings were corroborated by all the analytical techniques employed. Graphical abstract
AbstractList The reliable and durable corrosion protection of structural materials, such as the AA2024-T3 aircraft alloy, is the subject of intensive research worldwide. This alloy, highly doped in its composition, inherently exhibits increased susceptibility to electrochemical corrosion compared to pure aluminum. Among the most promising and environmentally friendly primers are Anodic Aluminum Oxide (AAO) and Cerium Conversion Coatings (CeCC). Consequently, the combined AAO/CeCC coating primers are anticipated to offer superior protective properties. However, the optimal approach and conditions for CeCC formation on the AAO layer remain uncertain. This study presents a comparative characterization of cathodically deposited CeCC on pre-formed AAO on the AA2024-T3 alloy, revealing the opportunity for electrochemical CeCC formation and potential detrimental effects. The CeCC depositions were conducted at current densities ranging from 0 to 25 mA cm−2. The analysis included the following: (1) color characterization and contact angle measurements, (2) surface observations using optical metallographic, atomic force, and scanning electron microscopy, (3) element distribution using energy dispersion X-ray and X-ray photoelectron spectroscopy, and (4) corrosion tests. These involved electrochemical impedance spectroscopy (EIS) and potentiodynamic scanning after 24, 168, 336, 504, and 672 h of exposure to a 3.5% NaCl model corrosive medium. The result analysis has revealed that the most favorable current densities for CeCC deposition on the surface of anodized AA2024-T3 alloy fall within the range of 0 to 5 mA cm−2. Higher values adversely affect the surface properties of the specimens. These findings were corroborated by all the analytical techniques employed.
The reliable and durable corrosion protection of structural materials, such as the AA2024-T3 aircraft alloy, is the subject of intensive research worldwide. This alloy, highly doped in its composition, inherently exhibits increased susceptibility to electrochemical corrosion compared to pure aluminum. Among the most promising and environmentally friendly primers are Anodic Aluminum Oxide (AAO) and Cerium Conversion Coatings (CeCC). Consequently, the combined AAO/CeCC coating primers are anticipated to offer superior protective properties. However, the optimal approach and conditions for CeCC formation on the AAO layer remain uncertain. This study presents a comparative characterization of cathodically deposited CeCC on pre-formed AAO on the AA2024-T3 alloy, revealing the opportunity for electrochemical CeCC formation and potential detrimental effects. The CeCC depositions were conducted at current densities ranging from 0 to 25 mA cm −2 . The analysis included the following: (1) color characterization and contact angle measurements, (2) surface observations using optical metallographic, atomic force, and scanning electron microscopy, (3) element distribution using energy dispersion X-ray and X-ray photoelectron spectroscopy, and (4) corrosion tests. These involved electrochemical impedance spectroscopy (EIS) and potentiodynamic scanning after 24, 168, 336, 504, and 672 h of exposure to a 3.5% NaCl model corrosive medium. The result analysis has revealed that the most favorable current densities for CeCC deposition on the surface of anodized AA2024-T3 alloy fall within the range of 0 to 5 mA cm −2 . Higher values adversely affect the surface properties of the specimens. These findings were corroborated by all the analytical techniques employed. Graphical abstract
Author Kozhukharov, Stephan
Portolesi, Stefania
Tsanev, Aleksandar
Girginov, Christian
Lilova, Vanya
Petkov, Plamen
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  givenname: Christian
  surname: Girginov
  fullname: Girginov, Christian
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  givenname: Stefania
  surname: Portolesi
  fullname: Portolesi, Stefania
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  surname: Petkov
  fullname: Petkov, Plamen
  organization: Department of Physics, University of Chemical Technology and Metallurgy
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CitedBy_id crossref_primary_10_3390_ma18020424
crossref_primary_10_3390_met15010020
crossref_primary_10_1016_j_matchemphys_2024_130226
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Keywords AA2024-T3 aircraft alloy
Cerium conversion coatings (CeCC) electrodeposition currents
Anodic aluminum oxide (AAO)
Surface characteristics
EIS
PDS
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PublicationTitle Journal of applied electrochemistry
PublicationTitleAbbrev J Appl Electrochem
PublicationYear 2024
Publisher Springer Netherlands
Springer Nature B.V
Publisher_xml – name: Springer Netherlands
– name: Springer Nature B.V
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Snippet The reliable and durable corrosion protection of structural materials, such as the AA2024-T3 aircraft alloy, is the subject of intensive research worldwide....
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SubjectTerms Aircraft
Aluminum
Aluminum base alloys
Aluminum oxide
Anodic protection
Cathodic protection
Cerium
Chemistry
Chemistry and Materials Science
Contact angle
Conversion coatings
Corrosion prevention
Corrosion tests
Current density
Deposition
Electrochemical corrosion
Electrochemical impedance spectroscopy
Electrochemistry
Energy distribution
Industrial Chemistry/Chemical Engineering
Photoelectrons
Physical Chemistry
Primers (coatings)
Research Article
Spectrum analysis
Surface properties
X ray photoelectron spectroscopy
Title Optimal current density for cathodic CeCC deposition on anodized AA2024-T3 aircraft alloy
URI https://link.springer.com/article/10.1007/s10800-024-02143-7
https://www.proquest.com/docview/3118467099
Volume 54
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